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1. 发明授权

US5380827A Water-soluble monoazodye containing a triazinyl or pyrimidinyl group and at least one vinyl sulfonyl type group in its structure 失效
标题翻译：其结构中含有三嗪基或嘧啶基和至少一个乙烯基磺酰基类的水溶性一抗体
公开(公告)号：US5380827A
公开(公告)日：1995-01-10
申请号：US49410
申请日：1993-04-20
申请人： Yousuke Takahashi , Yukiharu Shimizu , Toshio Hihara , Kiyoshi Himeno
发明人： Yousuke Takahashi , Yukiharu Shimizu , Toshio Hihara , Kiyoshi Himeno
IPC分类号： C09B62/51 , C09B62/44 , C09B62/028 , C09B62/085 , C09B62/245
CPC分类号： C09B62/4413 , C09B62/4424 , C09B62/51
摘要： A water-soluble monoazodye having the following formula (I) in its free acid form: ##STR1## wherein X is --CH.dbd.CH.sub.2 or --CH.sub.2 CH.sub.2 W wherein W is a leaving group removable by alkali; R.sup.1 is methyl, --NHCONH.sub.2 or --NHCOT.sup.1 wherein T.sup.1 is methyl, ethyl, --CH.sub.2 CH.sub.2 COOH or --CH.dbd.CHCOOH; R.sup.2 is hydrogen, lower alkyl or lower alkoxy;and Z is ##STR2## wherein P is cyano or halogen, each of Q and U which are independent of each other, is halogen, V is halogen or ##STR3## and Y is halogen or a group of the following formula (1) or (2): ##STR4## wherein R.sup.3, A, R.sup.4 and E are as defined in the disclosure and G is as defined above, has a moderate yellow to orange color and is particularly suitable for dyeing cellulose fibers or nitrogen-containing fibers.
摘要翻译：具有游离酸形式的下式（I）的水溶性单偶氮：其中X为-CH = CH 2或-CH 2 CH 2 W，其中W为可由碱除去的离去基团; 乙烯基，-CH 2 CH 2 COOH或-CH = CHCOOH; R 1为甲基，-NHCONH 2或-NHCOT 1，其中T 1为甲基， R2是氢，低级烷基或低级烷氧基; 其中P为氰基或卤素，Q和U各自独立地为卤素，V为卤素或式（1）或（2）：（1）N（ESO 2 X ）2（2）其中R3，A，R4和E如本公开中所定义，G如上所定义，具有中等的黄色至橙色，并且特别适用于染色纤维素纤维或含氮纤维。

2. 发明授权

US5744588A Blue type disperse dye mixture and process for its preparation 失效
标题翻译：蓝色分散染料混合物及其制备方法
公开(公告)号：US5744588A
公开(公告)日：1998-04-28
申请号：US729027
申请日：1996-10-09
申请人： Kiyoshi Himeno , Toshio Hihara , Yousuke Takahashi
发明人： Kiyoshi Himeno , Toshio Hihara , Yousuke Takahashi
IPC分类号： C09B67/22 , C09B41/00
CPC分类号： C09B67/0051 , Y10S534/01 , Y10S8/922
摘要： A blue type disperse dye mixture comprising 1.0 part by weight of at least one dye of the formula (1), from 0 to 0.2 part by weight of at least one dye of the formula (2), from 0.05 to 1.0 part by weight of at least one dye of the formula (3) and from 0.05 to 1.0 part by weight of at least one dye of the formula (4): ##STR1## wherein X is a chlorine atom or a bromine atom, R.sup.1 is a C.sub.1-5 alkyl group, R.sup.2 is a C.sub.1-4 alkyl group, and R.sup.3 is a C.sub.1-5 alkyl group or an allyl group, provided that R.sup.1, R.sup.2 and R.sup.3 may, respectively, be the same or different among the formulae (1) to (4).
摘要翻译：一种蓝色分散染料混合物，其包含1.0重量份的至少一种式（1）的染料，0至0.2重量份的至少一种式（2）的染料，0.05至1.0重量份的式至少一种式（3）的染料和0.05至1.0重量份的至少一种式（4）的染料：（1）（2）原子或溴原子，R 1 是C1-5烷基，R2是C1-4烷基，R3是C1-5烷基或烯丙基，条件是R1，R2和R3可以分别相同或不同，在式（1）〜（4）。

