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1. 发明授权

US5648510A Process for preparation of diaryl carbonate 失效
标题翻译：碳酸二芳基酯的制备方法
公开(公告)号：US5648510A
公开(公告)日：1997-07-15
申请号：US627897
申请日：1996-04-03
申请人： Katsumasa Harada , Yoichi Imbe , Keigo Nishihira , Shuji Tanaka , Satoru Fujitsu , Ryoji Sugise , Koichi Kashiwagi , Toshihiko Sumida
发明人： Katsumasa Harada , Yoichi Imbe , Keigo Nishihira , Shuji Tanaka , Satoru Fujitsu , Ryoji Sugise , Koichi Kashiwagi , Toshihiko Sumida
IPC分类号： C07C67/333 , C07C68/00 , C07D307/68 , C07D333/38 , C07C69/96
CPC分类号： C07C67/333 , C07C68/00 , C07D307/68 , C07D333/38
摘要： A diaryl carbonate is prepared at a high yield and a high selectivity by heating a diaryl oxalate in the presence of an organic phosphorous compound to release carbon monoxide therefrom. A halogen atom-containing compound can be employed in combination with the organic phosphorous compound.
摘要翻译：通过在有机磷化合物的存在下加热草酸二芳基酯从而释放一氧化碳，以高产率和高选择性制备碳酸二芳基酯。含卤原子的化合物可以与有机磷化合物组合使用。

2. 发明授权

US5892091A Catalyst for decarbonylation reaction 失效
标题翻译：催化剂用于脱羰反应
公开(公告)号：US5892091A
公开(公告)日：1999-04-06
申请号：US889390
申请日：1997-07-08
申请人： Katsumasa Harada , Yoichi Imbe , Keigo Nishihira , Shuji Tanaka , Satoru Fujitsu , Ryoji Sugise , Koichi Kashiwagi , Toshihiko Sumida , Takashi Doi , Masayuki Nishio
发明人： Katsumasa Harada , Yoichi Imbe , Keigo Nishihira , Shuji Tanaka , Satoru Fujitsu , Ryoji Sugise , Koichi Kashiwagi , Toshihiko Sumida , Takashi Doi , Masayuki Nishio
IPC分类号： C07C67/333 , C07C68/00 , C07D307/68 , C07D333/38 , C07C69/96
CPC分类号： C07C67/333 , C07C68/00 , C07D307/68 , C07D333/38
摘要： A catalyst composed of an organic phosphorus compound having a trivalent or pentavalent phosphorus atom and at least one carbon-phosphorus bonding or a combination of the organic phosphorus compound and a halogen atom-containing compound is effective for decarbonylation, that is, for releasing carbon monoxide from a compound containing a moiety of --CO--CO--O-- in its molecular structure.
摘要翻译：由具有三价或五价磷原子和至少一个碳 - 磷键的有机磷化合物或有机磷化合物和含卤素原子的化合物的组合的催化剂对脱碳作用是有效的，即用于释放一氧化碳来自在其分子结构中含有-CO-CO-O-部分的化合物。

