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1. 发明授权

US08231938B2 Method for production of enzyme granules and enzyme granules produced thus 有权
标题翻译：因此生产酶颗粒和酶颗粒的方法
公开(公告)号：US08231938B2
公开(公告)日：2012-07-31
申请号：US10560372
申请日：2004-05-26
申请人： Karlheinz Rümpler , Michael Jacob , Mike Waskow
发明人： Karlheinz Rümpler , Michael Jacob , Mike Waskow
IPC分类号： B05D7/00
CPC分类号： C12N9/98 , A23K20/189 , A23K40/10 , A23L29/06 , A23P10/22 , A61K9/1688 , B01J2/16 , C12N9/16
摘要： A method of producing enzyme granulates, enzyme granulates produced By the method, and the use thereof in formulations is provided, for example, for animal feed, foodstuffs, washing agents, rinsing agents or for pharmaceutical uses. The enzyme granulates have a high relative proportion of active enzyme, particular particle size, good shelf life, particularly small rounding factors and/or low residual moisture proportion, and further specific properties. The production of the enzyme granulates is achieved by linking of the thermal conditions in the injection zone and temperature conditions in the remainder of the apparatus. This is achieved by introduction of heated process gasses for drying exclusively in the injection zone. The secure introduction of articles into the injection zone is achieved by the specific geometric arrangement of the apparatus using gravity. The absolute value for enzyme activity of the enzyme granulates can be controlled by the addition of particles as seed material for the granules.
摘要翻译：提供了制备酶颗粒的方法，通过该方法制备的酶颗粒及其在制剂中的用途，例如用于动物饲料，食品，洗涤剂，漂洗剂或药物用途。酶颗粒具有高的相对比例的活性酶，特定的粒度，良好的保存期限，特别是小的圆化因子和/或低残留水分比例，以及进一步的具体特性。酶颗粒的生产通过在注射区中的热条件和装置的其余部分中的温度条件的连接来实现。这是通过引入用于在注射区域中专门干燥的加热过程气体来实现的。通过使用重力的装置的特定几何布置来实现将物品牢固地引入注射区域。酶颗粒的酶活性的绝对值可以通过加入颗粒作为颗粒的种子材料来控制。

2. 发明授权

US07767161B2 Fluidized bed apparatus for batch-by-batch or continuous process control and method for operating a fluidized bed apparatus 有权
标题翻译：用于分批或连续过程控制的流化床设备和用于操作流化床设备的方法
公开(公告)号：US07767161B2
公开(公告)日：2010-08-03
申请号：US11448406
申请日：2006-06-07
申请人： Michael Jacob , Karlheinz Rümpler , Mike Waskow
发明人： Michael Jacob , Karlheinz Rümpler , Mike Waskow
IPC分类号： B01J8/18 , F27B15/00
CPC分类号： B01J8/1854 , B01J8/1818 , B01J8/26 , B01J8/34 , B01J8/36 , B01J8/386 , B01J2208/00884
摘要： A fluidized bed apparatus for batch-by-batch or continuous process control is provided that allows the processes in the fluidization region to be influenced as desired, especially in terms of material movement and dwell time. The fluidized bed apparatus is formed from at least two processing regions and the processing regions are connected to each other by overflow channels. The first processing region is provided with a solids inlet and the last processing region is provided with a solids outlet. For influencing the dwell time, the material to be treated is supplied to at least two processing regions one after the other and flows through these regions, wherein the material transport direction is a cross flow relative to the flow of the fluidization means.
摘要翻译：提供了一种用于分批或连续过程控制的流化床设备，其允许流化区域中的过程受到影响，特别是在材料运动和停留时间方面。流化床装置由至少两个处理区域形成，并且处理区域通过溢流通道相互连接。第一处理区域设置有固体入口，最后一个处理区域设置有固体出口。为了影响停留时间，将待处理的材料一个接一个地供给至少两个处理区域，并且流过这些区域，其中材料输送方向是相对于流化装置的流动的横流。

