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1. 发明授权

US08007942B2 Ion-dissociative functional compound, method for production thereof, ionic conductor, and electrochemical device 失效
标题翻译：离子解离功能化合物，其制备方法，离子导体和电化学装置
公开(公告)号：US08007942B2
公开(公告)日：2011-08-30
申请号：US10567283
申请日：2004-08-04
申请人： Kazuaki Fukushima , Shuichi Takizawa , Koichiro Hinokuma , Atsushi Nishimoto , Kazuhiro Noda
发明人： Kazuaki Fukushima , Shuichi Takizawa , Koichiro Hinokuma , Atsushi Nishimoto , Kazuhiro Noda
IPC分类号： H01M6/18 , H01M8/10 , C07C313/00
CPC分类号： C07C309/24 , C07C311/48 , C07C2604/00 , C08J5/22 , C08J2327/12 , H01B1/122 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1039 , H01M2300/0082 , Y02P70/56 , Y10S977/735
摘要： Disclosed herein are an ion-dissociative functional compound, a method for production thereof, an ionic conductor, and an electrochemical device, the ion-dissociative functional compound being thermally and chemically stable under the condition required of fuel cells and being suitable for use as a material such as protonic conductor in fuel cells.The proton-dissociative functional compound shown in FIG. 1A is composed of a fullerene C60 molecule and about 10 sulfonic acid groups —SO3H as proton-dissociative groups each attached to the fullerene through a difluoromethane group —CF2—. The proton-dissociative functional compound shown in FIG. 1B is composed of fullerene molecules three-dimensionally connected to each other through a linking group —CF2SO2NHSO2CF2—. It contains, as the proton-dissociative group, sulfoneimide groups —SO2NHSO2— and sulfoneamide groups —SO2H2 in addition to sulfonic acid groups. These compounds are prepared by introduction of difluoro(fluorosulfonyl)methyl groups into fullerene molecules, and ensuing imidization and hydrolysis.
摘要翻译：本文公开了离子解离官能化合物，其制备方法，离子导体和电化学装置，离子解离官能化合物在燃料电池所需的条件下是热和化学稳定的并且适合用作材料如燃料电池中的质子导体。图1所示的质子解离官能团化合物 1A由富勒烯C60分子和约10个磺酸基-SO 3 H组成，作为通过二氟甲烷基-CF2-连接到富勒烯的质子解离基团。图1所示的质子解离官能团化合物 1B由通过连接基团-CF 2 SO 2 NHSO 2 CF 2彼此三维连接的富勒烯分子组成。作为质子解离基团，除了磺酸基之外，还包含砜酰亚胺基团-SO 2 NH 2 2-和磺酰胺基团-SO 2 H 2。这些化合物是通过将二氟（氟磺酰基）甲基引入富勒烯分子中制备的，随后进行酰亚胺化和水解。

