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1. 发明授权

US5395983A Process for producing 1-phenyl-1,3-propanediols having high optical purtiy 失效
标题翻译：具有高光学纯度的1-苯基-1,3-丙二醇的方法
公开(公告)号：US5395983A
公开(公告)日：1995-03-07
申请号：US182566
申请日：1994-01-18
申请人： Kazutoshi Miyazawa , Teruyo Sugiura , Yasuyuki Koizumi , Naoyuki Yoshida
发明人： Kazutoshi Miyazawa , Teruyo Sugiura , Yasuyuki Koizumi , Naoyuki Yoshida
IPC分类号： C07C29/78 , C07C33/26 , C07C29/76
CPC分类号： C07C29/78 , C07C33/26 , C07B2200/07
摘要： R or S-1-phenyl-1,3-propanediols having optical purity of 100% ee were obtained by recrystallization of R or S-1-phenyl-1,3-propanediols having optical purity of 20% ee to below 100% ee, the last diols are represented by the formula, ##STR1## It is possible to obtain optically pure 1-phenyl-3-propanediols from optically impure 1-phenyl-1,3-propanediols by a simple method.
摘要翻译：光学纯度为100％ee的R或S-1-苯基-1,3-丙二醇通过将光学纯度为20％ee的R或S-1-苯基-1,3-丙二醇重结晶至低于100％ee ，最后的二醇由下式表示：通过简单的方法可以从光学上不纯的1-苯基-1,3-丙二醇获得光学上纯的1-苯基-3-丙二醇。

2. 发明授权

US5449793A Process for producing an optically active 1,5-disubstituted-2,4-O-isopropylidene-2,4-dihydroxypentane 失效
标题翻译：光学活性1,5-二取代-2,4-O-异亚丙基-2,4-二羟基戊烷的制造方法
公开(公告)号：US5449793A
公开(公告)日：1995-09-12
申请号：US241994
申请日：1994-05-12
申请人： Kazutoshi Miyazawa , Teruyo Sugiura , Yasuyuki Koizumi , Naoyuki Yoshida
发明人： Kazutoshi Miyazawa , Teruyo Sugiura , Yasuyuki Koizumi , Naoyuki Yoshida
IPC分类号： C07D319/06 , C12P7/62 , C12P17/06 , C12P41/00
CPC分类号： C12P17/06 , C07D319/06 , C12P41/004 , C12P7/62
摘要： A novel optically active erythro-1-alkanoyloxy-2,4-O-isopropylidene-2,4-dihydroxy-5-substituted pentane expressed by the formula ##STR1## wherein R.sup.1 represents a halogen atom or cyano group and R.sup.2 represents an alkyl group of 1 to 6 carbon atoms, and a process for producing the above compound are provided, the compound being preferably usable as an intermediate for preparing a HMG-CoA reductase inhibitor and the process being practiced under mild conditions and with a high yield.
摘要翻译：由式（1）表示的新型光学活性的赤式-1-烷酰氧基-2,4-O-异亚丙基-2,4-二羟基-5-取代戊烷，其中R 1表示卤素原子或氰基，R 2表示提供1〜6个碳原子的烷基和上述化合物的制造方法，该化合物优选用作制备HMG-CoA还原酶抑制剂的中间体，该方法在温和条件下以高产率进行。

3. 发明授权

US5266728A Method for producing optically active 3-substituted-2-norbornanones and their intermediates 失效
标题翻译：光学活性3-取代-2-降冰片烯酮及其中间体的制备方法
公开(公告)号：US5266728A
公开(公告)日：1993-11-30
申请号：US931993
申请日：1992-08-19
申请人： Naoyuki Yoshida , Teruyo Sugiura , Kazutoshi Miyazawa , Yasuyuki Koizumi
发明人： Naoyuki Yoshida , Teruyo Sugiura , Kazutoshi Miyazawa , Yasuyuki Koizumi
IPC分类号： C07C45/29 , C07C45/68 , C07C49/433 , C07C49/653 , C07C49/657 , C07C61/13 , C07C61/29 , C07C62/06 , C07D207/40 , C07D207/408
CPC分类号： C07D207/408 , C07C45/29 , C07C45/68 , C07C49/433 , C07C49/653 , C07C49/657 , C07C61/13 , C07C61/29 , C07C62/06 , C07C2102/42
摘要： The present invention provides a method for producing optically active 3-substituted-2-norbornanones which are useful as starting materials for several kinds of physiologically active materials, and to their intermediates, optically active 2-hydroxy-2-norbornanecarboxylic acid and to a method for producing these intermediates.

