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1. 发明申请

US20090239738A1 Titanium Oxide Photocatalyst, Process For Producing The Same And Application 审中-公开
标题翻译：氧化钛光催化剂，生产方法及应用
公开(公告)号：US20090239738A1
公开(公告)日：2009-09-24
申请号：US12371196
申请日：2009-02-13
申请人： Katsumi Okada , Katsuhiro Nishihara , Yasuhiro Masaki , Haruhiko Kajimura , Michiyasu Takahashi , Tadashi Yao , Tadashi Ogasawara , Munetoshi Watanabe , Shiji Shimosaki , Kouji Oda , Sadanobu Nagaoka
发明人： Katsumi Okada , Katsuhiro Nishihara , Yasuhiro Masaki , Haruhiko Kajimura , Michiyasu Takahashi , Tadashi Yao , Tadashi Ogasawara , Munetoshi Watanabe , Shiji Shimosaki , Kouji Oda , Sadanobu Nagaoka
IPC分类号： B01J27/135
CPC分类号： B01J35/004 , B01D53/8609 , B01D53/8612 , B01D53/8628 , B01D53/8634 , B01D53/8662 , B01D2255/802 , B01J21/063 , B01J23/18 , B01J27/132 , B01J27/135 , B01J35/002 , B01J37/0238 , B01J37/22
摘要： Titanium oxide-based photocatalysts which contain a metal halide in titanium oxide and which are prepared from titanium oxide and/or its precursor, which may optionally be heat treated, by contact with a reactive gas containing a metal halide of the formula MXn or MOXn (wherein M=a metal, X=a halogen, and n=an integer) with heating stably develop a high photocatalytic activity with visible light irradiation. The photocatalysts may subsequently be stabilized by contact with water or by heat treatment, and/or promoted by contact with a heteropoly acid and/or an isopoly acid so as to include a metal complex in the titanium oxide. Photocatalysts prepared in this manner exhibit novel ESR features. The present invention also provides methods for preparing these photocatalysts, a photocatalyst dispersion and a photocatalytic coating fluid containing such a photocatalyst, and photocatalytic functional products and methods for their manufacture using the photocatalyst.
摘要翻译：二氧化钛基光催化剂，其在二氧化钛中含有金属卤化物，并且可以通过与含有式MXn或MOXn的金属卤化物的反应性气体接触而由氧化钛和/或其前体制备，其可以任选地进行热处理（其中M =金属，X =卤素，n =整数），加热可稳定地产生可见光照射的高光催化活性。可以随后通过与水接触或通过热处理来稳定光催化剂，和/或通过与杂多酸和/或异多酸接触来促进光催化剂，以在氧化钛中包括金属络合物。以这种方式制备的光催化剂显示出新的ESR特征。本发明还提供了制备这些光催化剂的方法，光催化剂分散体和含有这种光催化剂的光催化涂布液，以及光催化功能产物及其使用该光催化剂的制造方法。