2. 发明申请

US20090004525A1 Ion-Dissociative Functional Compound, Method for Production Thereof, Ionic Conductor, and Electrochemical Device 失效
标题翻译：离子解离功能化合物，其生产方法，离子导体和电化学装置
公开(公告)号：US20090004525A1
公开(公告)日：2009-01-01
申请号：US10567283
申请日：2004-08-04
申请人： Kazuaki Fukushima , Shuichi Takizawa , Koichiro Hinokuma , Atsushi Nishimoto , Kazuhiro Noda
发明人： Kazuaki Fukushima , Shuichi Takizawa , Koichiro Hinokuma , Atsushi Nishimoto , Kazuhiro Noda
IPC分类号： H01M8/10 , C07C309/23 , C07C311/10
CPC分类号： C07C309/24 , C07C311/48 , C07C2604/00 , C08J5/22 , C08J2327/12 , H01B1/122 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1039 , H01M2300/0082 , Y02P70/56 , Y10S977/735
摘要： Disclosed herein are an ion-dissociative functional compound, a method for production thereof, an ionic conductor, and an electrochemical device, the ion-dissociative functional compound being thermally and chemically stable under the condition required of fuel cells and being suitable for use as a material such as protonic conductor in fuel cells.The proton-dissociative functional compound shown in FIG. 1A is composed of a fullerene C60 molecule and about 10 sulfonic acid groups —SO3H as proton-dissociative groups each attached to the fullerene through a difluoromethane group —CF2—. The proton-dissociative functional compound shown in FIG. 1B is composed of fullerene molecules three-dimensionally connected to each other through a linking group —CF2SO2NHSO2CF2—. It contains, as the proton-dissociative group, sulfoneimide groups —SO2NHSO2— and sulfoneamide groups —SO2H2 in addition to sulfonic acid groups. These compounds are prepared by introduction of difluoro(fluorosulfonyl)methyl groups into fullerene molecules, and ensuing imidization and hydrolysis.
摘要翻译：本文公开了离子解离官能化合物，其制备方法，离子导体和电化学装置，离子解离官能化合物在燃料电池所需的条件下是热和化学稳定的并且适合用作材料如燃料电池中的质子导体。图1所示的质子解离官能团化合物 1A由富勒烯C60分子和约10个磺酸基-SO 3 H组成，作为通过二氟甲烷基-CF2-连接到富勒烯的质子解离基团。图1所示的质子解离官能团化合物 1B由通过连接基团-CF 2 SO 2 NHSO 2 CF 2彼此三维连接的富勒烯分子组成。作为质子解离基团，除了磺酸基之外，还包含砜酰亚胺基团-SO 2 NH 2 2-和磺酰胺基团-SO 2 H 2。这些化合物是通过将二氟（氟磺酰基）甲基引入富勒烯分子中制备的，随后进行酰亚胺化和水解。

3. 发明申请

US20070092800A1 IONIC CONDUCTOR, PROCESS FOR PRODUCTION THEREOF, AND ELECTROCHEMICAL DEVICE 失效
标题翻译：离子导体，其制造方法和电化学装置
公开(公告)号：US20070092800A1
公开(公告)日：2007-04-26
申请号：US11561609
申请日：2006-11-20
申请人： Koichiro Hinokuma , Bjoern Pietzak , Constance Rost , Masafumi Ata , Yongming Li , Kazuaki Fukushima
发明人： Koichiro Hinokuma , Bjoern Pietzak , Constance Rost , Masafumi Ata , Yongming Li , Kazuaki Fukushima
IPC分类号： H01M10/40 , C08J5/20
CPC分类号： B82Y30/00 , H01B1/122 , H01M4/8605 , H01M6/18 , H01M8/1004 , H01M8/1023 , H01M8/1039 , H01M8/1048 , H01M10/0562 , H01M10/347 , H01M12/00 , H01M2300/0068 , H01M2300/0082 , Y02P70/56
摘要： Disclosed herein are an ionic conductor including a proton conductor, a process for production thereof, and an electrochemical device (such as fuel cell) with said ionic conductor, said ionic conductor being superior in ionic conductivity, water resistance, and film forming properties. The ionic conductor is formed from a polymer in which carbon clusters having ion dissociating functional groups are bonded to each other through connecting groups. The polymer is less water-soluble and more chemically stable than a derivative composed solely of carbon clusters; therefore, it permits many ion dissociating functional group to be introduced thereinto. Moreover, if ion dissociating functional groups are introduced into also the connecting group, it is possible to prevent the concentration of ion dissociating functional groups from decreasing as the result of polymerization. The polymer can be easily synthesized by simple condensation, substitution, and hydrolysis. Therefore, the process is suitable for mass production in high yields.
摘要翻译：本文公开了包括质子导体，其制造方法和具有所述离子导体的电化学装置（例如燃料电池）的离子导体，所述离子导体的离子导电性，耐水性和成膜性优异。离子导体由具有离子解离官能团的碳簇通过连接基团彼此结合的聚合物形成。聚合物比仅由碳簇组成的衍生物更少的水溶性和化学稳定性; 因此，允许引入许多离子解离官能团。此外，如果将离子解离官能团引入连接基团，则可以防止离子解离官能团的浓度作为聚合的结果而降低。聚合物可以通过简单的缩合，取代和水解来容易地合成。因此，该方法适合大批量生产。