4. 发明授权

US5395766A Optically active trans-2-aryl-1-cyclohexanol derivatives and a process for producing the compounds 失效
标题翻译：光学活性的反式-2-芳基-1-环己醇衍生物及其制备方法
公开(公告)号：US5395766A
公开(公告)日：1995-03-07
申请号：US968311
申请日：1992-10-29
申请人： Yasuyuki Koizumi , Naoyuki Yoshida , Teruyo Sugiura , Kazutoshi Miyazawa
发明人： Yasuyuki Koizumi , Naoyuki Yoshida , Teruyo Sugiura , Kazutoshi Miyazawa
IPC分类号： C07D309/12 , C07C37/56 , C07C39/17 , C07C41/26 , C07C43/23 , C07C43/253 , C07C67/03 , C07C69/013 , C07C69/03 , C07D453/02 , C07F7/18 , C12P41/00 , C07D315/00 , C07C41/00 , C07C69/00
CPC分类号： C07C43/23 , C07C69/013 , C07D453/02 , C07C2101/14
摘要： The present invention provides an optically active trans-2-aryl-1-cyclohexanol derivative represented by the following general formula (I). ##STR1## The compounds can be obtained by transesterifiation reaction of the following compound (II) as a starting material with lipase. ##STR2## The optically active trans-2-aryl-1-cyclohexanol derivative can be used as an asymmetric source of asymmetric Diels-Alder reaction or a starting material of physiological active materials.
摘要翻译：本发明提供由以下通式（I）表示的光学活性的反式-2-芳基-1-环己醇衍生物。以下化合物（II）作为原料与脂肪酶的反应反应。（II）光学活性的反式-2-芳基-1-环己醇衍生物可用作不对称狄尔斯 - 阿尔德反应的不对称来源或生理活性物质的原料。

5. 发明授权

US5329018A Optically active 1-5-disubstituted-2,4-o-isopropylidene-2,4-dihydroxypentane and a process for producing the same 失效
标题翻译：光学活性的1-5-二取代-2,4-O-异亚丙基-2,4-二羟基戊烷及其制备方法
公开(公告)号：US5329018A
公开(公告)日：1994-07-12
申请号：US70985
申请日：1993-06-04
申请人： Kazutoshi Miyazawa , Teruyo Sugiura , Yasuyuki Koizumi , Naoyuki Yoshida
发明人： Kazutoshi Miyazawa , Teruyo Sugiura , Yasuyuki Koizumi , Naoyuki Yoshida
IPC分类号： C07D319/06 , C12P7/62 , C12P17/06 , C12P41/00
CPC分类号： C07D319/06 , C12P17/06 , C12P41/004 , C12P7/62
摘要： A novel optically active erythro-1-alkanoyloxy-2,4-O-isopropylidene-2,4-dihydroxy-5-substituted pentane expressed by the formula ##STR1## wherein R.sup.1 represents a halogen atom or cyano group and R.sup.2 represents an alkyl group of 1 to 6 carbon atoms, and a process for producing the above compound are provided, the compound being preferably usable as an intermediate for preparing a HMG-CoA reductase inhibitor and the process being practiced under mild conditions and with a high yield.
摘要翻译：由式（1）表示的新型光学活性的赤式-1-烷酰氧基-2,4-O-异亚丙基-2,4-二羟基-5-取代戊烷，其中R 1表示卤素原子或氰基，R 2表示提供1〜6个碳原子的烷基和上述化合物的制造方法，该化合物优选用作制备HMG-CoA还原酶抑制剂的中间体，该方法在温和条件下以高产率进行。

