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1. 发明授权

US5532334A Process for preparing polyamideimide resins having high molecular weight 失效
标题翻译：制备高分子量聚酰胺酰亚胺树脂的方法
公开(公告)号：US5532334A
公开(公告)日：1996-07-02
申请号：US339391
申请日：1994-11-14
申请人： Kil-Yeong Choi , Dong-Hack Suh , Mi-Hie Yi , Young-Taik Hong , Jong-Chan Won
发明人： Kil-Yeong Choi , Dong-Hack Suh , Mi-Hie Yi , Young-Taik Hong , Jong-Chan Won
IPC分类号： C08G73/14 , H01B3/30 , C08G69/26
CPC分类号： C08G73/14 , H01B3/303
摘要： A process for preparing polyamideimide resins having high molecular weights as described wherein major problems of prior art processes such as low heat resistance and low melt flowability are improved. Polyamideimide resins having an intrinsic viscosity of 0.4 to 1.50 dl/g as measured on a solution of dimethylacetamide as a solvent at a concentration of 0.5 g/dl at 30.degree. C., are prepared by reacting an aromatic tricarboxylic acid anhydride with an aromatic diamine in N-methyl pyrrolidone solvent in the presence of a first catalyst selected from a group consisting of thionyl chloride, p-toluenesulphonly chloride, sulfuryl chloride, cyanuric chloride and phosphorus trichloride at a temperature of 50.degree. C. to 130.degree. C. over a period of 1 to 5 hours and further reacting the resultant reaction mixture in the presence of a second catalyst which is a compound of the formula (RO).sub.3 P wherein R is an aliphatic or aromatic substituent, or a compound which is phosphoric acid, pyrophosphoric acid, phosphorous pentaoxide or phosphorous pentachloride as a second catalyst at a temperature of 50.degree. C. to 130.degree. C. over a period of 1 to 5 hours.
摘要翻译：制备如上所述的具有高分子量的聚酰胺酰亚胺树脂的方法，其中提高了诸如低耐热性和低熔融流动性的现有技术方法的主要问题。通过在30℃下以0.5g / dl的浓度作为溶剂的二甲基乙酰胺溶液测定的特性粘度为0.4至1.50dl / g的聚酰胺酰亚胺树脂通过芳族三羧酸酐与芳族二胺在N-甲基吡咯烷酮溶剂中，在50℃至130℃的温度下，在选自亚硫酰氯，对甲苯磺酰氯，磺酰氯，氰尿酰氯和三氯化磷的第一催化剂存在下，在时间为1至5小时，并且在第二催化剂存在下进一步反应，所述第二催化剂是式（RO）3P的化合物，其中R是脂族或芳族取代基，或者是磷酸化合物，焦磷酸，五氧化二磷或五氯化磷作为第二催化剂，温度为50〜130℃，时间为1〜5小时。

2. 发明授权

US5955568A Process for preparing polyamideimide resins by direct polymerization 失效
标题翻译：通过直接聚合制备聚酰胺酰亚胺树脂的方法
公开(公告)号：US5955568A
公开(公告)日：1999-09-21
申请号：US956923
申请日：1997-10-23
申请人： Kil-Yeong Choi , Dong-Hack Suh , Mi-Hie Yi , Young-Taik Hong , Moon-Young Jin
发明人： Kil-Yeong Choi , Dong-Hack Suh , Mi-Hie Yi , Young-Taik Hong , Moon-Young Jin
IPC分类号： C08G73/14 , C08G69/28
CPC分类号： C08G73/14
摘要： The disclosure describes a process for preparing a polyamideimide resin having high molecular weight in a simple manner wherein major problems of the prior processes such as low heat resistance and low melt flowability are improved. The process comprises condensation of an aromatic tricarboxylic acid anhydride and an aromatic diamine in a polar solvent, subjecting the resulting diimidedicarboxylic acid to acyl halogenating agent treatment to give an intermediate having good reactivity at low temperature, and then subjecting the latter to direct polymerization by using diamine as a nucleophilic agent to give a polyamideimide resin having high molecular weight. The polyamideimide resin prepared by the present invention can be used as major heat resistant structural material in advanced industries and as paint, sheet, adhesives, sliding material, fiber and film having heat resistance.
摘要翻译：本公开内容描述了以简单的方式制备具有高分子量的聚酰胺酰亚胺树脂的方法，其中诸如低耐热性和低熔融流动性的现有方法的主要问题得到改善。该方法包括在极性溶剂中将芳族三羧酸酐和芳族二胺缩合，将所得二酰亚胺二羧酸进行酰卤处理，得到在低温下具有良好反应性的中间体，然后使用后者通过使用二胺作为亲核剂，得到具有高分子量的聚酰胺酰亚胺树脂。本发明制备的聚酰胺酰亚胺树脂可用作先进工业中的主要耐热结构材料，可用作具有耐热性的油漆，片材，粘合剂，滑动材料，纤维和薄膜。