4. 发明授权

US07771891B2 Ionic conductor, process for production thereof, and electrochemical device 有权
标题翻译：离子导体，其制造方法和电化学装置
公开(公告)号：US07771891B2
公开(公告)日：2010-08-10
申请号：US12340021
申请日：2008-12-19
申请人： Koichiro Hinokuma , Bjoern Pietzak , Constance Gertrud Rost , Masafumi Ata , Yongming Li , Kazuaki Fukushima
发明人： Koichiro Hinokuma , Bjoern Pietzak , Constance Gertrud Rost , Masafumi Ata , Yongming Li , Kazuaki Fukushima
IPC分类号： H01M10/40 , H01M8/10 , H01M4/58 , C08J5/20
CPC分类号： B82Y30/00 , H01B1/122 , H01M4/8605 , H01M6/18 , H01M8/1004 , H01M8/1023 , H01M8/1039 , H01M8/1048 , H01M10/0562 , H01M10/347 , H01M12/00 , H01M2300/0068 , H01M2300/0082 , Y02P70/56
摘要： Disclosed herein are an ionic conductor including a proton conductor, a process for production thereof, and an electrochemical device (such as fuel cell) with said ionic conductor, said ionic conductor being superior in ionic conductivity, water resistance, and film forming properties. The ionic conductor is formed from a polymer in which carbon clusters having ion dissociating functional groups are bonded to each other through connecting groups. The polymer is less water-soluble and more chemically stable than a derivative composed solely of carbon clusters; therefore, it permits many ion dissociating functional group to be introduced thereinto. Moreover, if ion dissociating functional groups are introduced into also the connecting group, it is possible to prevent the concentration of ion dissociating functional groups from decreasing as the result of polymerization. The polymer can be easily synthesized by simple condensation, substitution, and hydrolysis. Therefore, the process is suitable for mass production in high yields.
摘要翻译：本文公开了包括质子导体，其制造方法和具有所述离子导体的电化学装置（例如燃料电池）的离子导体，所述离子导体的离子导电性，耐水性和成膜性优异。离子导体由具有离子解离官能团的碳簇通过连接基团彼此结合的聚合物形成。聚合物比仅由碳簇组成的衍生物更少的水溶性和化学稳定性; 因此，允许引入许多离子解离官能团。此外，如果将离子解离官能团引入连接基团，则可以防止离子解离官能团的浓度因聚合而降低。聚合物可以通过简单的缩合，取代和水解来容易地合成。因此，该方法适合大批量生产。

5. 发明授权

US07153608B2 Ionic conductor, process for production thereof, and electrochemical device 有权
公开(公告)号：US07153608B2
公开(公告)日：2006-12-26
申请号：US10280941
申请日：2002-10-25
申请人： Koichiro Hinokuma , Bjoern Pietzak , Constance Gertrud Rost , Masafumi Ata , Yongming Li , Kazuaki Fukushima
发明人： Koichiro Hinokuma , Bjoern Pietzak , Constance Gertrud Rost , Masafumi Ata , Yongming Li , Kazuaki Fukushima
IPC分类号： H01M4/58 , H01M8/10 , H01M10/40 , C08J5/20
CPC分类号： B82Y30/00 , H01B1/122 , H01M4/8605 , H01M6/18 , H01M8/1004 , H01M8/1023 , H01M8/1039 , H01M8/1048 , H01M10/0562 , H01M10/347 , H01M12/00 , H01M2300/0068 , H01M2300/0082 , Y02P70/56
摘要： An ionic conductor, such as a proton conductor, a process for production thereof, and an electrochemical device, such as fuel cell, that includes the ionic conductor is provided. The ionic conductor of the present invention is formed from a polymer in which carbon clusters having ion dissociating functional groups are bonded to each other through connecting groups which can also include one or more ion dissociating functional groups. In this regard, the polymer is less water-soluble and more chemically stable than a derivative composed solely of carbon clusters, thus displaying enhanced ionic conduction properties.

