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1. 发明授权

US07335675B2 Aqueous suspension formulation for foliar application fungicide 有权
标题翻译：用于叶面施用杀真菌剂的水性悬浮液制剂
公开(公告)号：US07335675B2
公开(公告)日：2008-02-26
申请号：US10564851
申请日：2004-07-07
申请人： Koichi Morinaga , Yuji Yanase , Kanemitsu Miyama , Hideo Kawashima
发明人： Koichi Morinaga , Yuji Yanase , Kanemitsu Miyama , Hideo Kawashima
IPC分类号： A01N43/56 , A01N25/04 , A01N25/30
CPC分类号： A01N43/56 , A01N25/24 , A01N25/30 , A01N25/04 , A01N2300/00
摘要： The present invention provides an aqueous suspension formulation containing (RS)-N-[2-(1,3-dimethylbutyl)thiophene-3-yl]-1-methyl-3-trifluoromethyl-1H-pyrazole-4-carboxamide and having high rain resistance and stable residual effectiveness.A aqueous suspension formulation for foliar application fungicide of the present invention contains a fungicidal active ingredient, (RS)-N-[2-(1,3-dimethylbutyl)thiophene-3-yl]-1-methyl-3-trifluoromethyl-1H-pyrazole-4-carboxamide, and a polyoxyalkylene rosin acid ester or liquid paraffin, and has improved rain resistance on plant leaves and excellent residual effectiveness.
摘要翻译：本发明提供含有（RS）-N- [2-（1,3-二甲基丁基）噻吩-3-基] -1-甲基-3-三氟甲基-1H-吡唑-4-甲酰胺并含有高耐雨性和稳定的残留效果。本发明的叶面施用杀真菌剂的水性悬浮液制剂含有杀真菌活性成分（RS）-N- [2-（1,3-二甲基丁基）噻吩-3-基] -1-甲基-3-三氟甲基-1H- - 吡唑-4-甲酰胺和聚氧化烯松香酸酯或液体石蜡，并且具有改善植物叶子的耐雨性和优异的残留效果。

2. 发明申请

US20060235066A1 Aqueous suspension preparation of bactericide for folieage application 有权
标题翻译：杀虫剂水性悬浮液制备方法
公开(公告)号：US20060235066A1
公开(公告)日：2006-10-19
申请号：US10564851
申请日：2004-07-07
申请人： Koichi Morinaga , Yuji Yanase , Kanemitsu Miyama , Hideo Kawashima
发明人： Koichi Morinaga , Yuji Yanase , Kanemitsu Miyama , Hideo Kawashima
IPC分类号： A01N43/56
CPC分类号： A01N43/56 , A01N25/24 , A01N25/30 , A01N25/04 , A01N2300/00
摘要： The present invention provides an aqueous suspension formulation containing (RS)—N-[2-(1,3-dimethylbutyl)thiophene-3-yl]-1-methyl-3-trifluoromethyl-1H-pyrazole-4-carboxamide and having high rain resistance and stable residual effectiveness. A aqueous suspension formulation for foliar application fungicide of the present invention contains a fungicidal active ingredient, (RS)—N-[2-(1,3-dimethylbutyl)thiophene-3-yl]-1-methyl-3-trifluoromethyl-1H-pyrazole-4-carboxamide, and a polyoxyalkylene rosin acid ester or liquid paraffin, and has improved rain resistance on plant leaves and excellent residual effectiveness.
摘要翻译：本发明提供含有（RS）-N- [2-（1,3-二甲基丁基）噻吩-3-基] -1-甲基-3-三氟甲基-1H-吡唑-4-甲酰胺并含有高耐雨性和稳定的残留效果。本发明的叶面施用杀真菌剂的水性悬浮液制剂含有杀真菌活性成分（RS）-N- [2-（1,3-二甲基丁基）噻吩-3-基] -1-甲基-3-三氟甲基-1H- - 吡唑-4-甲酰胺和聚氧化烯松香酸酯或液体石蜡，并且具有改善植物叶子的耐雨性和优异的残留效果。