3. 发明授权

US08690972B2 Hydrogen production system and reforming apparatus 有权
标题翻译：氢气生产系统和改造设备
公开(公告)号：US08690972B2
公开(公告)日：2014-04-08
申请号：US11631536
申请日：2005-07-07
申请人： Yoshinori Takata , Masanori Miyake , Toshihiko Sumida
发明人： Yoshinori Takata , Masanori Miyake , Toshihiko Sumida
IPC分类号： B01J7/00
CPC分类号： C01B3/56 , B01D53/0446 , B01D53/047 , B01D2253/102 , B01D2253/104 , B01D2253/108 , B01D2256/16 , B01D2257/102 , B01D2257/502 , B01D2257/504 , B01D2257/704 , B01D2259/40001 , B01D2259/65 , B01J8/0285 , B01J8/0411 , B01J8/0484 , B01J8/0492 , B01J8/0496 , B01J8/067 , B01J2208/00203 , B01J2208/00504 , B01J2208/00522 , B01J2208/0053 , C01B3/323 , C01B2203/0244 , C01B2203/043 , C01B2203/0465 , C01B2203/047 , C01B2203/0475 , C01B2203/048 , C01B2203/1223 , C01B2203/1288 , Y02C10/08 , Y02P20/152
摘要： A hydrogen production system (X1) according to the present invention includes a reforming apparatus (Y1) having a vaporizer (1) and a reforming reactor (2), and a PSA apparatus (5). In the vaporizer (1) a mixed material (hydrocarbon-based material, water, and oxygen) is heated and vaporized. In the reforming reactor (2), steam reforming reaction and partial oxidation reaction of the hydrocarbon-based material take place at a time, so that reformed gas (containing hydrogen) is led out from the vaporized mixed material. In the PSA apparatus (5), the reformed gas is introduced into an adsorption tower loaded with an adsorbing agent, so that an unnecessary component in the gas is adsorbed by the adsorbing agent and hence hydrogen-rich gas is led out of the tower, while the unnecessary component is desorbed from the adsorbing agent, so that hydrogen-containing desorbed gas that contains the unnecessary component and hydrogen remaining in the tower is discharged out of the tower. The desorbed gas is burnt in the vaporizer (1), and combustion gas generated by burning the desorbed gas is utilized as a heat source to heat the mixed material.
摘要翻译：根据本发明的氢生产系统（X1）包括具有蒸发器（1）和重整反应器（2）的重整装置（Y1）和PSA装置（5）。在蒸发器（1）中，混合材料（烃基材料，水和氧）被加热和蒸发。在重整反应器（2）中，烃类材料一次进行蒸汽重整反应和部分氧化反应，从汽化的混合材料引出重整气体（含氢气）。在PSA装置（5）中，将重整气体引入装载有吸附剂的吸附塔，使吸附剂吸附气体中的不必要成分，将富氢气体从塔内引出，同时不必要的成分从吸附剂中解吸，使得含有残留在塔中的不必要成分和氢的含氢脱附气体排出塔内。解吸气体在蒸发器（1）中燃烧，并且通过燃烧解吸气体产生的燃烧气体用作加热混合材料的热源。

4. 发明申请

US20050268780A1 Method of separating target gas 审中-公开
标题翻译：分离目标气体的方法
公开(公告)号：US20050268780A1
公开(公告)日：2005-12-08
申请号：US10523506
申请日：2003-08-06
申请人： Toshihiko Sumida , Hiroaki Sasano , Masanori Miyake
发明人： Toshihiko Sumida , Hiroaki Sasano , Masanori Miyake
IPC分类号： B01D53/04 , B01D53/047 , B01D53/02
CPC分类号： B01D53/047 , B01D53/261 , B01D2253/104 , B01D2253/108 , B01D2256/16 , B01D2257/102 , B01D2257/504 , B01D2257/7025 , B01D2257/80 , B01D2259/40015 , B01D2259/40024 , B01D2259/40026 , B01D2259/40032 , B01D2259/40045 , B01D2259/40052 , B01D2259/40071 , B01D2259/40075 , B01D2259/403 , Y02C10/08 , Y02C20/20
摘要： The present invention is a gas separation method using a plurality of adsorption columns packed with an adsorbent. A cycle including a series of steps (adsorption, first pressure reduction, second pressure reduction, desorption, scrubbing, and repressurization) is repeated in each adsorption column. In the adsorption step, a gas mixture (G1) is introduced into a column (A) so as to cause the adsorbent to adsorb unnecessary components, and a product gas (G2) is led outside of the column (FIG. 3A). In the first pressure reduction step, the internal pressure of the column (A) is reduced by lead-out of a gas (G3) (FIG. 4A). In the second pressure reduction step, the internal pressure of the column (A) is further reduced by lead-out of the gas (FIG. 4B). In the desorption step, the unnecessary components are desorbed from the adsorbent and purged from the column (A) (FIG. 4C). In the scrubbing step, introduction of the gas (G3) and purging of the gas (G4) are performed simultaneously (FIG. 5A). In the repressurizing step, the internal pressure of the column (A) is raised by introducing the gas (G3) (FIG. 5B). The gas (G3) that is led out from the column (A) during the first pressure reduction step is introduced into the column (C) during the scrubbing step (FIG. 4A), and the gas (G3) that is led out from the column (A) during the second pressure reduction step is introduced into the column (C) during the repressurizing step (FIG. 4B).
摘要翻译：本发明是使用填充有吸附剂的多个吸附塔的气体分离方法。在每个吸附塔中重复包括一系列步骤（吸附，第一次压力降低，第二次压力降低，解吸，洗涤和再加压）的循环。在吸附工序中，将气体混合物（G 1）引入塔（A），使吸附剂吸附不需要的成分，将产物气体（G 2）引入塔外（图3A ）。在第一减压工序中，塔（A）的内压通过气体导出（G 3）而减少（图4A）。在第二减压步骤中，塔（A）的内部压力通过气体引出而进一步减小（图4B）。在解吸步骤中，不必要的组分从吸附剂中解吸并从柱（A）中清除（图4C）。在洗涤步骤中，同时进行气体（G 3）的引入和气体的净化（G 4）（图5A）。在再加压步骤中，通过引入气体（G 3）使柱（A）的内压升高（图5B）。在洗涤步骤（图4A）期间，在第一减压步骤中从塔（A）引出的气体（G 3）被引入塔（C），而气体（G 3）在再加压步骤（图4B）期间，在第二减压步骤期间从塔（A）引出的塔（C）被引入塔（C）。

