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1. 发明授权

US09096441B2 Composition for manufacturing doped or undoped zinc oxide thin film and method for manufacturing zinc oxide thin film using same 有权
标题翻译：用于制造掺杂或未掺杂的氧化锌薄膜的组合物及其制造使用其的氧化锌薄膜的方法
公开(公告)号：US09096441B2
公开(公告)日：2015-08-04
申请号：US13265544
申请日：2010-04-21
申请人： Koichiro Inaba , Kouji Toyota , Kenichi Haga , Kouichi Tokudome
发明人： Koichiro Inaba , Kouji Toyota , Kenichi Haga , Kouichi Tokudome
IPC分类号： C01G9/02 , H01L31/18
CPC分类号： C01G9/02 , C01P2002/50 , C01P2002/52 , C01P2002/72 , C01P2002/86 , C01P2006/40 , C01P2006/42 , C01P2006/60 , H01L31/1884 , Y02E10/50
摘要： Disclosed is a composition for forming a zinc oxide thin film, which contains an organic zinc compound as a starting material, is not ignitable, and can be easily handled. The composition for forming a zinc oxide thin film is capable of forming a transparent zinc oxide thin film which is not doped or doped with a group 3B element by being heated at 300° C. or less. Also disclosed is a method for obtaining a transparent zinc oxide thin film, which is not doped or doped with a group 3B element, using the composition. Specifically, the composition for forming a zinc oxide thin film contains a product which is obtained by partially hydrolyzing an organic zinc compound by adding water to the organic zinc compound or a solution of the organic zinc compound and a group 3B element compound. In cases when a group 3B element compound is contained, the molar ratio of the group 3B element compound to the organic zinc compound is within the range of 0.005-0.3. The composition is applied to a substrate surface and then heated, thereby forming a zinc oxide thin film which is doped with the group 3B element.
摘要翻译：公开了一种用于形成氧化锌薄膜的组合物，其含有有机锌化合物作为原料，不可点燃，并且可以容易地处理。用于形成氧化锌薄膜的组合物能够通过在300℃或更低温度下加热而形成不掺杂3B族元素的透明氧化锌薄膜。还公开了使用该组合物获得不掺杂或掺杂有3B族元素的透明氧化锌薄膜的方法。具体地，用于形成氧化锌薄膜的组合物含有通过向有机锌化合物或有机锌化合物和3B族元素化合物的溶液中添加水部分水解有机锌化合物而获得的产物。在含有3B族元素化合物的情况下，3B族元素化合物与有机锌化合物的摩尔比在0.005〜0.3的范围内。将组合物施加到基材表面，然后加热，从而形成掺杂有3B族元素的氧化锌薄膜。

2. 发明申请

US20120094019A1 COMPOSITION FOR MANUFACTURING DOPED OR UNDOPED ZINC OXIDE THIN FILM AND METHOD FOR MANUFACTURING ZINC OXIDE THIN FILM USING SAME 有权
标题翻译：用于制造掺杂或未处理的氧化锌薄膜的组合物和使用其制造氧化锌薄膜的方法
公开(公告)号：US20120094019A1
公开(公告)日：2012-04-19
申请号：US13265544
申请日：2010-04-21
申请人： Koichiro Inaba , Kouji Toyota , Kenichi Haga , Kouichi Tokudome
发明人： Koichiro Inaba , Kouji Toyota , Kenichi Haga , Kouichi Tokudome
IPC分类号： C08K5/56 , B05D3/02 , B05D5/06 , C09D7/12
CPC分类号： C01G9/02 , C01P2002/50 , C01P2002/52 , C01P2002/72 , C01P2002/86 , C01P2006/40 , C01P2006/42 , C01P2006/60 , H01L31/1884 , Y02E10/50
摘要： Disclosed is a composition for forming a zinc oxide thin film, which contains an organic zinc compound as a starting material, is not ignitable, and can be easily handled. The composition for forming a zinc oxide thin film is capable of forming a transparent zinc oxide thin film which is not doped or doped with a group 3B element by being heated at 300° C. or less. Also disclosed is a method for obtaining a transparent zinc oxide thin film, which is not doped or doped with a group 3B element, using the composition. Specifically, the composition for forming a zinc oxide thin film contains a product which is obtained by partially hydrolyzing an organic zinc compound by adding water to the organic zinc compound or a solution of the organic zinc compound and a group 3B element compound. In cases when a group 3B element compound is contained, the molar ratio of the group 3B element compound to the organic zinc compound is within the range of 0.005-0.3. The composition is applied to a substrate surface and then heated, thereby forming a zinc oxide thin film which is doped with the group 3B element.
摘要翻译：公开了一种用于形成氧化锌薄膜的组合物，其含有有机锌化合物作为原料，不可点燃，并且可以容易地处理。用于形成氧化锌薄膜的组合物能够通过在300℃或更低温度下加热而形成不掺杂3B族元素的透明氧化锌薄膜。还公开了使用该组合物获得不掺杂或掺杂有3B族元素的透明氧化锌薄膜的方法。具体地，用于形成氧化锌薄膜的组合物含有通过向有机锌化合物或有机锌化合物和3B族元素化合物的溶液中添加水部分水解有机锌化合物而获得的产物。在含有3B族元素化合物的情况下，3B族元素化合物与有机锌化合物的摩尔比在0.005〜0.3的范围内。将组合物施加到基材表面，然后加热，从而形成掺杂有3B族元素的氧化锌薄膜。