3. 发明授权

US4654445A Preparation process of 2-chloropropionaldehyde 失效
标题翻译： 2-氯丙醛的制备方法
公开(公告)号：US4654445A
公开(公告)日：1987-03-31
申请号：US800966
申请日：1985-11-22
申请人： Hiroshi Ono , Kanemitsu Miyama , Takaharu Kasuga
发明人： Hiroshi Ono , Kanemitsu Miyama , Takaharu Kasuga
IPC分类号： C07C45/49 , C07C45/50
CPC分类号： C07C45/49
摘要： This invention relates to a process for preparing 2-chloropropionaldehyde (2-CPA) by using vinyl chloride, carbon monoxide and hydrogen as raw materials. Although processes making use of cobalt catalysts have conventionally been known, it is disclosed herein that by using a rhodium compound and a nitrogen- or phosphorus-containing Lewis base in combination as a catalyst, the reaction is allowed to proceed at temperature and pressure lower than those required for such conventional processes and the selectively toward the intended product is improved. It is also disclosed that by causing water to exist in the reaction system and using a water-insoluble organic solvent, fractionating the reaction mixture into a water layer and an organic layer after the reaction and then collecting 2-CPA from the water layer through distillation, extraction or the like, the rhodium compound contained substantially in its entirety in an organic layer can be reutilized in the form of its solution. This process is an extremely good process suitable for use in the preparation of 2-CPA which is useful as an intermediate for chemical products, agricultural chemicals, pharmaceutical products, etc.
摘要翻译：本发明涉及以氯乙烯，一氧化碳和氢为原料制备2-氯丙醛（2-CPA）的方法。虽然使用钴催化剂的方法通常是已知的，但是本文公开了通过组合使用铑化合物和含氮或磷的路易斯碱作为催化剂，使反应在低于这些常规方法所需的和选择性地朝向预期产品的那些被改进。还公开了通过使水存在于反应体系中并使用水不溶性有机溶剂，在反应后将反应混合物分馏成水层和有机层，然后通过蒸馏从水层中收集2-CPA ，提取物等，基本上在有机层中全部含有的铑化合物可以以其溶液的形式再利用。该方法是适用于制备2-CPA的非常好的方法，可用作化学产品，农药，药品等的中间体。

4. 发明授权

US5846904A Soil fumigant preparations 失效
标题翻译：土壤熏蒸剂
公开(公告)号：US5846904A
公开(公告)日：1998-12-08
申请号：US596490
申请日：1996-02-05
申请人： Masao Imai , Kanemitsu Miyama , Masaru Arai , Hitoshi Shimotori , Tamotsu Asano , Satoru Iwamori , Shohei Nozaki , Nobuhiro Fukuda
发明人： Masao Imai , Kanemitsu Miyama , Masaru Arai , Hitoshi Shimotori , Tamotsu Asano , Satoru Iwamori , Shohei Nozaki , Nobuhiro Fukuda
IPC分类号： A01N25/18 , A01N25/34 , A01N47/08 , A01N25/10
CPC分类号： A01N25/34 , A01N25/18 , A01N47/08
摘要： Described are a stick-shaped soil fumigant preparation and an application method therefor. The fumigant preparation comprises a water-soluble and/or biodegradable film and a soil sterilizer and/or nematocide hermetically packed in the form of a stick with the film. The soil sterilizer and nematocide are each in a liquid form at room temperature. The soil fumigant preparation according to the present invention remains suppressed in toxicity, volatility and irritation before application to the soil, but its active ingredient(s) are promptly released after application. In addition, the present invention makes it possible to provide a fumigant in such a form as permitting a substantial improvement in the efficiency of work by a fumigating worker and also to provide an effective application method therefor, without the need for any machine designed exclusively for fumigation.
摘要翻译：描述了一种棒状土壤熏蒸剂及其应用方法。熏蒸剂制剂包括水溶性和/或可生物降解的膜和以膜的形式气密地包装的土壤灭菌剂和/或杀线虫剂。土壤灭菌剂和杀线虫剂在室温下均为液体形式。根据本发明的土壤熏蒸剂制剂在施用于土壤之前仍然受到毒性，挥发性和刺激性的抑制，但其施用后其活性成分迅速释放。此外，本发明使得可以以允许熏蒸工人的工作效率显着提高的形式提供熏蒸剂，并且还提供了一种有效的施用方法，而不需要专门设计用于熏蒸。

