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1. 发明授权

US5091223A Process for forming a blackened layer on a zinciferous surface by contacting the surface with an aqueous solution containing nickel and cobalt ions 失效
标题翻译：通过用含镍和钴离子的水溶液接触表面，在锌表面形成黑色层的方法
公开(公告)号：US5091223A
公开(公告)日：1992-02-25
申请号：US544455
申请日：1990-06-27
申请人： Kazuhiko Mori , Toshi Miyawaki , Hitoshi Ishii
发明人： Kazuhiko Mori , Toshi Miyawaki , Hitoshi Ishii
IPC分类号： C23C22/53 , C23C22/60 , C23C22/68
CPC分类号： C23C22/60 , C23C22/53 , C23C22/68
摘要： Zinciferous surfaces, particularly those of galvanized steel, may be effectively coated with an adherent corrosion resistant black layer of fine metal particles by contacting the surfaces with an aqueous solution containing (A) at least 0.5 g/L of the treatment solution of Ni.sup.2+ and/or Co.sup.2+ ions; and (B) an amount, sufficient to complex all the ions of component (A), of a weak complexing component selected from the group consisting of ammonia, saturated aliphatic compounds having at least two amino groups of which at least one is a primary amino group, and/or amino acids; and, optionally but preferably, (C) at least 50 parts per million ("ppm") by weight of a component selected from the group consisting of nitrite ions, nitrate ions, carbonate ions, thiocyanate ions, thiosulfate ions, thiourea, hypophosphite ions, phosphite ions, and/or perchlorate ions.

2. 发明授权

US4985087A Treating zinciferous metal surfaces to blacken them 失效
标题翻译：处理含锌金属表面使其变黑
公开(公告)号：US4985087A
公开(公告)日：1991-01-15
申请号：US389071
申请日：1989-08-03
申请人： Kazuhiko Mori , Hitoshi Ishii , Toshi Miyawaki
发明人： Kazuhiko Mori , Hitoshi Ishii , Toshi Miyawaki
IPC分类号： C23C22/60 , C23C18/32 , C23C22/78
CPC分类号： C23C18/32 , C23C22/78
摘要： Zinc and zinc alloy surfaces can be given an effective corrosion inhibiting treatment by contact for less than a minute with an alkaline aqueous solution having a pH not more than 11 and containing at least 0.020 g/L of dissolved nickel ions and sufficient ammonia to give a molar ratio of ammonia to nickel ion of at least 6. If the concentration of nickel ions in the treating solution is at least 1.0 g/L, a durable blackening of the surface is also produced. Both the corrosion resistance and the quality of the blackening can usually be further improved by subsequent conventional phosphate conversion coating.
摘要翻译：锌和锌合金表面可以通过与pH不超过11的碱性水溶液接触不到一分钟并且含有至少0.020g / L的溶解的镍离子和足量的氨来给予有效的腐蚀抑制处理氨与镍离子的摩尔比至少为6.如果处理溶液中镍离子的浓度至少为1.0g / L，则还会产生耐久的表面黑化。通常可以通过后续的常规磷酸盐转化涂层来进一步改善耐腐蚀性和黑化质量。