3. 再颁专利

USRE37004E Water-soluble monoazodye containing a triazinyl or pyrimidinyl group and at least one vinyl sulfonyl type group in its structure 失效
标题翻译：其结构中含有三嗪基或嘧啶基和至少一个乙烯基磺酰基类的水溶性一抗体
公开(公告)号：USRE37004E
公开(公告)日：2000-12-26
申请号：US916366
申请日：1997-08-22
申请人： Yousuke Takahashi , Yukihara Shimizu , Toshio Hihara , Kiyoshi Himeno
发明人： Yousuke Takahashi , Yukihara Shimizu , Toshio Hihara , Kiyoshi Himeno
IPC分类号： C09B62/51 , C09B62/44 , C09B62/028 , C09B62/085 , C09B62/245
CPC分类号： C09B62/4413 , C09B62/4424 , C09B62/51
摘要： A water-soluble monoazodye having the following formula (I) in its free acid form: ##STR1## wherein X is --CH.dbd.CH.sub.2 or --CH.sub.2 CH.sub.2 W wherein W is a leaving group removable by alkali; R.sup.1 is methyl, --NHCONH.sub.2 or --NHCOT.sup.1 wherein T.sup.1 is methyl, ethyl, --CH.sub.2 CH.sub.2 COOH or --CH.dbd.CHCOOH; R.sup.2 is hydrogen, lower alkyl or lower alkoxy; and Z is ##STR2## wherein P is cyano or halogen, each of Q and U which are independent of each other, is halogen, V is halogen or ##STR3## and Y is halogen or a group of the following formula (1) or (2): ##STR4## wherein R.sup.3, A, R.sup.4 and E are as defined in the disclosure and G is as defined above, has a moderate yellow to orange color and is particularly suitable for dyeing cellulose fibers or nitrogen-containing fibers.
摘要翻译：具有游离酸形式的具有下式（I）的水溶性一抗体：其中X是-CH = CH 2或-CH 2 CH 2 W，其中W是可以被碱除去的离去基团; 乙烯基，-CH 2 CH 2 COOH或-CH = CHCOOH; R 1为甲基，-NHCONH 2或-NHCOT 1，其中T 1为甲基， R2是氢，低级烷基或低级烷氧基; 和Z是其中P是氰基或卤素，Q和U各自彼此独立，是卤素，V是卤素或Y是卤素或下式（1）或（2）的基团：其中R3 A，R4和E如本文所定义，G如上所定义，具有中等的黄色至橙色，并且特别适用于染色纤维素纤维或含氮纤维。

4. 发明授权

US5595575A Blue disperse dye mixture 失效
标题翻译：蓝色分散染料混合物
公开(公告)号：US5595575A
公开(公告)日：1997-01-21
申请号：US555171
申请日：1995-11-08
申请人： Kiyoshi Himeno , Toshio Hihara , Ryouichi Sekioka
发明人： Kiyoshi Himeno , Toshio Hihara , Ryouichi Sekioka
IPC分类号： C09B67/22 , D06P3/54
CPC分类号： C09B67/0051 , C09B67/0046 , Y10S8/922
摘要： A blue disperse dye mixture comprising a monoazo dye of the following formula (1) and at least one azo dye selected from the group consisting of dyes of the following formulas (2), (3), (4) and (5): ##STR1## wherein each of the variables is defined in the specification.
摘要翻译：包含下式（1）的单偶氮染料和至少一种选自下式（2），（3），（4）和（5）的染料的偶氮染料的蓝色分散染料混合物：GE （4）（5）其中每个变量在说明书中定义。

5. 发明授权

US5332404A Disperse dye mixtures 失效
标题翻译：分散染料混合物
公开(公告)号：US5332404A
公开(公告)日：1994-07-26
申请号：US988813
申请日：1992-12-10
申请人： Kiyoshi Himeno , Toshio Hihara , Hirotsugu Tsumura , Yoshiharu Hamano
发明人： Kiyoshi Himeno , Toshio Hihara , Hirotsugu Tsumura , Yoshiharu Hamano
IPC分类号： C09B67/22 , C09B67/38 , D06P1/18 , D06P3/54
CPC分类号： C09B67/0051 , C09B67/008 , D06P1/18 , Y10S8/922
摘要： A disperse dye mixture comprising a monoazo dye of the following formula (1) and a monoazo dye of the following formula (2) blended thereto in an amount of from 0.1 to 10 times by weight of the dye of the formula (1): ##STR1## wherein each of X.sup.1 and X.sup.2 which are independent of each other, is nitro, cyano, sulfomethyl or halogen, each of Y.sup.1, Y.sup.2, Z.sup.1 and Z.sup.2 which are independent of one another, is hydrogen, cyano, nitro, trifluoromethyl, halogen or sulfomethyl, each of W.sup.1 and W.sup.2 which are independent of each other, is hydrogen, halogen, C.sub.1 -C.sub.2 alkyl or alkoxy, and each of R.sup.1 and R.sup.2 which are independent of each other, is C.sub.1 -C.sub.4 alkyl, or C.sub.2 -C.sub.4 alkyl which is substituted by cyano, halogen, hydroxy, hydroxyalkoxy, C.sub.1 -C.sub.4 alkyl, hydroxyalkoxyalkoxy, acyloxyalkoxy, acyloxyalkoxyalkoxy or alkoxyalkoxy.
摘要翻译：一种分散染料混合物，其包含下式（1）的单偶氮染料和下式（2）的单偶氮染料，其量为式（1）染料的0.1-10倍重量：（1）其中X1和X2各自独立的是硝基，氰基，磺基甲基或卤素，Y1，Y2，Z1和Z2各自独立地是氢，氰基，硝基，三氟甲基，卤素或磺基甲基各自独立地为氢，卤素，C 1 -C 2烷基或烷氧基，R 1和R 2各自独立地为 C 1 -C 4烷基或被氰基，卤素，羟基，羟基烷氧基，C 1 -C 4烷基，羟基烷氧基烷氧基，酰氧基烷氧基，酰氧基烷氧基烷氧基或烷氧基烷氧基取代的C 2 -C 4烷基。

