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JP2011038977A Separation analysis method and separation analysis apparatus for redox material 有权
标题翻译：红外材料的分离分析方法和分离分析装置
公开(公告)号：JP2011038977A
公开(公告)日：2011-02-24
申请号：JP2009188756
申请日：2009-08-17
申请人： Kobe Univ , Sumitomo Electric Ind Ltd , 住友電気工業株式会社 , 国立大学法人神戸大学
发明人： SUGIHARA TAKAYASU , NAKAYAMA MOKICHI , OSAKAI TOSHIYUKI
IPC分类号： G01N27/416
摘要： PROBLEM TO BE SOLVED: To provide a separation analysis method and a separation analysis apparatus which are useful for separating a redox material in a sample solution by utilizing a redox reaction.
SOLUTION: The separation analysis apparatus is configured so that an eluent R (mobile phase) is fed to a separation-use flow type electrolytic cell 10 (separation column electrode 100) and a separation-use flow type electrolytic cell 20 (detection column electrode 200) successively through a sample injector 32 (injecting means) by using a pump 31 (liquid feeding means). When separating and analyzing the redox material in the sample solution, the sample solution is injected from the sample injector 32 and introduced into the separation column electrode 100, and then a pulse voltage is repeatedly applied while making the sample solution flow in the separation column electrode 100, thereby separating the redox material contained in the sample solution. Next, a pulse voltage is applied to the detection column electrode 200, and the concentration of the redox material in the sample solution is analyzed on the basis of a value of a current flowing at that time.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种分离分析方法和分离分析装置，其可用于通过利用氧化还原反应分离样品溶液中的氧化还原材料。解决方案：分离分析装置被配置为使得洗脱液R（流动相）被供给到分离用流动型电解槽10（分离柱电极100）和分离用流动型电解槽20（检测列电极200）通过使用泵31（液体供给装置）连续地通过样品注射器32（喷射装置）。当分析和分析样品溶液中的氧化还原材料时，将样品溶液从样品注射器32注入并引入分离柱电极100中，然后在使样品溶液流入分离柱电极的同时重复施加脉冲电压 100，从而分离样品溶液中所含的氧化还原材料。接下来，向检测用列电极200施加脉冲电压，根据该时刻流过的电流值对样品溶液中的氧化还原材料的浓度进行分析。版权所有（C）2011，JPO＆INPIT

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