3. 发明授权

US09156857B2 Diethylzinc composition, method for heat stabilization, and compound for heat stabilization 有权
标题翻译：二乙基锌组合物，热稳定化方法和热稳定化合物
公开(公告)号：US09156857B2
公开(公告)日：2015-10-13
申请号：US13989660
申请日：2011-12-15
申请人： Kenichi Haga , Shizuo Tomiyasu , Kohichi Tokudome , Kouji Toyota , Koichiro Inaba
发明人： Kenichi Haga , Shizuo Tomiyasu , Kohichi Tokudome , Kouji Toyota , Koichiro Inaba
IPC分类号： C07F3/06 , C08G65/12
CPC分类号： C07F3/06 , C08G65/12
摘要： [Object]To improve heat stability of diethylzinc which is used for a catalyst of polymerizing, an organic synthetic reaction reagent and a raw materials for providing a zinc film by MOCVD. And to offer the diethylzinc composition being superior in heat stability, even if it handles for a long term a metal zinc particle does not precipitate.[Means for Solving Problem]Use a diethylzinc composition added a compound which has particular carbon-carbon double bond to a diethylzinc.
摘要翻译：本发明提供用于聚合催化剂的二乙基锌的热稳定性，有机合成反应试剂和通过MOCVD提供锌膜的原料。并且为了提供热稳定性优异的二乙基锌组合物，即使其长期处理，金属锌颗粒也不会沉淀。 [解决问题的方法]使用二乙基锌组合物加入具有特定碳 - 碳双键的化合物至二乙基锌。

4. 发明申请

US20130281724A1 DIETHYLZINC COMPOSITION, METHOD FOR HEAT STABILIZATION, AND COMPOUND FOR HEAT STABILIZATION 有权
标题翻译：二氯乙烯组合物，热稳定化方法和用于热稳定化合物
公开(公告)号：US20130281724A1
公开(公告)日：2013-10-24
申请号：US13989660
申请日：2011-12-15
申请人： Kenichi Haga , Shizuo Tomiyasu , Kohichi Tokudome , Kouji Toyota , Koichiro Inaba
发明人： Kenichi Haga , Shizuo Tomiyasu , Kohichi Tokudome , Kouji Toyota , Koichiro Inaba
IPC分类号： C07F3/06
CPC分类号： C07F3/06 , C08G65/12
摘要： [Object]To improve heat stability of diethylzinc which is used for a catalyst of polymerizing, an organic synthetic reaction reagent and a raw materials for providing a zinc film by MOCVD. And to offer the diethylzinc composition being superior in heat stability, even if it handles for a long term a metal zinc particle does not precipitate.[Means for solving problem]Use a diethylzinc composition added a compound which has particular carbon-carbon double bond to a diethylzinc.
摘要翻译：本发明提供用于聚合催化剂的二乙基锌的热稳定性，有机合成反应试剂和通过MOCVD提供锌膜的原料。并且为了提供热稳定性优异的二乙基锌组合物，即使其长期处理，金属锌颗粒也不会沉淀。 [解决问题的方法]使用二乙基锌组合物向二乙基锌中加入特定碳 - 碳双键的化合物。