3. 发明授权

US5919942A Cyclohexane-1,2,4,5-diimide derivative and process for preparing the same 失效
标题翻译：环己烷-1,4,5-二酰亚胺衍生物及其制备方法
公开(公告)号：US5919942A
公开(公告)日：1999-07-06
申请号：US879977
申请日：1997-06-20
申请人： Kil-Yeong Choi , Dong-Hack Suh , Young-Taik Hong , Sang-Hyun Park
发明人： Kil-Yeong Choi , Dong-Hack Suh , Young-Taik Hong , Sang-Hyun Park
IPC分类号： C07D487/04 , C08G73/10
CPC分类号： C07D487/04 , C08G73/10
摘要： The disclosure describes a cyclohexane-1,2,4,5-diimide derivative which can be used for the production of colorless transparent polymer and novel engineering plastics having good processability and solubility with an excellent physical property, and a process for preparing the same which comprises reacting a bicyclooctene-1,2,4,5-tetracarboxylic anhydride with alkylamine and aniline derivative and then oxidizing the resulting product with ozone, potassium permanganate, ruthenium chloride hydroxide and aqeous hydrogen peroxide under non-basic condition to convert double bond to dicarboxylic acid or dialdehyde without destroying the imide group.
摘要翻译：本公开内容描述了可用于生产无色透明聚合物的环己烷-1,2,4,5-二酰亚胺衍生物和具有优异物理性能的具有良好加工性和溶解性的新型工程塑料及其制备方法，包括使双环辛烯-1,2,4,5-四羧酸酐与烷基胺和苯胺衍生物反应，然后在非碱性条件下用臭氧，高锰酸钾，氯化钌和过氧化氢氧化所得产物，以将双键转化成二羧酸酸或二醛，而不会破坏酰亚胺基团。

4. 发明授权

US6018055A Polyarylether containing N-substituted imide groups and process for producing the same 失效
标题翻译：含有N-取代的酰亚胺基团的聚芳醚基及其制备方法
公开(公告)号：US6018055A
公开(公告)日：2000-01-25
申请号：US892707
申请日：1997-07-15
申请人： Kil-Yeong Choi , Dong-Hack Suh , Young-Taik Hong , Eun-Young Chung
发明人： Kil-Yeong Choi , Dong-Hack Suh , Young-Taik Hong , Eun-Young Chung
IPC分类号： C07D487/04 , C08G65/40 , C08G73/06 , C07D487/02
CPC分类号： C07D487/04 , C08G73/0672
摘要： A polyarylether of the formula (VIII) ##STR1## wherein wherein Z' is 1-3 optionally substituted rings selected from the group consisting of an aromatic ring, a hetero aromatic ring or an aliphatic ring.A is --R.sub.1 --Z--Y in which R.sub.1 is H, C.sub.1 -C.sub.30 -alkyl or -aralkyl or phenyl, Z is a direct bond or CH.sub.2, S, O or NH, Y is CH.sub.3, OR.sub.3, SR.sub.3, NHR.sub.3, N(R.sub.3).sub.2, COOR.sub.3, COOM, SO.sub.3 R.sub.3 or SO.sub.3 M in which R.sub.3 is C.sub.1 -C.sub.30 alkyl and M is alkali metal,produced from 3,6-dihalogen- or -dintro-1,2,4,5-diimide having an N,N-substituent and which is suitable for use as a monomer for high temperature structural and functional polymers, and a process for producing the same are disclosed.
摘要翻译：式（VIII）的聚芳醚，其中Z'为1-3个选自芳香环，杂芳环或脂族环的任选取代的环。 A是-R1-ZY，其中R1是H，C1-C30 - 烷基或 - 烷基或苯基，Z是直接键或CH2，S，O或NH，Y是CH3，OR3，SR3，NHR3，N ）2，CO 3，COOM，SO 3 R 3或SO 3 M，其中R 3为C 1 -C 30烷基且M为碱金属，由具有N，N的3,6-二卤代 - 或二苯并1,2,4,5-二酰亚胺并且其适合用作高温结构和功能性聚合物的单体，并且公开了其制备方法。