5. 发明申请

US20100000408A1 HYDROGEN GAS SEPARATION METHOD AND SEPARATION APPARATUS 审中-公开
标题翻译：氢气分离方法和分离装置
公开(公告)号：US20100000408A1
公开(公告)日：2010-01-07
申请号：US12513940
申请日：2007-10-31
申请人： Kazuo Haruma , Hiroaki Sasano , Toshihiko Sumida , Mayumi Fukushima
发明人： Kazuo Haruma , Hiroaki Sasano , Toshihiko Sumida , Mayumi Fukushima
IPC分类号： B01D53/047
CPC分类号： C01B3/382 , B01D53/047 , B01D2253/102 , B01D2253/108 , B01D2256/16 , B01D2259/40071 , B01D2259/403 , B01D2259/4146 , C01B3/56 , C01B2203/0244 , C01B2203/043 , C01B2203/0465 , C01B2203/047 , C01B2203/0475 , C01B2203/048
摘要： A method is provided for separating hydrogen gas from a mixed gas obtained by autothermal reforming reaction of hydrocarbon-based material in which air is added. In this method, by pressure swing adsorption using adsorption towers (A-C) each filled with an adsorbent, a cycle is repeatedly performed, including an adsorption step of introducing the mixed gas into the adsorption tower to adsorb unnecessary gas contained in the mixed gas by the adsorbent to discharge product gas with high hydrogen gas concentration from the adsorption tower, and a desorption step of desorbing the unnecessary gas from the adsorbent to discharge the unnecessary gas from the adsorption tower. The adsorbent includes a 10 to 50% filling percentage of activated carbon-based first adsorbent (D) arranged in the adsorption tower at an upstream portion in the flow direction of the mixed gas and a 90 to 50% filling percentage of zeolite-based second adsorbent (E) arranged in the adsorption tower at a downstream portion in the flow direction.
摘要翻译：提供一种从通过添加空气的烃类材料的自热重整反应得到的混合气体中分离氢气的方法。在该方法中，通过使用吸附塔（AC）进行的变压吸附塔，反复进行循环，包括将混合气体引入吸附塔的吸附工序，吸附混合气体中所含的不需要的气体用于从吸附塔排出具有高氢气浓度的产物气体的吸附剂，以及从吸附剂解吸不需要的气体以从吸附塔排出不需要的气体的解吸步骤。吸附剂包括在混合气体的流动方向的上游部分配置在吸附塔中的活性炭基第一吸附剂（D）的填充百分比为10〜50％，沸石类第二吸附剂的填充率为90〜50％吸附剂（E），其在流动方向的下游部分设置在吸附塔中。