2. 发明授权

US07521133B2 Titanium oxide photocatalyst, process for producing the same and application 有权
标题翻译：氧化钛光催化剂，其制备方法及应用
公开(公告)号：US07521133B2
公开(公告)日：2009-04-21
申请号：US10508871
申请日：2003-03-20
申请人： Katsumi Okada , Katsuhiro Nishihara , Yasuhiro Masaki , Haruhiko Kajimura , Michiyasu Takahashi , Tadashi Yao , Tadashi Ogasawara , Munetoshi Watanabe , Shiji Shimosaki , Kouji Oda , Sadanobu Nagaoka
发明人： Katsumi Okada , Katsuhiro Nishihara , Yasuhiro Masaki , Haruhiko Kajimura , Michiyasu Takahashi , Tadashi Yao , Tadashi Ogasawara , Munetoshi Watanabe , Shiji Shimosaki , Kouji Oda , Sadanobu Nagaoka
IPC分类号： B32B9/00 , C09D1/00 , C04B35/00
CPC分类号： B01J35/004 , B01D53/8609 , B01D53/8612 , B01D53/8628 , B01D53/8634 , B01D53/8662 , B01D2255/802 , B01J21/063 , B01J23/18 , B01J27/132 , B01J27/135 , B01J35/002 , B01J37/0238 , B01J37/22
摘要： Titanium oxide-based photocatalysts which contain a metal halide in titanium oxide and which are prepared from titanium oxide and/or its precursor, which may optionally be heat treated, by contact with a reactive gas containing a metal halide of the formula MXn or MOXn (wherein M=a metal, X=a halogen, and n=an integer) with heating stably develop a high photocatalytic activity with visible light irradiation. The photocatalysts may subsequently be stabilized by contact with water or by heat treatment, and/or promoted by contact with a heteropoly acid and/or an isopoly acid so as to include a metal complex in the titanium oxide. Photocatalysts prepared in this manner exhibit novel ESR features. The present invention also provides methods for preparing these photocatalysts, a photocatalyst dispersion and a photocatalytic coating fluid containing such a photocatalyst, and photocatalytic functional products and methods for their manufacture using the photocatalyst.
摘要翻译：二氧化钛基光催化剂，其在氧化钛中含有金属卤化物，其可由可选择地经过热处理的氧化钛和/或其前体制备，所述氧化钛和/或其前体通过与含有式MXn或MOXn的金属卤化物的反应性气体接触其中M =金属，X =卤素，n =整数），加热可稳定地产生可见光照射的高光催化活性。可以随后通过与水接触或通过热处理来稳定光催化剂，和/或通过与杂多酸和/或异多酸接触来促进光催化剂，以在氧化钛中包括金属络合物。以这种方式制备的光催化剂显示出新的ESR特征。本发明还提供了制备这些光催化剂的方法，光催化剂分散体和含有这种光催化剂的光催化涂布液，以及光催化功能产物及其使用该光催化剂的制造方法。

3. 发明申请

US20050227008A1 Titanium oxide photocatalyst, process for producing the same and application 有权
标题翻译：氧化钛光催化剂，其制备方法及应用
公开(公告)号：US20050227008A1
公开(公告)日：2005-10-13
申请号：US10508871
申请日：2003-03-20
申请人： Katsumi Okada , Katsuhiro Nishihara , Yasuhiro Masaki , Haruhiko Kajimura , Michiyasu Takahashi , Tadashi Yao , Tadashi Ogasawara , Munetoshi Watanabe , Shiji Shimosaki , Kouji Oda , Sadanobu Nagaoka
发明人： Katsumi Okada , Katsuhiro Nishihara , Yasuhiro Masaki , Haruhiko Kajimura , Michiyasu Takahashi , Tadashi Yao , Tadashi Ogasawara , Munetoshi Watanabe , Shiji Shimosaki , Kouji Oda , Sadanobu Nagaoka
IPC分类号： B01D53/86 , B01J21/06 , B01J23/18 , B01J27/132 , B01J27/135 , B01J35/00 , B01J37/02 , B01J37/22 , B05D3/02
CPC分类号： B01J35/004 , B01D53/8609 , B01D53/8612 , B01D53/8628 , B01D53/8634 , B01D53/8662 , B01D2255/802 , B01J21/063 , B01J23/18 , B01J27/132 , B01J27/135 , B01J35/002 , B01J37/0238 , B01J37/22
摘要： Titanium oxide-based photocatalysts which contain a metal halide in titanium oxide and which are prepared from titanium oxide and/or its precursor, which may optionally be heat treated, by contact with a reactive gas containing a metal halide of the formula MXn or MOXn (wherein M=a metal, X=a halogen, and n=an integer) with heating stably develop a high photocatalytic activity with visible light irradiation. The photocatalysts may subsequently be stabilized by contact with water or by heat treatment, and/or promoted by contact with a heteropoly acid and/or an isopoly acid so as to include a metal complex in the titanium oxide. Photocatalysts prepared in this manner exhibit novel ESR features. The present invention also provides methods for preparing these photocatalysts, a photocatalyst dispersion and a photocatalytic coating fluid containing such a photocatalyst, and photocatalytic functional products and methods for their manufacture using the photocatalyst.
摘要翻译：二氧化钛基光催化剂，其在氧化钛中含有金属卤化物，并且其可由氧化钛和/或其前体制备，其可任选地被热处理，通过与含有式MX的金属卤化物的反应性气体接触，（其中M =金属，X =卤素，n =整数）与可见光照射一起稳定地产生高的光催化活性。可以随后通过与水接触或通过热处理来稳定光催化剂，和/或通过与杂多酸和/或异多酸接触来促进光催化剂，以在氧化钛中包括金属络合物。以这种方式制备的光催化剂显示出新的ESR特征。本发明还提供了制备这些光催化剂的方法，光催化剂分散体和含有这种光催化剂的光催化涂布液，以及光催化功能产物及其使用该光催化剂的制造方法。