5. 发明授权

US09000157B2 Metallic compound and organic electroluminescence device comprising the same 有权
标题翻译：金属化合物和包含其的有机电致发光器件
公开(公告)号：US09000157B2
公开(公告)日：2015-04-07
申请号：US12913274
申请日：2010-10-27
申请人： Dong-Hack Suh , Jin-Sik Choi , Jin-Soo Lim , Song-Ho Kim , Dae-Beom Kim
发明人： Dong-Hack Suh , Jin-Sik Choi , Jin-Soo Lim , Song-Ho Kim , Dae-Beom Kim
IPC分类号： C07F1/00 , C07F3/00 , C07F3/08 , C07F5/00 , C07F5/06 , C07F7/00 , C07F9/00 , C07F11/00 , C07F13/00 , C07F15/00 , C07F17/00 , H05B33/14 , C09K11/06
CPC分类号： H05B33/14 , C09K11/06 , C09K2211/185
摘要： The present invention relates to an organic electroluminescence device containing a light emitting metallic compound of Chemical Formula 1. In the Chemical Formula 1, M is selected from Ir, Pt, Rh, Re, and Os, and m is 2, provided that m is 1 when M is Pt.
摘要翻译：本发明涉及含有化学式1的发光金属化合物的有机电致发光元件。在化学式1中，M选自Ir，Pt，Rh，Re和Os，m为2，条件是m为 1当M为Pt时。

6. 发明申请

US20080200678A1 Metallic Compound and Organic Electroluminescence Device Comprising the Same 有权
标题翻译：金属化合物及其组成的有机电致发光器件
公开(公告)号：US20080200678A1
公开(公告)日：2008-08-21
申请号：US11913216
申请日：2007-01-08
申请人： Dong-Hack Suh , Jin-Soo Lim , Ji-Ho Kim , Sun-Hyun Choi
发明人： Dong-Hack Suh , Jin-Soo Lim , Ji-Ho Kim , Sun-Hyun Choi
IPC分类号： C07D213/79 , C07D263/52
CPC分类号： C07F15/0033
摘要： The present invention relates to a light-emitting transition metal compound represented by the Chemical Formula 1 and Chemical Formula 2 and an organic electroluminescence device including the same.In the Chemical Formulae 1 and 2, M is Ir, Pt, Rh, Re, Os, and the like, m is 2 or 3, n is 0 or 1, the sum of m and n is 3, provided that the sum of m and n is 2 when M is Pt, X, and Z are the same or different, N or P, and Y and Q are O, S, or Se, R1 and R5 are hydrogen, a C1 to C20 alkyl excluding an aromatic cyclic substituent, a cycloalkyl, a halogen, a linear or branched substituent including at least one halogen, or a linear or branched substituent including at least one heteroatom, and R2, R3, R4, R6, R7, R8, R9, and R10 are hydrogen, a C1 to C20 alkyl, an aryl, a cycloalkyl, a halogen, a linear or branched substituent including at least one halogen, a linear or branched substituent including at least one heteroatom, carbonyl, vinyl, or acetylenyl, or may form a cycle, and may be the same or different.
摘要翻译：本发明涉及由化学式1和化学式2表示的发光过渡金属化合物和包含其的有机电致发光器件。在化学式1和2中，M是Ir，Pt，Rh，Re，Os等，m是2或3，n是0或1，m和n之和是3，条件是当M是Pt，X和Z相同或不同时，N和P分别为2，Y和Q为O，S或Se，R 1和R 2彼此相同或不同， 5是氢，不包括芳族环状取代基的C1至C20烷基，环烷基，卤素，包含至少一个卤素的直链或支链取代基或包含至少一个杂原子的直链或支链取代基，R R 2，R 3，R 4，R 6，R 7，R 7，R 7， R 9，R 9和R 10是氢，C 1至C 20烷基，芳基，环烷基，卤素，直链或支链取代基，包括至少一个卤素，包括至少一个杂原子的直链或支链取代基，羰基，乙烯基或乙炔基，或可以形成一个环，并且可以相同或不同。