6. 发明授权

US07438746B2 Off-gas feed method and target gas purification system 有权
标题翻译：废气进料方式和目标气体净化系统
公开(公告)号：US07438746B2
公开(公告)日：2008-10-21
申请号：US10546713
申请日：2004-02-16
申请人： Toshihiko Sumida , Hiroaki Sasano , Masanori Miyake
发明人： Toshihiko Sumida , Hiroaki Sasano , Masanori Miyake
IPC分类号： B01D53/047
CPC分类号： B01D53/047 , B01D2253/102 , B01D2253/104 , B01D2253/108 , B01D2256/16 , B01D2257/102 , B01D2257/502 , B01D2257/7025 , B01D2259/40001 , B01D2259/40003 , B01D2259/40007 , B01D2259/40015 , B01D2259/40018 , B01D2259/40024 , B01D2259/4003 , B01D2259/40045 , B01D2259/40052 , B01D2259/40071 , B01D2259/40075 , B01D2259/40081 , B01D2259/403 , B01D2259/404 , Y02C20/20
摘要： The invention provides an off-gas feeding method that supplies the off-gas discharged from a plurality of adsorption towers (A, B, C) to an off-gas consumption unit (1), when performing a pressure swing adsorption process of repeating a cycle including a plurality of steps, to enrich and separate the target gas out of a gas mixture in the adsorption towers (A, B, C) loaded with an adsorbent. The method allows at least one of the plurality of adsorption towers (A, B, C) to discharge the off-gas, in all the steps included in the cycle, so as to continue to supply the off-gas to the off-gas consumption unit (1) without interruption.
摘要翻译：本发明提供一种废气进料方法，其在进行变压吸附过程中，将多个吸附塔（A，B，C）排出的废气供给废气消耗单元（1）循环，包括多个步骤，以从装载有吸附剂的吸附塔（A，B，C）中的气体混合物中富集和分离目标气体。该方法允许多个吸附塔（A，B，C）中的至少一个在循环中包括的所有步骤中排出废气，以便继续向废气中提供废气消费单位（1）不间断。

7. 发明申请

US20060236860A1 Off-gas feed method and object gas purification system 有权
标题翻译：废气进料方法和对象气体净化系统
公开(公告)号：US20060236860A1
公开(公告)日：2006-10-26
申请号：US10546713
申请日：2004-02-16
申请人： Toshihiko Sumida , Hiroaki Sasano , Masanori Miyake
发明人： Toshihiko Sumida , Hiroaki Sasano , Masanori Miyake
IPC分类号： B01D53/02
CPC分类号： B01D53/047 , B01D2253/102 , B01D2253/104 , B01D2253/108 , B01D2256/16 , B01D2257/102 , B01D2257/502 , B01D2257/7025 , B01D2259/40001 , B01D2259/40003 , B01D2259/40007 , B01D2259/40015 , B01D2259/40018 , B01D2259/40024 , B01D2259/4003 , B01D2259/40045 , B01D2259/40052 , B01D2259/40071 , B01D2259/40075 , B01D2259/40081 , B01D2259/403 , B01D2259/404 , Y02C20/20
摘要： The invention provides an off-gas feeding method that supplies the off-gas discharged from a plurality of adsorption towers (A, B, C) to an off-gas consumption unit (1), when performing a pressure swing adsorption process of repeating a cycle including a plurality of steps, to enrich and separate the target gas out of a gas mixture in the adsorption towers (A, B, C) loaded with an adsorbent. The method allows at least one of the plurality of adsorption towers (A, B, C) to discharge the off-gas, in all the steps included in the cycle, so as to continue to supply the off-gas to the off-gas consumption unit (1) without interruption.
摘要翻译：本发明提供一种废气进料方法，其在进行变压吸附过程中，将多个吸附塔（A，B，C）排出的废气供给废气消耗单元（1）循环，包括多个步骤，以从装载有吸附剂的吸附塔（A，B，C）中的气体混合物中富集和分离目标气体。该方法允许多个吸附塔（A，B，C）中的至少一个在循环中包括的所有步骤中排出废气，以便继续向废气中提供废气消费单位（1）不间断。