4. 发明申请

US20090123769A1 VISIBLE LIGHT RESPONSE-TYPE TITANIUM OXIDE PHOTOCATALYST, METHOD FOR MANUFACTURING THE VISIBLE LIGHT RESPONSE-TYPE TITANIUM OXIDE PHOTOCATALYST, AND USE OF THE VISIBLE LIGHT RESPONSE-TYPE TITANIUM OXIDE PHOTOCATALYST 审中-公开
标题翻译：可见光反应型氧化钛光催化剂，用于制造可见光反应型氧化钛光催化剂的方法，以及可见光反应型氧化钛光催化剂的使用
公开(公告)号：US20090123769A1
公开(公告)日：2009-05-14
申请号：US12295101
申请日：2007-03-22
申请人： Yasuhiro Masaki , Katsuhiro Nishihara , Tadashi Fukuda , Katsumi Okada , Masahito Tasaka , Shinji Shimosaki , Hideaki Kanno , Sadanobu Nagaoka , Kazuomi Azuma , Tadashi Ogasawara
发明人： Yasuhiro Masaki , Katsuhiro Nishihara , Tadashi Fukuda , Katsumi Okada , Masahito Tasaka , Shinji Shimosaki , Hideaki Kanno , Sadanobu Nagaoka , Kazuomi Azuma , Tadashi Ogasawara
IPC分类号： B32B15/04 , B01J27/24
CPC分类号： C01G23/053 , B01D53/885 , B01D2255/20707 , B01D2255/802 , B01D2257/206 , B01D2257/30 , B01D2257/404 , B01D2257/406 , B01D2257/70 , B01D2257/91 , B01D2259/802 , B01J21/063 , B01J35/002 , B01J35/004 , B01J37/0209 , B01J37/0219 , B01J37/0225 , B01J37/0244 , B01J37/03 , B01J37/031 , B01J37/10 , C01P2002/54 , C01P2002/84 , C01P2002/85 , Y02P20/154 , Y10T428/31678
摘要： A titanium oxide photocatalyst responsive to visible light which can exhibit a high photocatalytic activity in response to visible light is produced by subjecting titanium oxide and/or titanium hydroxide obtained by neutralizing an acidic titanium compound with a nitrogen-containing base to heat treatment in an atmosphere containing a hydrolyzable metal compound (e.g., a titanium halide) and then to additional heat treatment in a gas having a moisture content of 0.5-4.0 volume % at a temperature of 350° C. or above. The photocatalyst which is a nitrogen-containing titanium oxide has no substantial peak at a temperature of 600° C. or above in a mass fragment spectrum obtained by thermal desorption spectroscopy in which the ratio m/e of the mass number m to the electric charged e of ions is 28, and the peak having the smallest half band width is in the range of 400-600° C. in the spectrum. The nitrogen content calculated from the peak appearing at 400 eV±1.0 eV in the N1s shell bonding energy spectrum obtained by XPS measurement of this photocatalyst is at least 20 times larger than the nitrogen content obtained by chemical analysis.
摘要翻译：通过将通过用含氮碱中和酸化钛化合物得到的氧化钛和/或氢氧化钛在大气中进行热处理来制造响应于可见光而具有高光催化活性的可见光的氧化钛光催化剂含有可水解金属化合物（例如，卤化钛），然后在350℃或更高的温度下在含水量为0.5-4.0体积％的气体中进行额外的热处理。作为含氮氧化钛的光催化剂在600℃以上的温度下，在通过热解吸光谱法获得的质量碎片光谱中没有显着的峰值，其中质量数m与电荷的比率m / e e的离子是28，并且具有最小半带宽的峰在光谱中在400-600℃的范围内。在通过该光催化剂的XPS测定得到的N1s壳结合能谱中，以400eV±1.0eV出现的峰计算出的氮含量比通过化学分析获得的氮含量大至少20倍。