7. 发明授权

US07973168B2 Metallic compound and organic electroluminescence device comprising the same 有权
标题翻译：金属化合物和包含其的有机电致发光器件
公开(公告)号：US07973168B2
公开(公告)日：2011-07-05
申请号：US11913222
申请日：2007-01-08
申请人： Dong-Hack Suh , Jin-Soo Lim , Ji-Ho Kim , Sun-Hyun Choi
发明人： Dong-Hack Suh , Jin-Soo Lim , Ji-Ho Kim , Sun-Hyun Choi
IPC分类号： C07F15/00 , H01J1/63
CPC分类号： H05B33/14 , C07F15/0033 , C09K11/06 , C09K2211/185 , H01L51/0085 , H01L51/009 , H01L51/5016 , Y10S428/917
摘要： The present invention relates to a light emitting binuclear transition metal compound of Chemical Formulae 1 and 2, and an organic electroluminescence device including the compound. In the Chemical Formulae 1 and 2, M is selected from Ir, Pt, Rh, Re, and Os, and m is 2, provided that the m is 1 when M is Pt.
摘要翻译：本发明涉及化学式1和2的发光双核过渡金属化合物和包含该化合物的有机电致发光器件。在化学式1和2中，M选自Ir，Pt，Rh，Re和Os，m为2，条件是当M为Pt时m为1。

8. 发明授权

US07858783B2 Metallic compound and organic electroluminescence device comprising the same 有权
标题翻译：金属化合物和包含其的有机电致发光器件
公开(公告)号：US07858783B2
公开(公告)日：2010-12-28
申请号：US11913196
申请日：2007-01-08
申请人： Dong-Hack Suh , Jin-Sik Choi , Jin-Soo Lim , Song-Ho Kim , Dae-Beom Kim
发明人： Dong-Hack Suh , Jin-Sik Choi , Jin-Soo Lim , Song-Ho Kim , Dae-Beom Kim
IPC分类号： C07F1/00 , C07F3/00 , C07F3/08 , C07F5/00 , C07F5/06 , C07F7/00 , C07F9/00 , C07F11/00 , C07F13/00 , C07F15/00 , C07F17/00
CPC分类号： H05B33/14 , C09K11/06 , C09K2211/185
摘要： The present invention relates to a light emitting metallic compound of Chemical Formula 1 and an organic electroluminescence device including the compound. In the Chemical Formula 1, M is selected from Ir, Pt, Rh, Re, and Os, and m is 2, provided that m is 1 when M is Pt.
摘要翻译：本发明涉及化学式1的发光金属化合物和包含该化合物的有机电致发光器件。在化学式1中，M选自Ir，Pt，Rh，Re和Os，m为2，条件是当M为Pt时m为1。