5. 发明授权

US08673413B2 Method for packing solid organometallic compound and packed container 有权
标题翻译：固体有机金属化合物和包装容器包装方法
公开(公告)号：US08673413B2
公开(公告)日：2014-03-18
申请号：US11340739
申请日：2006-01-27
申请人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
发明人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
IPC分类号： B29D22/00 , C23C16/00
CPC分类号： C23C16/4481 , Y10T428/13
摘要： A method for packing a solid organometallic compound into a container for packing the compound is provided, wherein the solid organometallic compound can be stably supplied to a vapor phase epitaxial growth apparatus such as an MOCVD apparatus at a constant concentration for a long period of time. In the method for packing a solid organometallic compound into a container for packing, the compound is composed of grains having a grain size of 8 mm or less and the grains of the compound essentially comprise grains having a grain size of 2.5 to 6 mm.
摘要翻译：提供了一种将固体有机金属化合物填充到用于填充化合物的容器中的方法，其中固体有机金属化合物可以长时间稳定地供给到恒定浓度的诸如MOCVD装置的气相外延生长装置。在将固体有机金属化合物填充到用于包装的容器中的方法中，化合物由粒径为8mm以下的晶粒构成，该化合物的晶粒基本上包含粒径为2.5〜6mm的晶粒。

6. 发明申请

US20070175397A1 Method for packing solid organometallic compound and packed container 有权
标题翻译：固体有机金属化合物和包装容器包装方法
公开(公告)号：US20070175397A1
公开(公告)日：2007-08-02
申请号：US11340739
申请日：2006-01-27
申请人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
发明人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
IPC分类号： C23C16/00
CPC分类号： C23C16/4481 , Y10T428/13
摘要： A method for packing a solid organometallic compound into a container for packing the compound is provided, wherein the solid organometallic compound can be stably supplied to a vapor phase epitaxial growth apparatus such as an MOCVD apparatus at a constant concentration for a long period of time. In the method for packing a solid organometallic compound into a container for packing, the compound is composed of grains having a grain size of 8 mm or less and the grains of the compound essentially comprise grains having a grain size of 2.5 to 6 mm.
摘要翻译：提供了一种将固体有机金属化合物填充到用于填充化合物的容器中的方法，其中固体有机金属化合物可以长时间稳定地供给到恒定浓度的诸如MOCVD装置的气相外延生长装置。在将固体有机金属化合物填充到用于包装的容器中的方法中，化合物由粒径为8mm以下的晶粒构成，化合物的粒子基本上包含粒径为2.5〜6mm的晶粒。

7. 发明授权

US08722561B2 Diethylzinc composition, method for heat stabilization, and compound for heat stabilization 有权
标题翻译：二乙基锌组合物，热稳定化方法和热稳定化合物
公开(公告)号：US08722561B2
公开(公告)日：2014-05-13
申请号：US13394129
申请日：2010-09-01
申请人： Kenichi Haga , Shizuo Tomiyasu , Kohichi Tokudome
发明人： Kenichi Haga , Shizuo Tomiyasu , Kohichi Tokudome
IPC分类号： C08F4/50 , C07C13/48 , C07C13/16 , C07C13/465
CPC分类号： C07F3/06 , C08F4/50 , C08F2410/01
摘要： [Object]To improve heat stability of diethylzinc which is used for a catalyst of polymerizing, an organic synthetic reaction reagent and a raw materials for providing a zinc film by MOCVD. And to offer the diethylzinc composition being superior in heat stability, even if it handles for a long term a metal zinc particle does not precipitate.[Solving Means]Use a diethylzinc composition added a compound which is added an aromatic compound as an additive which has isopropenyl group bonded as a side chain.
摘要翻译：本发明提供用于聚合催化剂的二乙基锌的热稳定性，有机合成反应试剂和通过MOCVD提供锌膜的原料。并且为了提供热稳定性优异的二乙基锌组合物，即使其长期处理，金属锌颗粒也不会沉淀。 [解决方法]使用二乙基锌组合物，加入加入芳族化合物作为侧链键合有异丙烯基的添加剂的化合物。