5. 发明申请

US20070248831A1 Titanium Oxide Base Photocatalyst, Process for Producing the Same and Use Thereof 审中-公开
标题翻译：氧化钛基光催化剂，其生产方法及用途
公开(公告)号：US20070248831A1
公开(公告)日：2007-10-25
申请号：US11578874
申请日：2005-04-19
申请人： Katsuhiro Nishihara , Yasuhiro Masaki , Tadashi Fukuda , Katsumi Okada , Shinji Shimosaki , Sadanobu Nagaoka , Hideaki Kanno , Kazuomi Azuma , Tadashi Ogasawara
发明人： Katsuhiro Nishihara , Yasuhiro Masaki , Tadashi Fukuda , Katsumi Okada , Shinji Shimosaki , Sadanobu Nagaoka , Hideaki Kanno , Kazuomi Azuma , Tadashi Ogasawara
IPC分类号： B01J35/02 , B32B9/00
CPC分类号： C01G23/0536 , B01J21/063 , B01J35/002 , B01J35/004 , B01J37/031 , C01P2006/12 , Y10T428/31678
摘要： A highly active titanium oxide photocatalyst of the type responsive to visible light is prepared by subjecting a titanium (hydr)oxide raw material obtained by neutralizing an acidic titanium compound in ammonia or an amine under conditions such that the final pH is 7 or below to heat treatment in an atmosphere containing a hydrolyzable compound followed by contact with water and additional heat treatment at a temperature of at least 350° C. The resulting titanium oxide photocatalyst comprises titanium oxide with a specific surface area of at most 120 m2/g and with the amount of surface hydroxyl groups being at least 600 μeq/g. Preferably the density of surface hydroxyl groups is at least 8 μeq/m2, and the ratio of the amount of terminal type hydroxyl groups (T) to the amount of bridge type hydroxyl groups (B) in the surface hydroxyl groups satisfies T/B≧0.20. This titanium oxide photocatalyst has an ESR spectrum having two types of triplet signal for which the g values of the main spectra are 1.993-2.003 and 2.003-2.011, respectively, and it is also identified by having ratios of the strengths of these signals before irradiation with visible light, under irradiation, and immediately after the stop of irradiation which are different from conventional products.
摘要翻译：通过使在最终pH为7以下的条件下将氨基或胺中的酸性钛化合物得到的钛（氢化物）氧化物原料进行加热，制备对可见光敏感的高活性氧化钛光催化剂在含有可水解化合物的气氛中进行处理，然后与水接触，并在至少350℃的温度下进行额外的热处理。所得到的氧化钛光催化剂包括比表面积至多为120μm2的氧化钛， / SUP / g，表面羟基的量为至少600mueq / g。优选地，表面羟基的密度为至少8mueq / m 2，并且末端型羟基（T）的量与桥型羟基的量的比例（B）在表面羟基满足T / B> = 0.20。该氧化钛光催化剂具有ESR谱，其具有两种类型的三重态信号，其主要光谱的g值分别为1.993-2.003和2.003-2.011，并且还通过在照射前具有这些信号的强度比来鉴定具有可见光，照射下，以及在与常规产品不同的照射停止之后。