6. 发明授权

US06319570B1 Liquid crystalline compound, liquid crystal composition comprising the liquid crystal-line compound, and liquid crystal display device using the liquid crystal composition 有权
标题翻译：液晶化合物，包含液晶线化合物的液晶组合物和使用该液晶组合物的液晶显示装置
公开(公告)号：US06319570B1
公开(公告)日：2001-11-20
申请号：US09597280
申请日：2000-06-19
申请人： Tugumiti Andou , Shuichi Matsui , Kazutoshi Miyazawa , Hiroyuki Takeuchi , Yasuyuki Koizumi , Yasuko Sekiguchi , Etsuo Nakagawa , Fusayuki Takeshita
发明人： Tugumiti Andou , Shuichi Matsui , Kazutoshi Miyazawa , Hiroyuki Takeuchi , Yasuyuki Koizumi , Yasuko Sekiguchi , Etsuo Nakagawa , Fusayuki Takeshita
IPC分类号： C09K1934
CPC分类号： C07D239/26 , C07C43/192 , C07C43/225 , C07C69/753 , C07C69/76 , C07D319/06 , C09K19/04 , C09K19/0403 , C09K19/3001 , C09K19/3066 , C09K19/3068 , C09K19/42 , C09K19/44 , C09K19/46 , C09K2019/0407 , C09K2019/0448 , C09K2019/0451 , C09K2019/3027 , Y10T428/10
摘要： The invention is to provide liquid crystalline compounds which have a low viscosity, high negative dielectric anisotropy, high resistivity, and high voltage holding ratio, and are stable against heat and ultraviolet light; to provide liquid crystal compositions comprising the liquid crystalline compound; and to provide liquid crystal display devices using the liquid crystal composition therein; the liquid crystalline compound is expressed by the general formula (1) wherein R1 and Y1 represent an alkyl group having 1 to 20 carbon atoms; X1, X2, and X3 independently represent single bond, 1,2-ethylene group, vinylene group, —COO—, —CF2O—, or —OCF2—; ring A1, ring A2, ring A3, and ring A4 independently represent trans-1,4-cycloliexylene, or 1,4-phenylene hydrogen atom on the ring may be replaced by fluorine atom or chlorine atom provided that at least one of ring A2, ring A3, and ring A4 represents 2,3-difluoro-1,4-phenylene; m and n are 0 or 1, and each element which constitutes this compound may be replaced by its isotope.
摘要翻译：本发明提供具有低粘度，高负电介质各向异性，高电阻率和高电压保持率的液晶化合物，并且对于热和紫外光是稳定的; 以提供包含液晶化合物的液晶组合物; 并提供使用其中的液晶组合物的液晶显示装置;液晶化合物由通式（1）表示，其中R 1和Y 1表示具有1至20个碳原子的烷基; X1，X2和X3独立地表示单键，1,2-亚乙基，亚乙烯基，-COO-，-CF2O-或-OCF2-; 环A1，环A2，环A3和环A4独立地表示反式-1,4-亚噻二环，或者环上的1,4-亚苯基氢原子可以被氟原子或氯原子代替，条件是环A2中的至少一个环A3，环A4表示2,3-二氟-1,4-亚苯基; m和n为0或1，并且构成该化合物的每个元素可以被其同位素代替。

7. 发明授权

US5776367A Alkenylcyclohexane derivatives, liquid crystal composition and liquid crystal display element 失效
标题翻译：烯基环己烷衍生物，液晶组合物和液晶显示元件
公开(公告)号：US5776367A
公开(公告)日：1998-07-07
申请号：US666832
申请日：1996-06-19
申请人： Shuichi Matsui , Yasuyuki Koizumi , Takashi Kato , Kazutoshi Miyazawa , Norihisa Hachiya , Etsuo Nakagawa
发明人： Shuichi Matsui , Yasuyuki Koizumi , Takashi Kato , Kazutoshi Miyazawa , Norihisa Hachiya , Etsuo Nakagawa
IPC分类号： C07C13/28 , C07C255/50 , C07C255/55 , C09K19/30 , C09K19/42 , C09K19/44 , C09K19/46 , C07C19/08 , C09K19/52
CPC分类号： C09K19/46 , C07C13/28 , C07C255/50 , C07C255/55 , C09K19/3001 , C09K19/3028 , C09K19/3048 , C09K19/42 , C09K19/44 , C07C2101/14 , C09K2019/0448 , C09K2019/0451
摘要： A novel liquid crystalline compound having a low viscosity and a high elastic constant ratio and at the same time, a superior compatibility with other known liquid crystalline compounds, and a liquid crystal composition and a liquid crystal display element containing the novel compound, are provided. The compound is an alkenylcyclohexane derivative expressed by the formula (1): ##STR1## wherein R.sup.1 and R.sup.2 represent a linear or branched alkyl group of 1 to 15 carbon atoms or alkenyl group of 2 to 15 carbon atoms; at least one of R.sup.1 and R.sup.2 represents an alkenyl group; in these groups, one or more non-adjacent CH.sub.2 groups may be replaced by oxygen atom, sulfur atom or --C.tbd.C-- group; ring A.sup.1, ring A.sup.2 and ring A.sup.3 each independently represent 1,4-cyclohexylene group wherein one or more CH.sub.2 groups on the ring may be replaced by oxygen atom or sulfur atom, or 1,4-phenylene group wherein one or more CH groups on the ring may be replaced by nitrogen atom; Z.sup.1 and Z.sup.2 each independently represent --CH.sub.2 CH.sub.2 --, --CH.sub.2 O--, --OCH.sub.2 --, --CH.dbd.CH--, --C.tbd.C-- or single bond; Z.sup.3 represents --(CH.sub.2).sub.4 --, --CH.dbd.CH--(CH.sub.2).sub.2 --, --CH.sub.2 --CH.dbd.CH--CH.sub.2 -- or --(CH.sub.2).sub.2 --CH.dbd.CH--; and m, n and i each independently represent 0 or 1.
摘要翻译：提供了具有低粘度和高弹性常数比的新型液晶化合物，同时与其它已知的液晶化合物具有优异的相容性，以及液晶组合物和含有该新化合物的液晶显示元件。化合物是由式（1）表示的烯基环己烷衍生物：其中R1和R2表示碳原子数为1〜15的直链或支链烷基或碳原子数2〜15的烯基; R 1和R 2中的至少一个表示烯基; 在这些基团中，一个或多个不相邻的CH 2基团可以被氧原子，硫原子或-C 3 D C基团取代; 环A1，环A2和环A3各自独立地表示1,4-亚环己基，其中环上的一个或多个CH 2基团可以被氧原子或硫原子替代，或1,4-亚苯基，其中一个或多个CH基团在该环可以被氮原子取代; Z 1和Z 2各自独立地表示-CH 2 CH 2 - ， - CH 2 O - ， - OCH 2 - ， - CH = CH - ， - C 3BOND C-或单键; Z 3表示 - （CH 2）4 - ， - CH = CH-（CH 2）2 - ， - CH 2 -CH = CH-CH 2 - 或 - （CH 2）2 -CH = CH-; m，n和i各自独立地表示0或1。