8. 发明申请

US20070237691A1 Hydrogen Production System and Reforming Apparatus 有权
标题翻译：氢气生产系统和改造设备
公开(公告)号：US20070237691A1
公开(公告)日：2007-10-11
申请号：US11631536
申请日：2005-07-07
申请人： Yoshinori Takata , Masanori Miyake , Toshihiko Sumida
发明人： Yoshinori Takata , Masanori Miyake , Toshihiko Sumida
IPC分类号： C01B3/38 , B01D53/04 , C01B3/56
CPC分类号： C01B3/56 , B01D53/0446 , B01D53/047 , B01D2253/102 , B01D2253/104 , B01D2253/108 , B01D2256/16 , B01D2257/102 , B01D2257/502 , B01D2257/504 , B01D2257/704 , B01D2259/40001 , B01D2259/65 , B01J8/0285 , B01J8/0411 , B01J8/0484 , B01J8/0492 , B01J8/0496 , B01J8/067 , B01J2208/00203 , B01J2208/00504 , B01J2208/00522 , B01J2208/0053 , C01B3/323 , C01B2203/0244 , C01B2203/043 , C01B2203/0465 , C01B2203/047 , C01B2203/0475 , C01B2203/048 , C01B2203/1223 , C01B2203/1288 , Y02C10/08 , Y02P20/152
摘要： A hydrogen production system (X1) according to the present invention includes a reforming apparatus (Y1) having a vaporizer (1) and a reforming reactor (2), and a PSA apparatus (5). In the vaporizer (1) a mixed material (hydrocarbon-based material, water, and oxygen) is heated and vaporized. In the reforming reactor (2), steam reforming reaction and partial oxidation reaction of the hydrocarbon-based material take place at a time, so that reformed gas (containing hydrogen) is led out from the vaporized mixed material. In the PSA apparatus (5), the reformed gas is introduced into an adsorption tower loaded with an adsorbing agent, so that an unnecessary component in the gas is adsorbed by the adsorbing agent and hence hydrogen-rich gas is led out of the tower, while the unnecessary component is desorbed from the adsorbing agent, so that hydrogen-containing desorbed gas that contains the unnecessary component and hydrogen remaining in the tower is discharged out of the tower. The desorbed gas is burnt in the vaporizer (1), and combustion gas generated by burning the desorbed gas is utilized as a heat source to heat the mixed material.
摘要翻译：根据本发明的氢生产系统（X 1）包括具有蒸发器（1）和重整反应器（2）的重整装置（Y 1）和PSA装置（5）。在蒸发器（1）中，混合材料（烃基材料，水和氧）被加热和蒸发。在重整反应器（2）中，烃类材料一次进行蒸汽重整反应和部分氧化反应，从汽化的混合材料引出重整气体（含氢气）。在PSA装置（5）中，将重整气体引入装载有吸附剂的吸附塔，使吸附剂吸附气体中的不必要成分，将富氢气体从塔内引出，同时不必要的成分从吸附剂中解吸，使得含有残留在塔中的不必要成分和氢的含氢脱附气体排出塔内。解吸气体在蒸发器（1）中燃烧，并且通过燃烧解吸气体产生的燃烧气体用作加热混合材料的热源。