6. 发明申请

US20210371227A1 SHEET FEEDING DEVICE AND IMAGE FORMING APPARATUS INCORPORATING SAME 有权
公开(公告)号：US20210371227A1
公开(公告)日：2021-12-02
申请号：US17322756
申请日：2021-05-17
申请人： Katsumi Okada , Takuya Moriyama , Kenichiroh Yamahiro
发明人： Katsumi Okada , Takuya Moriyama , Kenichiroh Yamahiro
IPC分类号： B65H23/00 , B65H7/08
摘要： A sheet feeding device includes a support, a rotation driver, a guide, a support shaft, a biasing member, a leading end sensor, a roller, an outer diameter sensor, and circuitry. The circuitry causes the rotation driver to rotate a spool in a winding direction to determine a timing at which a signal change rate exceeds a change rate threshold as a passing time at which a leading end of a continuous sheet passes through the leading end sensor, causes the rotation driver to rotate the spool by a rotation angle in the winding direction, from the passing time, to position the leading end of the continuous sheet at a feeding start position, and rotates the spool in a feeding direction to feed the continuous sheet from the feeding start position along a guide portion. Further, the circuitry changes the change rate threshold based on an outer diameter of a roll.

7. 发明申请

US20070098424A1 Image forming device 有权
标题翻译：图像形成装置
公开(公告)号：US20070098424A1
公开(公告)日：2007-05-03
申请号：US11259144
申请日：2005-10-27
申请人： Katsumi Okada
发明人： Katsumi Okada
IPC分类号： G03G15/02
CPC分类号： G03G15/0283
摘要： The size of a resonance noise due to a signal of an alternating voltage applied to a charging member (charging roller) is detected by a piezoelectric device (PZ), and in cases in which the size of the detected resonance noise (detection signal level) exceeds a predetermined size, the frequency of the alternating voltage signal applied to the charging member is shifted, by a control unit (50), by a predetermined frequency amount only.
摘要翻译：由施加到充电部件（充电辊）的交流电压的信号引起的谐振噪声的大小由压电器件（PZ）检测，并且在检测到的谐振噪声（检测信号电平）超过预定尺寸，施加到充电部件的交流电压信号的频率仅由控制单元（50）偏移预定频率量。

8. 发明授权

US5613390A Corner reduction device equipped with corner rolls, control device thereof, and method of rolling by using these devices 失效
标题翻译：具有拐角辊的减角装置及其控制装置以及使用这些装置的轧制方法
公开(公告)号：US5613390A
公开(公告)日：1997-03-25
申请号：US344677
申请日：1994-11-21
申请人： Takashi Ishikawa , Takao Yunde , Toshisada Takechi , Katsumi Okada , Takatoshi Amakawa
发明人： Takashi Ishikawa , Takao Yunde , Toshisada Takechi , Katsumi Okada , Takatoshi Amakawa
IPC分类号： B21B1/02 , B21B13/06 , B21B13/10 , B21B37/22 , B21B39/16 , B21B1/30
CPC分类号： B21B1/026 , B21B13/06 , B21B37/22 , B21B13/10 , B21B39/16
摘要： In a corner reduction device for reducing side corners of a slab with corner rolls, a pair of upper and lower corner rolls are mounted inside a unitary unit frame, and a corner roll unit housing the unitary frame which is movable in the direction of width and vertical direction of the material is formed. Vertical position of the corner roll unit is controlled by a lifting power control cylinder through a push rod and position in direction of material width is controlled by a reduction cylinder. Driving of cylinder servo valves is controlled in accordance with position set values set by position setters, load set values set by load setters, and feedback signals from position sensors, thereby controlling the corner roll positions to fixed lateral and vertical positions. The driving of the servo valves is corrected according to values detected by cylinder pressure sensors, to evenly reduce the right and left corners of the material.
摘要翻译：在用于减少具有拐角辊的板坯的侧角的角落减速装置中，一对上下角辊安装在一体的单元框架内，角落辊单元容纳可沿宽度方向移动的整体框架，形成材料的垂直方向。角落辊单元的垂直位置由提升动力控制缸通过推杆控制，并且在材料宽度方向上的位置由减速缸控制。气缸伺服阀的驱动根据由位置设定器设定的位置设定值，由负载设定器设定的负载设定值和来自位置传感器的反馈信号进行控制，从而将角落位置控制为固定的横向和垂直位置。根据气缸压力传感器检测到的值校正伺服阀的驱动，以均匀地减小材料的左右角。