5. 发明授权

US5268506A Process for producing .alpha., .beta.-unsaturated carboxylic acid 失效
标题翻译：生产α，β-不饱和羧酸的方法
公开(公告)号：US5268506A
公开(公告)日：1993-12-07
申请号：US34464
申请日：1993-03-19
申请人： Minato Karasawa , Takeshi Hiraiwa , Sinji Tokunoh , Hiroharu Kageyama , Kanemitsu Miyama , Masamitsu Inomata
发明人： Minato Karasawa , Takeshi Hiraiwa , Sinji Tokunoh , Hiroharu Kageyama , Kanemitsu Miyama , Masamitsu Inomata
IPC分类号： B01J27/18 , C07C51/06 , C07C57/065 , C07C51/353 , C07C57/04
CPC分类号： B01J27/1804 , C07C51/06
摘要： An .alpha., .beta.-unsaturated carboxylic acid is produced by catalytically reacting an .alpha.-hydroxycarboxylic acid amide of the formula (1), ##STR1## where R.sub.1 and R.sub.2 are independently selected from the group consisting of hydrogen and C.sub.1 -C.sub.4 alkyl groups, provided that at least one of R.sub.1 and R.sub.2 is the alkyl group, with water in the presence of a solid acid catalyst containing a high surface area rare earth phosphate anhydride having the monoclinic system structure producible by heating a rare earth phosphate of the hexagonal system structure at 60.degree.-200.degree. C. in a solution of an inorganic acid, an inorganic acid salt and/or an inorganic acid ester where the molar ratio of the inorganic acid component to the rare earth phosphate of the hexagonal system structure is 0.5-400.

6. 发明授权

US5387715A Process for producing .alpha.-hydroxy-isobutyramide 失效
标题翻译： α-羟基 - 异丁酰胺的制备方法
公开(公告)号：US5387715A
公开(公告)日：1995-02-07
申请号：US983700
申请日：1992-02-01
申请人： Minato Karasawa , Masamitsu Inomata , Hiroharu Kageyama , Kanemitsu Miyama
发明人： Minato Karasawa , Masamitsu Inomata , Hiroharu Kageyama , Kanemitsu Miyama
IPC分类号： B01J23/34 , C07C231/06
CPC分类号： C07C231/065 , B01J23/34
摘要： Alpha-hydroxy-isobutyramide is produced by continuously hydrating acetone cyanohydrin in a liquid phase in the presence of a manganese dioxide catalyst and in the presence of a particular oxide dissolved in water, oxoacid, heteropolyacid or a salt of the acids.
摘要翻译： α-羟基 - 异丁酰胺通过在二氧化锰催化剂的存在下和溶于水，含氧酸，杂多酸或酸的盐的特定氧化物存在下，以液相连续水合丙酮氰醇来制备。

7. 发明授权

US5276185A Process for producing amide compounds 失效
标题翻译：酰胺化合物的制备方法
公开(公告)号：US5276185A
公开(公告)日：1994-01-04
申请号：US997111
申请日：1992-12-24
申请人： Minato Karasawa , Masamitsu Inomata , Hiroharu Kageyama , Masahiro Tokumitsu , Sinji Tokunoh , Kanemitsu Miyama
发明人： Minato Karasawa , Masamitsu Inomata , Hiroharu Kageyama , Masahiro Tokumitsu , Sinji Tokunoh , Kanemitsu Miyama
IPC分类号： C07C231/06
CPC分类号： C07C231/065
摘要： Amides are produced by reacting nitriles with water in a liquid phase in the presence of a manganese oxide containing an element selected from Groups IIIA, IVA, VA, IIIB, IVB, VB , VIB and VIII of the Periodic Table.
摘要翻译：酰胺通过在含有选自元素周期表的IIIA，IVA，VA，IIIB，IVB，VB，VIB和VIII族元素的锰氧化物存在下，在液相中使腈与水反应制备。

8. 发明授权

US5268503A Process for producing .alpha.,.beta.-unsaturated carboxylic acid esters 失效
标题翻译：制备α，β-不饱和羧酸酯的方法
公开(公告)号：US5268503A
公开(公告)日：1993-12-07
申请号：US29419
申请日：1993-03-09
申请人： Minato Karasawa , Sinji Tokunoh , Masamitsu Inomata , Takeshi Hiraiwa , Hiroharu Kageyama , Kanemitsu Miyama
发明人： Minato Karasawa , Sinji Tokunoh , Masamitsu Inomata , Takeshi Hiraiwa , Hiroharu Kageyama , Kanemitsu Miyama
IPC分类号： C07C67/08 , C07C67/20
CPC分类号： C07C67/08 , C07C67/20
摘要： .alpha.,.beta.-Unsaturated carboxylic acid esters are produced by a catalytic reaction of .alpha.,.beta.-unsaturated carboxylic acids and/or .alpha.,.beta.-unsaturated carboxylic acid amides with aliphatic alcohols in the presence of a solid acid catalyst comprising zirconium oxide, titanium oxide or a composite oxide thereof containing phosphorus.

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