3. 发明授权

US5318640A Surface treatment method and composition for zinc coated steel sheet 失效
标题翻译：镀锌钢板的表面处理方法和组成
公开(公告)号：US5318640A
公开(公告)日：1994-06-07
申请号：US916096
申请日：1992-07-28
申请人： Hitoshii Ishii , Kazuhiko Mori , Toshi Miyawaki , Shizuo Shima
发明人： Hitoshii Ishii , Kazuhiko Mori , Toshi Miyawaki , Shizuo Shima
IPC分类号： C23C22/60 , C23C22/78 , C23C18/46
CPC分类号： C23C22/60 , C23C22/78
摘要： A nickel and/or cobalt deposition process which can be run at a nearly neutral pH and which rapidly deposits nickel and/or cobalt in quantities large enough to improve the paint adhesion and post coating corrosion resistance, and which has a good solution stability, is achieved by treating zinc coated sheet steel with an aqueous solution that has a pH between 5 and 10 inclusive and comprises (A) a total of at least 0.01 g/L of metal ions selected from the group consisting of Ni.sup.2+ and Co.sup.2+ ions and (B) a sufficient amount to fully complex the metal ions recited in part (A) of complexing agents selected from the group consisting of ammonia and organic compounds having at least one amino group in the neutral region.The substitution precipitation reaction of nickel and cobalt is substantially accelerated by the presence, as a third component in addition to the metal ion and complexing agent, of at least one ionic species or compound selected from the nitrite ion, nitrate ion, thiocyanate ion, thiosulfate ion, thiourea, phosphite ion, hypophosphite ion, and perchlorate ion.
摘要翻译： PCT No.PCT / US91 / 00531 Sec。 371日期：1992年7月28日 102（e）日期1992年7月28日PCT 1991年1月25日PCT PCT。出版物WO91 / 11542 日期：1991年8月8日。镍和/或钴沉积方法，其可以在接近中性的pH下运行，并且以足够大的量快速沉积镍和/或钴以改善涂料粘附性和后涂层耐腐蚀性，以及哪些具有良好的溶液稳定性，通过用pH为5〜10的水溶液处理镀锌钢板而实现，其包含（A）总计至少0.01g / L的金属离子，所述金属离子选自 Ni2 +和Co2 +离子和（B）足够的量使得在中性区域中具有至少一个氨基的氨和有机化合物中选择的一组络合剂部分（A）中所述的金属离子完全复合。作为除了金属离子和络合剂之外的至少一种离子种类或选自亚硝酸根离子，硝酸根离子，硫氰酸根离子，硫代硫酸盐的化合物的第三成分，镍和钴的取代沉淀反应基本上加快离子，硫脲，亚磷酸根离子，次磷酸根离子和高氯酸根离子。

4. 发明授权

US4904544A Zn-based composite-plated metallic material and plating method 失效
标题翻译：锌基复合镀金属材料及电镀方法
公开(公告)号：US4904544A
公开(公告)日：1990-02-27
申请号：US226483
申请日：1988-08-01
申请人： Kazuhiko Mori , Toshi Miyawaki
发明人： Kazuhiko Mori , Toshi Miyawaki
IPC分类号： C25D15/02 , C25D3/56 , C25D5/26 , C25D15/00
CPC分类号： C25D15/00 , C25D3/565 , Y10T428/12792 , Y10T428/12799
摘要： Disclosed is a Zn-based composite-plated metallic material, comprising a plating layer on a metal substrate. The plating layer consists essentially of (1) Zn or as Zn alloy electroplated onto a metallic substrate and (2) the cathodic precipitation reaction product of aluminum, calcium, magnesium, strontium, titanium, zirconium, molybdenum, and/or tungsten. The latter metal constitutes 0.002 to 10% by weight of the plating layer. The cathodic precipitation-reaction product may be hydroxide, hydroxide hydrate or a phosphate.

5. 发明授权

US4517030A Process for activating steel surface prior to phosphating treatment aqueous activating solution therefor 失效
标题翻译：在磷化处理之前激活钢表面的方法水活化溶液
公开(公告)号：US4517030A
公开(公告)日：1985-05-14
申请号：US637755
申请日：1984-08-06
申请人： Tsukasa Yamamoto , Asao Mochizuki , Hiroshi Okita , Toshi Miyawaki , Yoshiji Shirogane , Kazuhiko Mori
发明人： Tsukasa Yamamoto , Asao Mochizuki , Hiroshi Okita , Toshi Miyawaki , Yoshiji Shirogane , Kazuhiko Mori
IPC分类号： C23C22/80 , C23F7/10
CPC分类号： C23C22/80
摘要： This invention discloses a process for activating steel surface prior to phosphating treatment wherein the steel surface is cleaned, the cleaned steel surface is then treated with an aqueous activating solution containing titanium and pyrophosphate ion, and thereafter the steel surface is treated with a phosphating solution, characterized in that magnesium ion is included in said aqueous activating solution in order to suppress formation of an inactive film on said steel surface due to the presence of said pyrophosphate ion, and then said steel surface is treated with the resulting aqueous activating solution.
摘要翻译：本发明公开了一种在磷化处理之前激活钢表面的方法，其中钢表面被清洁，然后用含有钛和焦磷酸根离子的水性活化溶液处理被清洁的钢表面，然后用磷酸盐溶液处理钢表面，其特征在于，在所述活性水溶液中含有镁离子，以便由于存在所述焦磷酸根离子而在所述钢表面上抑制非活性膜的形成，然后用所得水性活化溶液处理所述钢表面。