6. 发明授权

US5734028A Blue type disperse dye mixture 失效
标题翻译：蓝色分散染料混合物
公开(公告)号：US5734028A
公开(公告)日：1998-03-31
申请号：US732723
申请日：1996-10-18
申请人： Kiyoshi Himeno , Toshio Hihara , Ryouchi Sekioka
发明人： Kiyoshi Himeno , Toshio Hihara , Ryouchi Sekioka
IPC分类号： C09B67/22 , D06P1/18 , D06P1/20 , D06P3/54
CPC分类号： C09B67/0041 , D06P1/18 , D06P1/20 , Y10S534/01
摘要： A blue type disperse dye mixture comprising a monoazo dye of the formula (1) in an amount of 1.0 part by weight and at least one of anthraquinone dyes of the formulae (2) to (4) in a total amount of from 0.2 to 3.0 parts by weight: ##STR1##
摘要翻译：一种蓝色分散染料混合物，其包含1.0重量份的式（1）的单偶氮染料和至少一种式（2）至（4）的蒽醌染料，其总量为0.2-3.0 （1）（2）（3）（4）

7. 发明授权

US5368612A Method of dyeing a fiber mixture with water-insoluble naphthalic acid imide dyestuffs 失效
标题翻译：用水不溶性萘二甲酰亚胺染料染色纤维混合物的方法
公开(公告)号：US5368612A
公开(公告)日：1994-11-29
申请号：US100294
申请日：1993-08-02
申请人： Kiyoshi Himeno , Toshio Hihara
发明人： Kiyoshi Himeno , Toshio Hihara
IPC分类号： C09B62/02 , D06P1/382
CPC分类号： C09B62/021 , Y10S8/922 , Y10S8/924 , Y10S8/926
摘要： Water-insoluble naphthalic acid imide dyestuffs of the following formula: ##STR1## wherein D is ##STR2## wherein R.sup.1 is C.sub.1 -C.sub.8 alkyl which may be substituted, R.sup.2 is hydrogen, halogen, lower alkyl, lower alkoxy or cyano, X is oxygen or sulfur, and m is 0 or 1; A is phenylene, alkylene, aralkylene or --C.sub.2 H.sub.4 OC.sub.2 H.sub.4 --; B is oxygen, sulfur or ##STR3## wherein R.sup.3 is hydrogen or lower alkyl; Y is a 6-membered nitrogen-containing heterocyclic ring having at least one active halogen atom; and n is 0 or 1.
摘要翻译：下式的水不溶性萘二甲酰亚胺染料：其中D是其中R 1是可被取代的C 1 -C 8烷基，R 2是氢，卤素，低级烷基，低级烷氧基或氰基， X是氧或硫，m是0或1; A是亚苯基，亚烷基，亚芳基或-C 2 H 4 OC 2 H 4 - ; B是氧，硫或者其中R 3是氢或低级烷基; Y是具有至少一个活性卤素原子的6元含氮杂环; n为0或1。

8. 发明授权

US4743684A Reactive phthalocyanine dyes 失效
标题翻译：活性酞菁染料
公开(公告)号：US4743684A
公开(公告)日：1988-05-10
申请号：US766312
申请日：1985-08-16
申请人： Toshio Niwa , Kiyoshi Himeno , Toshio Hihara , Kanzi Shimizu
发明人： Toshio Niwa , Kiyoshi Himeno , Toshio Hihara , Kanzi Shimizu
IPC分类号： C09B47/04 , C09B62/10 , C09B62/523 , D06P1/382
CPC分类号： D06P1/382 , C09B62/10
摘要： A reactive phthalocyanine dye having a specific substituent capable of dyeing cellulose fibers or a mixed fibers of polyester fibers and cellulose fibers to provide Turkish blue-dyed fibers excellent in color fastness to light and color fastness to washing is disclosed, which is represented by general formula [I] ##STR1##
摘要翻译：公开了具有能够染色纤维素纤维的特定取代基的反应性酞菁染料或聚酯纤维和纤维素纤维的混合纤维，以提供具有优异的耐色牢度和耐洗色牢度的土耳其蓝染色纤维，其通式为 [I] [I]