8. 发明授权

US5755994A Ester derivative, liquid crystal composition and liquid crystal display element 失效
标题翻译：酯衍生物，液晶组合物和液晶显示元件
公开(公告)号：US5755994A
公开(公告)日：1998-05-26
申请号：US605776
申请日：1996-02-22
申请人： Tomoyuki Kondo , Shuichi Matsui , Yasuyuki Koizumi , Koichi Shibata , Yasuhiro Haseba , Norihisa Hachiya , Etsuo Nakagawa , Kazutoshi Miyazawa
发明人： Tomoyuki Kondo , Shuichi Matsui , Yasuyuki Koizumi , Koichi Shibata , Yasuhiro Haseba , Norihisa Hachiya , Etsuo Nakagawa , Kazutoshi Miyazawa
IPC分类号： C07C69/773 , C09K19/20 , C09K19/30 , C09K19/42 , C09K19/46 , C07C41/00 , C07C69/76
CPC分类号： C09K19/3068 , C09K19/2007 , C09K19/3001 , C09K19/42 , C09K19/46
摘要： A novel liquid crystalline compound having a large dielectric anisotropy value, a small change in the threshold voltage depending upon temperatures, and an improved solubility in other liquid crystal materials at low temperatures, and a liquid crystal composition containing the compound are provided, which liquid crystalline compound is expressed by the formula (1) ##STR1## wherein R is H or an alkyl group of 1 to 10C; l is an integer of 1 to 9; m, n and o are each independently 0 or 1; A.sub.1, A.sub.2 and A.sub.3 are each independently trans-1,4-cyclohexylene group, 1,4-phenylene group, one or more H atoms on the ring of which group may be replaced by F, or the like group; Z.sub.1, Z.sub.2 and Z.sub.3 are each independently --COO--, etc., but at least one of them is --COO--; X is CF.sub.3, etc.; and Y.sub.1, and Y.sub.2 are each independently H or F.
摘要翻译：提供了具有大的介电各向异性值，根据温度的阈值电压的小的变化以及在低温下在其它液晶材料中的溶解度的改进的新型液晶化合物和含有该化合物的液晶组合物，化合物由式（1）表示：其中R是H或1至10的烷基; l为1〜9的整数; m，n和o各自独立地为0或1; A1，A2和A3各自独立地为反式-1,4-亚环己基，1,4-亚苯基，其中一个或多个可被F取代基的H原子或类似基团; Z1，Z2和Z3各自独立地为-COO-等，但它们中的至少一个为-COO-; X是CF3等; Y1和Y2各自独立地为H或F.