8. 发明申请

US20090283041A1 SOLID ORGANOMETALLIC COMPOUND-FILLED CONTAINER AND FILLING METHOD THEREOF 有权
标题翻译：固体有机化合物填充容器及其填充方法
公开(公告)号：US20090283041A1
公开(公告)日：2009-11-19
申请号：US12464333
申请日：2009-05-12
申请人： Shizuo TOMIYASU , Kohichi Tokudome , Kenichi Haga
发明人： Shizuo TOMIYASU , Kohichi Tokudome , Kenichi Haga
IPC分类号： C23C16/00 , B65B1/04
CPC分类号： C30B25/14 , C23C16/4481 , Y10T428/13
摘要： A solid organometallic compound novel filled container stably supplies an apparatus for vapor phase epitaxial growth such as an MOCVD apparatus with a solid organometallic compound over a long term. The solid organometallic compound-filled container has a carrier gas inlet and a carrier gas outlet. The interior of the filled container is separated into a plurality of vertical compartments. A carrier gas introduced via the carrier gas inlet flows through each of the vertical compartments and is then discharged via the carrier gas outlet.
摘要翻译：固体有机金属化合物新型填充容器长期稳定地供给诸如具有固体有机金属化合物的MOCVD装置的气相外延生长装置。固体有机金属化合物填充容器具有载气入口和载气出口。填充容器的内部被分成多个垂直隔室。通过载气进口引入的载气流过每个垂直隔室，然后通过载气出口排出。

9. 发明申请

US20120184432A1 DIETHYLZINC COMPOSITION, METHOD FOR HEAT STABILIZATION, AND COMPOUND FOR HEAT STABILIZATION 有权
标题翻译：二氯乙烯组合物，热稳定化方法和用于热稳定化合物
公开(公告)号：US20120184432A1
公开(公告)日：2012-07-19
申请号：US13394129
申请日：2010-09-01
申请人： Kenichi Haga , Shizuo Tomiyasu , Kohichi Tokudome
发明人： Kenichi Haga , Shizuo Tomiyasu , Kohichi Tokudome
IPC分类号： C08F4/50 , C07C13/48 , C07C13/16 , C07C13/465
CPC分类号： C07F3/06 , C08F4/50 , C08F2410/01
摘要： [Object]To improve heat stability of diethylzinc which is used for a catalyst of polymerizing, an organic synthetic reaction reagent and a raw materials for providing a zinc film by MOCVD. And to offer the diethylzinc composition being superior in heat stability, even if it handles for a long term a metal zinc particle does not precipitate.[Solving Means]Use a diethylzinc composition added a compound which is added an aromatic compound as an additive which has isopropenyl group bonded as a side chain.
摘要翻译：本发明提供用于聚合催化剂的二乙基锌的热稳定性，有机合成反应试剂和通过MOCVD提供锌膜的原料。并且为了提供热稳定性优异的二乙基锌组合物，即使其长期处理，金属锌颗粒也不会沉淀。 [解决方法]使用二乙基锌组合物，加入加入芳族化合物作为侧链键合有异丙烯基的添加剂的化合物。

10. 发明授权

US07547363B2 Solid organometallic compound-filled container and filling method thereof 有权
标题翻译：固体有机金属化合物填充容器及其填充方法
公开(公告)号：US07547363B2
公开(公告)日：2009-06-16
申请号：US10865880
申请日：2004-06-14
申请人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
发明人： Shizuo Tomiyasu , Kohichi Tokudome , Kenichi Haga
IPC分类号： C23C16/448 , C23C16/18 , C23C16/00
CPC分类号： C30B25/14 , C23C16/4481 , Y10T428/13
摘要： A solid organometallic compound novel filled container stably supplies an apparatus for vapor phase epitaxial growth such as an MOCVD apparatus with a solid organometallic compound over a long term. The solid organometallic compound-filled container has a carrier gas inlet and a carrier gas outlet. The interior of the filled container is separated into a plurality of vertical compartments. A carrier gas introduced via the carrier gas inlet flows through each of the vertical compartments and is then discharged via the carrier gas outlet.
摘要翻译：固体有机金属化合物新型填充容器长期稳定地供给诸如具有固体有机金属化合物的MOCVD装置的气相外延生长装置。固体有机金属化合物填充容器具有载气入口和载气出口。填充容器的内部被分成多个垂直隔室。通过载气进口引入的载气流过每个垂直隔室，然后通过载气出口排出。

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