6. 发明申请

US20090105357A1 IONIC CONDUCTOR, PROCESS FOR PRODUCTION THEREOF, AND ELECTROCHEMICAL DEVICE 有权
标题翻译：离子导体，其制造方法和电化学装置
公开(公告)号：US20090105357A1
公开(公告)日：2009-04-23
申请号：US12340021
申请日：2008-12-19
申请人： Koichiro Hinokuma , Bjoern Pietzak , Constance Gertrud Rost , Masafumi Ata , Yongming Li , Kazuaki Fukushima
发明人： Koichiro Hinokuma , Bjoern Pietzak , Constance Gertrud Rost , Masafumi Ata , Yongming Li , Kazuaki Fukushima
IPC分类号： C08J5/20
CPC分类号： B82Y30/00 , H01B1/122 , H01M4/8605 , H01M6/18 , H01M8/1004 , H01M8/1023 , H01M8/1039 , H01M8/1048 , H01M10/0562 , H01M10/347 , H01M12/00 , H01M2300/0068 , H01M2300/0082 , Y02P70/56
摘要： Disclosed herein are an ionic conductor including a proton conductor, a process for production thereof, and an electrochemical device (such as fuel cell) with said ionic conductor, said ionic conductor being superior in ionic conductivity, water resistance, and film forming properties. The ionic conductor is formed from a polymer in which carbon clusters having ion dissociating functional groups are bonded to each other through connecting groups. The polymer is less water-soluble and more chemically stable than a derivative composed solely of carbon clusters; therefore, it permits many ion dissociating functional group to be introduced thereinto. Moreover, if ion dissociating functional groups are introduced into also the connecting group, it is possible to prevent the concentration of ion dissociating functional groups from decreasing as the result of polymerization. The polymer can be easily synthesized by simple condensation, substitution, and hydrolysis. Therefore, the process is suitable for mass production in high yields.
摘要翻译：本文公开了包括质子导体，其制造方法和具有所述离子导体的电化学装置（例如燃料电池）的离子导体，所述离子导体的离子导电性，耐水性和成膜性优异。离子导体由具有离子解离官能团的碳簇通过连接基团彼此结合的聚合物形成。聚合物比仅由碳簇组成的衍生物更少的水溶性和化学稳定性; 因此，允许引入许多离子解离官能团。此外，如果将离子解离官能团引入连接基团，则可以防止离子解离官能团的浓度因聚合而降低。聚合物可以通过简单的缩合，取代和水解来容易地合成。因此，该方法适合大批量生产。