9. 发明申请

US20080193795A1 Metallic Compound and Organic Electroluminescence Device Comprising the Same 有权
标题翻译：金属化合物及其组成的有机电致发光器件
公开(公告)号：US20080193795A1
公开(公告)日：2008-08-14
申请号：US11910161
申请日：2007-04-10
申请人： Dong-Hack Suh , Song-Ho Kim , Chi-Hum Kim , Dae-Beom Kim
发明人： Dong-Hack Suh , Song-Ho Kim , Chi-Hum Kim , Dae-Beom Kim
IPC分类号： C09K11/06 , B32B9/00 , C07F17/02
CPC分类号： C09K11/06 , C07F15/0033 , C09K2211/1011 , C09K2211/1029 , C09K2211/1033 , C09K2211/1037 , C09K2211/1044 , C09K2211/1059 , C09K2211/1092 , C09K2211/185 , H05B33/14 , Y10S428/917
摘要： The present invention relates to a light emitting metallic compound of Chemical Formula 1 and an organic electroluminescence device including the compound. In the Chemical Formula 1, M is selected from Ir, Pt, Rh, Re, and Os, m is 2, provided that m is 1 when M is Pt. X is a N or P atom, Y is S, O, or Se, and Z is SiR5R6, CR5R6, PR5, S, SO2, carbonyl, or NR5, and L2 is represented by Chemical Formulae 2, 3, or 4. R1, R2, R3, R4, R5, R6, R7, and R8 are the same or different, and are selected from hydrogen, a C1 to C20 alkyl, an aryl, a cycloalkyl, a halogen, a linear or branched substituent including at least one halogen, a linear or branched substituent including at least one heteroatom, carbonyl, vinyl, and acetylenyl, or may form a cycle, and R9 is hydrogen, a C1 to C20 alkyl excluding an aromatic cyclic substituent, a cycloalkyl, a halogen, a linear or branched substituent including at least one halogen; or a linear or branched substituent including at least one heteroatom.
摘要翻译：本发明涉及化学式1的发光金属化合物和包含该化合物的有机电致发光器件。在化学式1中，M选自Ir，Pt，Rh，Re和Os，m为2，条件是当M为Pt时m为1。 X是N或P原子，Y是S，O或Se，Z是SiR 5 R 6，CR 5， SUP 6，PR 5，S，SO 2，羰基或NR 5，L 2， / SUP>由化学式2,3或4表示。R 1，R 2，R 3，R 4， R 5，R 6，R 7，R 8和R 8相同或不同，并且选自氢，C1至C20烷基，芳基，环烷基，卤素，包括至少一个卤素的直链或支链取代基，包括至少一个杂原子的直链或支链取代基，羰基，乙烯基和乙炔基或可以形成一个周期，R 9是氢，不包括芳族环状取代基的C 1至C 20烷基，环烷基，卤素，包括至少一个卤素的直链或支链取代基; 或包含至少一个杂原子的直链或支链取代基。

10. 发明授权

US07939669B2 Metallic compound and organic electroluminescence device comprising the same 有权
标题翻译：金属化合物和包含其的有机电致发光器件
公开(公告)号：US07939669B2
公开(公告)日：2011-05-10
申请号：US11913192
申请日：2007-01-08
申请人： Dong-Hack Suh , Jin-Sik Choi , Jin-Soo Lim , Song-Ho Kim , Chi-Hun Kim
发明人： Dong-Hack Suh , Jin-Sik Choi , Jin-Soo Lim , Song-Ho Kim , Chi-Hun Kim
IPC分类号： C07D277/62 , C07D263/54
CPC分类号： H05B33/10 , C07F15/004 , C09K11/06 , C09K2211/1007 , C09K2211/1029 , C09K2211/1033 , C09K2211/1044 , C09K2211/1059 , C09K2211/1096 , H01L51/0085 , H01L51/009
摘要： The present invention relates to a light emitting transition metal compound of Chemical Formula 1 and an organic electroluminescence device including the compound.In the Chemical Formula 1, M is selected from Ir, Pt, Rh, Re, and Os, m is 2 or 3, n is 0 or 1, the sum of m and n is 3, provided that the sum of m and n is 2 M is Pt. X is a N or P atom, and Y is S, O, or Se.
摘要翻译：本发明涉及化学式1的发光过渡金属化合物和包含该化合物的有机电致发光器件。在化学式1中，M选自Ir，Pt，Rh，Re和Os，m为2或3，n为0或1，m和n之和为3，条件是m和n之和是2 M是Pt。 X是N或P原子，Y是S，O或Se。

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