6. 发明授权

US5254238A Surface treating solution and surface treating process for zinc-plated steel plates 失效
标题翻译：表面处理溶液和镀锌钢板表面处理工艺
公开(公告)号：US5254238A
公开(公告)日：1993-10-19
申请号：US645816
申请日：1991-01-25
申请人： Hitoshi Ishii , Toshi Miyawaki
发明人： Hitoshi Ishii , Toshi Miyawaki
IPC分类号： C25D9/08 , C23C22/53 , C25D5/48
CPC分类号： C25D5/48
摘要： A treating solution for forming a hydroxide film on each surface of zinc-plated steel plates by cathodic electrolysis is here disclosed which comprises (a) 0.2 to 50 g/l of one or more metal ions selected from the group consisting of Mg.sup.2+, Cr.sup.3+, Ca.sup.2+, Ni.sup.2+, Co.sup.2+ and Al.sup.3+, and (b) 0.1 to 50 g/l of one or more oxidizing agents selected from the group consisting of nitrate ions, nitrite ions, chlorate ions, bromate ions and hydrogen peroxide. A process for the surface treatment of the zinc-plated steel plates by the use of this treating solution is also disclosed.
摘要翻译：这里公开了通过阴极电解在镀锌钢板的每个表面上形成氢氧化物膜的处理溶液，其包含（a）0.2至50g / l的一种或多种选自Mg 2+，Cr 3+， Ca2 +，Ni2 +，Co2 +和Al3 +，以及（b）0.1-50g / l的一种或多种选自硝酸根离子，亚硝酸根离子，氯酸根离子，溴酸根离子和过氧化氢的氧化剂。还公开了通过使用该处理溶液对镀锌钢板进行表面处理的方法。

7. 发明授权

US5000799A Zinc-nickel phosphate conversion coating composition and process 失效
标题翻译：锌 - 镍磷酸盐转化涂层组成及工艺
公开(公告)号：US5000799A
公开(公告)日：1991-03-19
申请号：US412063
申请日：1989-09-25
申请人： Toshi Miyawaki
发明人： Toshi Miyawaki
IPC分类号： C23C22/12 , C23C22/17 , C23C22/18 , C23C22/36
CPC分类号： C23C22/365 , C23C22/17 , C23C22/184
摘要： The operation of zinc-nickel phosphate conversion coating of active metals is improved by using phosphating solutions containing formic acid or formate ions. Such solutions can work effectively at low temperatures and provide excellent substrates for paint, particularly that applied by electrodeposition.
摘要翻译：通过使用含有甲酸或甲酸根离子的磷酸盐溶液改善了活性金属的磷酸锌镍转化膜的操作。这样的溶液可以在低温下有效地工作，并提供优异的油漆基材，特别是通过电沉积涂覆的基材。

8. 发明授权

US4728401A Electrolytic post-treatment of phosphated surface 失效
标题翻译：电解后处理磷化表面
公开(公告)号：US4728401A
公开(公告)日：1988-03-01
申请号：US40432
申请日：1987-04-20
申请人： Toshi Miyawaki , Atsunori Yoshida , Yoshikazu Saito
发明人： Toshi Miyawaki , Atsunori Yoshida , Yoshikazu Saito
IPC分类号： B05D3/10 , B05D7/14 , C23C22/24 , C23C22/83 , C25D11/38 , C25D11/00
CPC分类号： C23C22/83 , C25D11/38
摘要： An improved process for preparing a phosphated metal surface for painting comprises electrolyzing the surface as cathode in an aqueous solution containing hexavalent and trivalent chromium in specified concentrations and weight ratios.
摘要翻译：一种用于制备磷酸化金属表面的改进方法包括在含有六价铬和三价铬的水溶液中以特定浓度和重量比将该表面电解为阴极。

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