9. 发明授权

US11878886B2 Sheet feeding device and image forming apparatus incorporating same 有权
公开(公告)号：US11878886B2
公开(公告)日：2024-01-23
申请号：US17322756
申请日：2021-05-17
申请人： Katsumi Okada , Takuya Moriyama , Kenichiroh Yamahiro
发明人： Katsumi Okada , Takuya Moriyama , Kenichiroh Yamahiro
IPC分类号： B65H23/00 , B65H7/08
CPC分类号： B65H23/005 , B65H7/08 , B65H2601/11
摘要： A sheet feeding device includes a support, a rotation driver, a guide, a support shaft, a biasing member, a leading end sensor, a roller, an outer diameter sensor, and circuitry. The circuitry causes the rotation driver to rotate a spool in a winding direction to determine a timing at which a signal change rate exceeds a change rate threshold as a passing time at which a leading end of a continuous sheet passes through the leading end sensor, causes the rotation driver to rotate the spool by a rotation angle in the winding direction, from the passing time, to position the leading end of the continuous sheet at a feeding start position, and rotates the spool in a feeding direction to feed the continuous sheet from the feeding start position along a guide portion. Further, the circuitry changes the change rate threshold based on an outer diameter of a roll.

10. 发明授权

US07116933B2 Developing unit, image forming apparatus, and developing method 有权
标题翻译：显影单元，成像设备和显影方法
公开(公告)号：US07116933B2
公开(公告)日：2006-10-03
申请号：US10948560
申请日：2004-09-23
申请人： Katsumi Okada
发明人： Katsumi Okada
IPC分类号： G03G15/08
CPC分类号： G03G15/0907
摘要： A developing unit is adapted to an image forming apparatus of an electrophotographic system that has a two component developing agent. The developing unit deposits a thin layer of toner on a developing roller by way of a magnetic brush on a magnetic roller. The toner then is transferred from the developing roller to a photosensitive drum. Developing bias voltages applied to the rollers have DC and AC components. Thus, electric current alternately flows in the magnetic roller and the developing roller to accelerate toner transfer. Sufficient toner is supplied from the magnetic roller to the developing roller, and sufficient toner is recovered from the developing roller to the magnetic roller. This arrangement lowers the amplitude of the AC bias voltage, thereby eliminating an influence on the photosensitive drum. Further, the frequencies of the AC bias voltages are constant. Thus AC bias voltage generating circuits have a low cost.
摘要翻译：显影单元适用于具有双组分显影剂的电子照相系统的图像形成装置。显影单元通过磁刷将磁性辊上的薄层调色剂沉积在显影辊上。然后将调色剂从显影辊转印到感光鼓上。施加到辊上的显影偏压具有DC和AC分量。因此，电流在磁性辊和显影辊中交替流动，以加速调色剂转印。足够的调色剂从磁辊供应到显影辊，并且足够的调色剂从显影辊回收到磁性辊。这种布置降低了AC偏置电压的幅度，从而消除了对感光鼓的影响。此外，AC偏置电压的频率是恒定的。因此，交流偏压产生电路具有低成本。

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