9. 发明授权

US4707546A Reactive monoazo dyestuffs 失效
标题翻译：活性单偶氮染料
公开(公告)号：US4707546A
公开(公告)日：1987-11-17
申请号：US822680
申请日：1986-01-23
申请人： Toshio Niwa , Kiyoshi Himeno , Toshio Hihara
发明人： Toshio Niwa , Kiyoshi Himeno , Toshio Hihara
IPC分类号： C09B62/085 , C09B62/343 , D06P1/382 , D06P3/85
CPC分类号： C09B62/085
摘要： A reactive monoazo dyestuff of the general formula [I]: ##STR1## wherein R.sup.1 and R.sup.2 each represents substituted or unsubstituted alkyl, cyclohexyl, aralkyl or substituted or unsubstituted aryl, Z represents hydrogen, chlorine, methyl or acylamino, (A) represents substituted or unsubstituted alkylene, (B) represents oxygen or --NH--, X represents fluorine or chlorine, and Y represents --NR.sup.4 R.sup.5 or --OR.sup.6 wherein R.sup.4, R.sup.5 and R.sup.6 each represents hydrogen, substituted or unsubstituted alkyl, alkenyl, cyclohexyl, aryl or aralkyl, or --NR.sup.4 R.sup.5 represents a 5- or 6-membered nitrogen-containing heterocyclic ring formed by combining R.sup.4 and R.sup.5.
摘要翻译：通式[I]的反应性单偶氮染料：其中R 1和R 2各自表示取代或未取代的烷基，环己基，芳烷基或取代或未取代的芳基，Z表示氢，氯，甲基或酰氨基，（A ）表示取代或未取代的亚烷基，（B）表示氧或-NH-，X表示氟或氯，Y表示-NR4R5或-OR6，其中R4，R5和R6各自表示氢，取代或未取代的烷基，烯基，环己基，芳基或芳烷基，或-NR4R5表示通过组合R4和R5形成的5-或6-元含氮杂环。

10. 发明授权

US4623719A Disazo dyestuffs having a monofluorotriazinyl group 失效
标题翻译：具有单氟三嗪基的双偶氮染料
公开(公告)号：US4623719A
公开(公告)日：1986-11-18
申请号：US843927
申请日：1986-03-24
申请人： Toshio Niwa , Kiyoshi Himeno , Toshio Hihara
发明人： Toshio Niwa , Kiyoshi Himeno , Toshio Hihara
IPC分类号： C09B31/14 , C09B62/09 , D06P1/382 , C07C107/06
CPC分类号： D06P1/382 , C09B62/09
摘要： This invention relates to disazo dyestuffs for cellulose or cellulose-containing fibers represented by the formula: ##STR1## wherein R.sup.1 represents a hydrogen atom, a nitro group, a halogen atom, an alkyl group of 1 or 2 carbon atoms or an acetylamino group; R.sup.2 and R.sup.3 each represents a hydrogen atom, an alkyl group of 1 or 2 carbon atoms, and alkoxy group or an acetylamino group; Y.sup.1 and Y.sup.2 each represents a hydrogen atom or an alkyl group, and alkenyl group, a cyclohexyl group, an aryl group or an aralkyl group which group ma optionally be substituted by cyano, hydroxyl, lower alkoxy or dialkylamino, or NY.sup.1 Y.sup.2 represents a 5-membered or 6-membered nitrogen-containing heretocyclic ring formed by combination of Y.sup.1 and Y.sup.2, and the total carbon atoms in Y.sup.1 and Y.sup.2 is 18 or less.
摘要翻译：本发明涉及由下式表示的纤维素或含纤维素纤维的双偶氮染料：其中R1表示氢原子，硝基，卤素原子，1或2个碳原子的烷基或乙酰氨基; R2和R3各自表示氢原子，1或2个碳原子的烷基和烷氧基或乙酰氨基; Y1和Y2各自表示氢原子或烷基，以及基团任选被氰基，羟基，低级烷氧基或二烷基氨基取代的烯基，环己基，芳基或芳烷基，或者NY1Y2表示5- 通过Y1和Y2的组合形成的6-元或6元含氮杂环，Y1和Y2中的总碳原子数为18以下。

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