9. 发明授权

US5093505A Novel heterocyclic compound, carcinostatic agent, and carcinoma controlling method 失效
标题翻译：新型杂环化合物，制癌剂和癌症控制方法
公开(公告)号：US5093505A
公开(公告)日：1992-03-03
申请号：US528826
申请日：1990-05-25
申请人： Hoyoku Nishino , Yukihiro Kodera , Toshihiko Sumida , Susumu Yoshida , Hiromichi Matsuura , Yoichi Itakura
发明人： Hoyoku Nishino , Yukihiro Kodera , Toshihiko Sumida , Susumu Yoshida , Hiromichi Matsuura , Yoichi Itakura
IPC分类号： A61K31/35 , A61K31/351 , A61K31/44 , A61K31/4409 , A61K31/4418 , A61K31/4425 , A61K36/896 , A61P35/00 , C07D213/69 , C07D213/70 , C07D309/34 , C07D309/38 , C07D309/40
CPC分类号： C07D213/69 , C07D213/70 , C07D309/34 , C07D309/40
摘要： Heterocyclic compounds of the general formula: ##STR1## wherein R.sup.11 is a hydroxyl group or a lower alkoxy group, R.sup.12 is a lower alkoxy group, R.sup.13 is a saturated or unsaturated hydrocarbon group, X is an oxygen atom or a sulfur atom, and Y is an oxygen atom or --NH-- which may have a lower alkyl substituent, or salts thereof are novel and effective in controlling carcinoma.
摘要翻译：其中R11为羟基或低级烷氧基，R12为低级烷氧基，R13为饱和或不饱和烃基，X为氧原子或硫原子，Y为氧原子或硫原子的杂环化合物，可以具有低级烷基取代基的氧原子或-NH-，或其盐在控制癌中是新颖有效的。

10. 发明授权

US08048177B2 Method for treatment of drain in hydrogen production and hydrogen production system 有权
标题翻译：氢气生产和氢气生产系统排水处理方法
公开(公告)号：US08048177B2
公开(公告)日：2011-11-01
申请号：US12300366
申请日：2007-05-07
申请人： Toshihiko Sumida , Yoshinori Takata , Masanori Miyake , Yoshiaki Imoto
发明人： Toshihiko Sumida , Yoshinori Takata , Masanori Miyake , Yoshiaki Imoto
IPC分类号： B01J7/00 , C01B3/36 , C01B6/24 , C01B3/02 , C10J3/46 , C02F1/72 , C02F1/68
CPC分类号： C01B3/323 , B01J8/025 , B01J2208/00203 , B01J2208/00504 , B01J2208/0053 , B01J2208/00716 , C01B2203/0233 , C01B2203/0261 , C01B2203/043 , C01B2203/0495 , C01B2203/0822 , C01B2203/0827 , C01B2203/0883 , C01B2203/1076 , C01B2203/1223 , C01B2203/1288 , C01B2203/1604 , H01M8/0631 , H01M8/0662 , Y02P20/128 , Y02P20/52
摘要： A method for treating drain in hydrogen production includes steps of gasifying in a gasifier (1), reforming in a reformer (2), gas-liquid separation in a gas-liquid separator (4), PSA gas separation in a PSA separator (5) and evaporation in a drain treatment unit (6). In the gasifying, a mixed material containing methanol is heated and gasified. In the reforming, reformed gas containing hydrogen is produced from the mixed material by reforming reaction of methanol. In the gas-liquid separation, a liquid component is separated from the reformed gas and discharged as drain. In the PSA gas separation, hydrogen-rich gas and offgas are extracted from the reformed gas by PSA separation using an adsorption tower. In the gasifying, the offgas is burned, and the mixed material is heated by using the combustion gas as heat source. In the evaporation, drain is evaporated using the combustion gas after heating the mixed material as heat source.
摘要翻译：用于处理氢气生产中的排水的方法包括在气化器（1）中气化，重整器（2）中的重整，气 - 液分离器（4）中的气液分离，PSA分离器（5）中的PSA气体分离）并在排水处理单元（6）中蒸发。在气化中，将含有甲醇的混合物质加热并气化。在重整中，通过甲醇的重整反应，由混合材料产生含氢气的重整气体。在气液分离中，将液体成分从重整气体中分离出来，排出。在PSA气体分离中，使用吸附塔通过PSA分离从重整气体中提取富氢气体和废气。在气化中，废气被燃烧，并且通过使用燃烧气体作为热源来加热混合物。在蒸发中，加热混合材料作为热源后，使用燃烧气体蒸发排出物。

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