3. 发明授权

US07691438B2 Enzyme granulate production method and resulting enzyme granulates 有权
标题翻译：酶粒生产方法和所得酶制粒
公开(公告)号：US07691438B2
公开(公告)日：2010-04-06
申请号：US10862238
申请日：2004-06-07
申请人： Michael Jacob , Karlheinz Rümpler , Mike Waskow
发明人： Michael Jacob , Karlheinz Rümpler , Mike Waskow
IPC分类号： B05D7/00
CPC分类号： C12N9/98 , A23K20/189 , A23K40/10 , A23L29/06 , A23P10/22 , A61K9/1688 , B01J2/16 , C12N9/16
摘要： A method for producing enzyme granulates, the resulting enzyme granulates, and their use in formulations, e.g., for animal feed, food, washing means, rinsing means, and/or for pharmaceutical purposes and the like. The enzyme granulates show, in particular, a high relative percentage of active enzymes, certain grain sizes, good storage stability, especially small roundness factor, and/or low residual moisture percentage as well as preferably additional specific properties. According to the invention, the enzyme granulates are produced by linking the thermal conditions in the spray zone and the temperature conditions in the remaining region of the fluidized bed. In the process according to the invention, this is achieved in that the supply of heated processing gas is realized for drying exclusively in the injection region. The reliable supply of particles in the injection region is realized through the special geometrical shape of the apparatus under the use of gravity. Through the addition of inert particles as nuclei material for cores, the absolute content of enzyme activity of the enzyme granulate can be controlled.
摘要翻译：生产酶颗粒的方法，所得的酶颗粒及其在制剂中的用途，例如用于动物饲料，食品，洗涤方法，漂洗装置和/或用于药物目的等。酶颗粒特别表现出活性酶的高相对百分比，某些晶粒尺寸，良好的储存稳定性，特别是小圆度因子和/或低残留水分百分比以及优选额外的特定性质。根据本发明，通过将喷雾区中的热条件和流化床的剩余区域中的温度条件相关联来生产酶颗粒。在根据本发明的方法中，实现了加热处理气体的供应被实现用于仅在喷射区域中进行干燥。通过重力使用设备的特殊几何形状，可以实现注射区域中可靠的颗粒供应。通过添加惰性颗粒作为芯的核材料，可以控制酶颗粒的酶活性的绝对含量。

4. 发明授权

US07241425B2 Fluidized bed apparatus for batch-by-batch or continuous process control and method for operating a fluidized bed apparatus 有权
标题翻译：用于分批或连续过程控制的流化床设备和用于操作流化床设备的方法
公开(公告)号：US07241425B2
公开(公告)日：2007-07-10
申请号：US10756093
申请日：2004-01-13
申请人： Michael Jacob , Karlheinz Rümpler , Mike Waskow
发明人： Michael Jacob , Karlheinz Rümpler , Mike Waskow
IPC分类号： B32B5/02
CPC分类号： B01J8/1854 , B01J8/1818 , B01J8/26 , B01J8/34 , B01J8/36 , B01J8/386 , B01J2208/00884
摘要： A fluidized bed apparatus for batch-by-batch or continuous process control is provided that allows the processes in the fluidization region to be influenced as desired, especially in terms of material movement and dwell time. The fluidized bed apparatus is formed from at least two processing regions and the processing regions are connected to each other by overflow channels. The first processing region is provided with a solids inlet and the last processing region is provided with a solids outlet. For influencing the dwell time, the material to be treated is supplied to at least two processing regions one after the other and flows through these regions, wherein the material transport direction is a cross flow relative to the flow of the fluidization means.
摘要翻译：提供了一种用于分批或连续过程控制的流化床设备，其允许流化区域中的过程受到影响，特别是在材料运动和停留时间方面。流化床装置由至少两个处理区域形成，并且处理区域通过溢流通道相互连接。第一处理区域设置有固体入口，最后一个处理区域设置有固体出口。为了影响停留时间，将待处理的材料一个接一个地供给至少两个处理区域，并且流过这些区域，其中材料输送方向是相对于流化装置的流动的横流。

5. 发明授权

US07709036B2 Method for granulating malt extracts 有权
标题翻译：造粒麦芽提取物的方法
公开(公告)号：US07709036B2
公开(公告)日：2010-05-04
申请号：US11151629
申请日：2005-06-13
申请人： Karlheinz Rümpler , Mike Waskow , Bernhard Wand
发明人： Karlheinz Rümpler , Mike Waskow , Bernhard Wand
IPC分类号： A23L3/46
CPC分类号： A23P10/20
摘要： A method for producing granules made from malt extract is provided. The method provides for producing granules continuously or in batches under the prevention as much as possible of non-uniform temperature distributions in the production process. Simultaneously, the controllability of the granulation in the production is improved. This is realized by linking thermal conditions in the spraying zone and the temperature conditions in other region of the apparatus. This is achieved such that the supply of the heated process gas for drying is realized exclusively in the spraying region. The reliable supply of particles into the spraying region is performed through the special geometric configuration of the apparatus under the use of gravity.
摘要翻译：提供了由麦芽提取物制造颗粒的方法。该方法提供了在生产过程中尽可能多地预防不均匀的温度分布来连续或分批地生产颗粒。同时，生产中造粒的可控性提高。这是通过将喷涂区中的热条件和装置的其他区域中的温度条件相关联来实现的。实现这一点，使得仅在喷射区域中实现用于干燥的加热过程气体的供应。通过重力使用设备的特殊几何结构，可以将可靠的颗粒供应到喷涂区域。