7. 发明授权

US07651803B2 Ionic conductor, process for production thereof, and electrochemical device 失效
公开(公告)号：US07651803B2
公开(公告)日：2010-01-26
申请号：US11561609
申请日：2006-11-20
申请人： Koichiro Hinokuma , Bjoern Pietzak , Constance Gertrud Rost , Masafumi Ata , Yongming Li , Kazuaki Fukushima
发明人： Koichiro Hinokuma , Bjoern Pietzak , Constance Gertrud Rost , Masafumi Ata , Yongming Li , Kazuaki Fukushima
IPC分类号： H01M4/58 , H01M8/10 , H01M10/40 , C08J5/20
CPC分类号： B82Y30/00 , H01B1/122 , H01M4/8605 , H01M6/18 , H01M8/1004 , H01M8/1023 , H01M8/1039 , H01M8/1048 , H01M10/0562 , H01M10/347 , H01M12/00 , H01M2300/0068 , H01M2300/0082 , Y02P70/56
摘要： Disclosed herein are an ionic conductor including a proton conductor, a process for production thereof, and an electrochemical device (such as fuel cell) with said ionic conductor, said ionic conductor being superior in ionic conductivity, water resistance, and film forming properties. The ionic conductor is formed from a polymer in which carbon clusters having ion dissociating functional groups are bonded to each other through connecting groups. The polymer is less water-soluble and more chemically stable than a derivative composed solely of carbon clusters; therefore, it permits many ion dissociating functional group to be introduced thereinto. Moreover, if ion dissociating functional groups are introduced into also the connecting group, it is possible to prevent the concentration of ion dissociating functional groups from decreasing as the result of polymerization. The polymer can be easily synthesized by simple condensation, substitution, and hydrolysis. Therefore, the process is suitable for mass production in high yields.

8. 发明授权

US07524916B2 Hybrid silica polymer, method for production thereof, and proton-conducting material 失效
标题翻译：杂化二氧化硅聚合物，其制造方法和质子传导材料
公开(公告)号：US07524916B2
公开(公告)日：2009-04-28
申请号：US11568368
申请日：2005-04-08
申请人： Nawal Kishor Mal , Koichiro Hinokuma , Kazuhiro Noda
发明人： Nawal Kishor Mal , Koichiro Hinokuma , Kazuhiro Noda
IPC分类号： C08G77/22 , C08G75/00 , C08G75/04 , H01B1/00
CPC分类号： C08G77/28 , C08L83/08 , H01B1/122 , H01M8/04291 , H01M8/1027 , H01M8/1037 , H01M8/1072 , H01M2300/0082 , H01M2300/0091 , Y02P70/56
摘要： Hybrid silica polymer applicable to electrochemical elements and a method for economical production thereof, the former excelling in thermal stability, mechanical stability, solvent resistance, and proton conductivity at low humidity is provided. The method includes a step of heating a mixture of 3-mercaptopropyltrialkoxylsilane, surfactant, water, and base or acid for their reaction with one another at 25 to 180° C., thereby providing a hybrid thiol group-containing silica polymer, and an optional step of oxidizing said hybrid thiol group-containing silica polymer with a peroxide, thereby giving a hybrid silica polymer which is composed of hybrid (thiol group-containing and/or sulfonic group-containing) silica polymer. The resulting silica polymer is used as a proton conducting material for electrochemical elements such as fuel cells, capacitors, and electrolytic cells.
摘要翻译：提供了适用于电化学元件的混合二氧化硅聚合物及其经济生产方法，前者在低湿度下具有优异的热稳定性，机械稳定性，耐溶剂性和质子传导性。该方法包括在25〜180℃下加热3-巯基丙基三烷氧基硅烷，表面活性剂，水和碱或酸的混合物进行反应的步骤，由此提供含杂硫基的二氧化硅聚合物和任选的用过氧化物氧化所述含杂硫基的二氧化硅聚合物的步骤，从而得到由杂化（含硫醇基和/或磺酸基）二氧化硅聚合物组成的混合二氧化硅聚合物。所得二氧化硅聚合物用作电化学元件如燃料电池，电容器和电解槽的质子传导材料。