9. 发明授权

US06190576B1 Liquid crystal compounds, liquid crystal compostions containing the compounds, and liquid crystal display devices made by using the compositions 有权
标题翻译：液晶化合物，含有该化合物的液晶组合物，以及使用该组合物制成的液晶显示装置
公开(公告)号：US06190576B1
公开(公告)日：2001-02-20
申请号：US09155595
申请日：1998-09-30
申请人： Tugumiti Andou , Shuichi Matsui , Kazutoshi Miyazawa , Hiroyuki Takeuchi , Yasuyuki Koizumi , Yasuko Sekiguchi , Etsuo Nakagawa , Fusayuki Takeshita
发明人： Tugumiti Andou , Shuichi Matsui , Kazutoshi Miyazawa , Hiroyuki Takeuchi , Yasuyuki Koizumi , Yasuko Sekiguchi , Etsuo Nakagawa , Fusayuki Takeshita
IPC分类号： C09K1934
CPC分类号： C07D239/26 , C07C43/192 , C07C43/225 , C07C69/753 , C07C69/76 , C07D319/06 , C09K19/04 , C09K19/0403 , C09K19/3001 , C09K19/3066 , C09K19/3068 , C09K19/42 , C09K19/44 , C09K19/46 , C09K2019/0407 , C09K2019/0448 , C09K2019/0451 , C09K2019/3027 , Y10T428/10
摘要： The invention is to provide liquid crystalline compounds which have a low viscosity, high negative dielectric anisotropy, high resistivity, and high voltage holding ratio, and are stable against heat and ultraviolet light; to provide liquid crystal compositions comprising the liquid crystalline compound; and to provide liquid crystal display devices using the liquid crystal composition therein; the liquid crystalline compound is expressed by the general formula (1) wherein R1 and Y1 represent an alkyl group having 1 to 20 carbon atoms; X1, X2, and X3 independently represent single bond, 1,2-ethylene group, vinylene group, —COO—, —CF2O—, or —OCF2—; ring A1, ring A2, ring A3, and ring A4 independently represent trans-1,4-cyclohexylene, or 1,4-phenylene hydrogen atom on the ring may be replaced by fluorine atom or chlorine atom provided that at least one of ring A2, ring A3, and ring A4 represents 2,3-difluoro-1,4-phenylene; m and n are 0 or 1, and each element which constitutes this compound may be replaced by its isotope.
摘要翻译：本发明提供具有低粘度，高负电介质各向异性，高电阻率和高电压保持率的液晶化合物，并且对于热和紫外光是稳定的; 以提供包含液晶化合物的液晶组合物; 并提供使用其中的液晶组合物的液晶显示装置;液晶化合物由通式（1）表示，其中R 1和Y 1表示具有1至20个碳原子的烷基; X1，X2和X3独立地表示单键，1,2-亚乙基，亚乙烯基，-COO-，-CF2O-或-OCF2-; 环A1，环A2，环A3和环A4独立地表示反式-1,4-亚环己基，或环上的1,4-亚苯基氢原子可以被氟原子或氯原子代替，条件是环A2中的至少一个环A3，环A4表示2,3-二氟-1,4-亚苯基; m和n为0或1，并且构成该化合物的每个元素可以被其同位素代替。

10. 发明授权

US5820784A Liquid crystal compostion and liquid crystal display device 失效
标题翻译：液晶组合液晶显示装置
公开(公告)号：US5820784A
公开(公告)日：1998-10-13
申请号：US606032
申请日：1996-02-22
申请人： Tomoyuki Kondo , Shuichi Matsui , Yasuyuki Koizumi , Koichi Shibata , Yasuhiro Haseba , Norihisa Hachiya , Etsuo Nakagawa , Kazutoshi Miyazawa
发明人： Tomoyuki Kondo , Shuichi Matsui , Yasuyuki Koizumi , Koichi Shibata , Yasuhiro Haseba , Norihisa Hachiya , Etsuo Nakagawa , Kazutoshi Miyazawa
IPC分类号： C07C69/773 , C09K19/20 , C09K19/30 , C09K19/42 , C09K19/46
CPC分类号： C09K19/3068 , C09K19/2007 , C09K19/3001 , C09K19/42 , C09K19/46
摘要： A liquid crystal composition is disclosed which contains, as the first component, at least one compound expressed by the formula (I-a) or (I-b) and contains, as the second component, at least one compound expressed by any one of the formulas (II-a) to (II-g), each of the formulas being recited in the specification. According to the present invention, a liquid crystal composition which is particularly excellent in compatibility in low temperatures, and has a suitably large .DELTA.n and a small V.sub.th can be provided while satisfying several characteristics required for liquid crystal compositions for AM-LCD.
摘要翻译：公开了一种液晶组合物，其含有作为第一组分的由式（Ia）或（Ib）表示的至少一种化合物，并且含有作为第二组分的至少一种式（II -a）至（II-g），每个式在本说明书中叙述。根据本发明，可以提供在AM-LCD液晶组合物中满足几种特性的情况下，可以提供在低温下相容性特别优异且具有适当大的ΔTAn和小Vth的液晶组合物。

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