6. 发明申请

US20090087351A1 APPARATUS FOR DEPOSITING FLUIDS IN A SOLIDS FLOW OF A SPOUTED BED APPARATUS 有权
标题翻译：用于在散发的床装置的固体流中沉积流体的装置
公开(公告)号：US20090087351A1
公开(公告)日：2009-04-02
申请号：US12193553
申请日：2008-08-18
申请人： Michael Jacob , Karlheinz Rumpler , Mike Waskow
发明人： Michael Jacob , Karlheinz Rumpler , Mike Waskow
IPC分类号： B01J8/18
CPC分类号： B01J2/16
摘要： An apparatus for introducing fluids into a solids flow of a spouted bed apparatus is provided. The apparatus includes a spray nozzle which opens into a reaction space of the spouted bed apparatus. A lower region of the reaction space is provided with a rectangular cross section for the spouted bed apparatus and is limited in an axial direction by at least one inclined stream return flow wall and an oppositely inclined stream inlet wall with the formation of an axial gap through the reaction space for supplying inlet air. At least one nozzle is also provided for introducing fluid above the gap opens into the reaction space.
摘要翻译：提供了一种用于将流体引入喷射床装置的固体流中的装置。该装置包括通向喷射床装置的反应空间的喷嘴。反应空间的下部区域设置有用于喷射床装置的矩形横截面，并且通过至少一个倾斜流回流壁和相对倾斜的流入口壁沿轴向方向限制，其形成轴向间隙通过用于供应入口空气的反应空间。还提供至少一个喷嘴，用于将间隙上方的流体引入反应空间。

7. 发明申请

US20070093403A1 Method for production of enzyme granules and enzyme granules produced thus 有权
标题翻译：因此生产酶颗粒和酶颗粒的方法
公开(公告)号：US20070093403A1
公开(公告)日：2007-04-26
申请号：US10560372
申请日：2004-05-26
申请人： Karlheinz Rumpler , Michael Jacob , Mike Waskow
发明人： Karlheinz Rumpler , Michael Jacob , Mike Waskow
IPC分类号： C11D3/386 , C12N11/04
CPC分类号： C12N9/98 , A23K20/189 , A23K40/10 , A23L29/06 , A23P10/22 , A61K9/1688 , B01J2/16 , C12N9/16
摘要： A method of producing enzyme granulates, enzyme granulates produced by the method, and the use thereof in formulations is provided, for example, for animal feed, foodstuffs, washing agents, rinsing agents or for pharmaceutical uses. The enzyme granulates have a high relative proportion of active enzyme, particular particle size, good shelf life, particularly small rounding factors and/or low residual moisture proportion, and further specific properties. The production of the enzyme granulates is achieved by linking of the thermal conditions in the injection zone and temperature conditions in the remainder of the apparatus. This is achieved by introduction of heated process gasses for drying exclusively in the injection zone. The secure introduction of articles into the injection zone is achieved by the specific geometric arrangement of the apparatus using gravity. The absolute value for enzyme activity of the enzyme granulates can be controlled by the addition of particles as seed material for the granules.
摘要翻译：提供了制备酶颗粒的方法，通过该方法制备的酶颗粒及其在制剂中的用途，例如用于动物饲料，食品，洗涤剂，漂洗剂或用于制药用途。酶颗粒具有高的相对比例的活性酶，特定的粒度，良好的保存期限，特别是小的圆化因子和/或低残留水分比例，以及进一步的具体特性。酶颗粒的生产通过在注射区中的热条件和装置的其余部分中的温度条件的连接来实现。这是通过引入用于在注射区域中专门干燥的加热过程气体来实现的。通过使用重力的装置的特定几何布置来实现将物品牢固地引入注射区域。酶颗粒的酶活性的绝对值可以通过加入颗粒作为颗粒的种子材料来控制。