9. 发明授权

US5764401A Optical apparatus 失效
标题翻译：光学仪器
公开(公告)号：US5764401A
公开(公告)日：1998-06-09
申请号：US555813
申请日：1995-11-09
申请人： Tohru Udaka , Hideharu Miyagaki , Kazuhiro Noda , Koichiro Hinokuma
发明人： Tohru Udaka , Hideharu Miyagaki , Kazuhiro Noda , Koichiro Hinokuma
IPC分类号： G02F1/15 , G02F1/153
CPC分类号： G02F1/1506
摘要： An optical apparatus includes a first electrode that can be kept in a transparent state in a visible light region, and a second electrode electrically separated from the first electrode. A space is provided between the first and second electrodes. A certain function is used to provide a driving potential to the first and second electrodes. An electrolyte is poured into the space between the electrodes. The electrolyte is composed of a solution prepared by dissolving a silver salt in at least one type of solvent selected from a group consisting of dimethylformamide, diethylformamide, N, N-dimethylacetamide, N-methylpropionamide, N-methylpyrrolidone, 2-ethoxyethanol, and 2-methoxyethanol. By use of this electrolyte, silver is precipitated and dissolved under driving control over the first and second electrodes. As a result, color-developing and color-fading are effected by precipitation and dissolution of silver, respectively.
摘要翻译：光学装置包括可以在可见光区域保持透明状态的第一电极和与第一电极电隔离的第二电极。在第一和第二电极之间设置空间。使用某种功能来为第一和第二电极提供驱动电位。将电解质注入电极之间的空间。电解质由将银盐溶解在选自二甲基甲酰胺，二乙基甲酰胺，N，N-二甲基乙酰胺，N-甲基丙酰胺，N-甲基吡咯烷酮，2-乙氧基乙醇，和2-乙氧基乙醇的至少一种溶剂中而成的溶液 - 甲氧基乙醇。通过使用该电解质，银在第一和第二电极的驱动控制下沉淀并溶解。结果，显色和褪色分别通过银的沉淀和溶解来实现。

10. 发明申请

US20070213494A1 HYBRID SILICA POLYMER, METHOD FOR PRODUCTION THEREROF, AND PROTON-CONDUCTING MATERIAL 失效
标题翻译：混合二氧化硅聚合物，其生产方法和导体材料
公开(公告)号：US20070213494A1
公开(公告)日：2007-09-13
申请号：US11568368
申请日：2005-04-08
申请人： Nawal Mal , Koichiro Hinokuma , Kazuhiro Noda
发明人： Nawal Mal , Koichiro Hinokuma , Kazuhiro Noda
IPC分类号： C08G77/28 , H01B1/06 , H01M8/02 , H01M8/10
CPC分类号： C08G77/28 , C08L83/08 , H01B1/122 , H01M8/04291 , H01M8/1027 , H01M8/1037 , H01M8/1072 , H01M2300/0082 , H01M2300/0091 , Y02P70/56
摘要： Disclosed herein are a hybrid silica polymer applicable to electrochemical elements and a method for economical production thereof, the former excelling in thermal stability, mechanical stability, solvent resistance, and proton conductivity at low humidity. Said method includes a step of heating a mixture of 3-mercaptopropyltrialkoxylsilane, surfactant, water, and base or acid for their reaction with one another at 25 to 180° C., thereby giving a hybrid thiol group-containing silica polymer, and an optional step of oxidizing said hybrid thiol group-containing silica polymer with a peroxide, thereby giving a hybrid silica polymer which is composed of hybrid (thiol group-containing and/or sulfonic group-containing) silica polymer. The resulting silica polymer is used as a proton conducting material for electrochemical elements such as fuel cells, capacitors, and electrolytic cells.
摘要翻译：本文公开了适用于电化学元件的混合二氧化硅聚合物及其经济生产方法，前者在低湿度下具有优异的热稳定性，机械稳定性，耐溶剂性和质子传导性。所述方法包括在25至180℃下加热3-巯基丙基三烷氧基硅烷，表面活性剂，水和碱或酸的混合物彼此反应的步骤，从而得到含杂硫族基团的二氧化硅聚合物和任选的用过氧化物氧化所述含杂硫基的二氧化硅聚合物的步骤，从而得到由杂化（含硫醇基和/或磺酸基）二氧化硅聚合物组成的混合二氧化硅聚合物。所得二氧化硅聚合物用作电化学元件如燃料电池，电容器和电解槽的质子传导材料。

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