8. 发明申请

US20060228661A1 Fluidized bed apparatus for batch-by-batch or continuous process control and method for operating a fluidized bed apparatus 有权
标题翻译：用于分批或连续过程控制的流化床设备和用于操作流化床设备的方法
公开(公告)号：US20060228661A1
公开(公告)日：2006-10-12
申请号：US11448406
申请日：2006-06-07
申请人： Michael Jacob , Karlheinz Rumpler , Mike Waskow
发明人： Michael Jacob , Karlheinz Rumpler , Mike Waskow
IPC分类号： F27B15/00
CPC分类号： B01J8/1854 , B01J8/1818 , B01J8/26 , B01J8/34 , B01J8/36 , B01J8/386 , B01J2208/00884
摘要： A fluidized bed apparatus for batch-by-batch or continuous process control is provided that allows the processes in the fluidization region to be influenced as desired, especially in terms of material movement and dwell time. The fluidized bed apparatus is formed from at least two processing regions and the processing regions are connected to each other by overflow channels. The first processing region is provided with a solids inlet and the last processing region is provided with a solids outlet. For influencing the dwell time, the material to be treated is supplied to at least two processing regions one after the other and flows through these regions, wherein the material transport direction is a cross flow relative to the flow of the fluidization means.
摘要翻译：提供了一种用于分批或连续过程控制的流化床设备，其允许流化区域中的过程受到影响，特别是在材料运动和停留时间方面。流化床装置由至少两个处理区域形成，并且处理区域通过溢流通道相互连接。第一处理区域设置有固体入口，最后一个处理区域设置有固体出口。为了影响停留时间，将待处理的材料一个接一个地供给至少两个处理区域，并且流过这些区域，其中材料输送方向是相对于流化装置的流动的横流。

9. 发明授权

US07993595B2 Apparatus for depositing fluids in a solids flow of a spouted bed apparatus 有权
标题翻译：用于在喷射床装置的固体流中沉积流体的装置
公开(公告)号：US07993595B2
公开(公告)日：2011-08-09
申请号：US12193553
申请日：2008-08-18
申请人： Michael Jacob , Karlheinz Rumpler , Mike Waskow
发明人： Michael Jacob , Karlheinz Rumpler , Mike Waskow
IPC分类号： B01J8/18
CPC分类号： B01J2/16
摘要： An apparatus for introducing fluids into a solids flow of a spouted bed apparatus is provided. The apparatus includes a spray nozzle which opens into a reaction space of the spouted bed apparatus. A lower region of the reaction space is provided with a rectangular cross section for the spouted bed apparatus and is limited in an axial direction by at least one inclined stream return flow wall and an oppositely inclined stream inlet wall with the formation of an axial gap through the reaction space for supplying inlet air. At least one nozzle is also provided for introducing fluid above the gap opens into the reaction space.
摘要翻译：提供了一种用于将流体引入喷射床装置的固体流中的装置。该装置包括通向喷射床装置的反应空间的喷嘴。反应空间的下部区域设置有用于喷射床装置的矩形横截面，并且通过至少一个倾斜流回流壁和相对倾斜的流入口壁沿轴向方向限制，其形成轴向间隙通过用于供应入口空气的反应空间。还提供至少一个喷嘴，用于将间隙上方的流体引入反应空间。

10. 发明申请

US20060035022A1 Process to coat granular and powdered materials 审中-公开
公开(公告)号：US20060035022A1
公开(公告)日：2006-02-16
申请号：US11253380
申请日：2005-10-19
申请人： Karlheinz Rumpler , Michael Jacob , Mike Waskow
发明人： Karlheinz Rumpler , Michael Jacob , Mike Waskow
IPC分类号： B05D7/00
CPC分类号： C11D17/0039 , A23P10/22 , A23P10/30 , A23P10/35 , A23V2002/00 , B01J2/006 , B01J2/16 , C01B15/106 , C11D1/90 , C11D3/3942 , C11D11/0088 , A23V2250/1842 , A23V2200/224
摘要： A process to coat granular through powdered material for particular bulk products that is cost-effective for bulk products and in which the coated product is produced continuously and in a quality and throughput that meets requirements for bulk products is provided. This is attained by the coating material being applied to the granular through powdered material particles in the form of a coating matrix that does not completely envelope the material particles with coating material, with the matrix then being dried and solidified by the process air, the coating material is applied continuously to the bed of material in a continuously operated fluidized bed in at least two different zones. The coating material is applied to the material particles located in the fluidized bed in the form of solutions, suspensions or melts with a solids fraction of 0.5 to 100%, preferably 2 to 20%. The coating materials are preferably inorganic salts, fats, waxes, celluloses, stearates, metals or metal compounds, and the temperature of the air fed to the fluidized bed for the coating area is dependent on the material, and is between −20° C. to +300° C. The end product is continuously discharged from the fluidized bed.

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