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1. 发明专利

JP2011012009A Method for producing alicyclic alcohol 有权
标题翻译：生产水性醇的方法
公开(公告)号：JP2011012009A
公开(公告)日：2011-01-20
申请号：JP2009157125
申请日：2009-07-01
申请人： Kao Corp , Mitsubishi Gas Chemical Co Inc , 三菱瓦斯化学株式会社 , 花王株式会社
发明人： KITAMURA MITSUHARU , KOTACHI SHINJI , NAGASAWA SHINYA , ATAKA YOSHIHARU
IPC分类号： C07C29/154 , C07B61/00 , C07C33/14
CPC分类号： C07C29/149 , C07C51/58 , C07C67/14 , C07C2601/14 , C07C31/1355 , C07C69/75 , C07C61/08
摘要： PROBLEM TO BE SOLVED: To produce an alicyclic alcohol useful as a raw material of a formulation perfumery, at a low cost and in a high yield.SOLUTION: This alicyclic alcohol expressed by formula (III) can be produced under low CO pressure in the high yield by carbonylating an unsaturated hydrocarbon expressed by formula (I) by using carbon monoxide in the presence of HF to obtain a cyclohexane carbonyl compound expressed by formula (II) and then reducing the cyclohexane carbonyl compound expressed by formula (II) [in these formulae, Ris 1-4C alkyl; Ris 1-4C alkyl; Ris any of OH, F and OR; and Ris 1-4C alkyl].
摘要翻译：要解决的问题：以低成本和高产率制备可用作配方香料原料的脂环族醇。溶液：由式（III）表示的该脂环醇可以在低CO压力下生产通过在HF存在下使用一氧化碳羰基化由式（I）表示的不饱和烃而得到由式（II）表示的环己烷羰基化合物，然后还原由式（II）表示的环己烷羰基化合物[在这些中 Ris 1-4C烷基; Ris 1-4C烷基; 任何OH，F和OR; 和Ris 1-4C烷基]。

2. 发明专利

JP2010215529A Method for producing cyclohexyl alkanol 有权
标题翻译：生产环丙基亚胺醇的方法
公开(公告)号：JP2010215529A
公开(公告)日：2010-09-30
申请号：JP2009061468
申请日：2009-03-13
申请人： Kao Corp , 花王株式会社
发明人： NAGASAWA SHINYA , KOTACHI SHINJI , TOKI NAOTOSHI
IPC分类号： C07C29/14 , C07B61/00 , C07C29/143 , C07C31/135 , C07C33/14 , C11B9/00
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a cyclohexyl alkanol which can impart the floral fragrance having creamy sweetness possessed by natural flowers and much includes a cis-form isomer and a perfume composition containing the cyclohexyl alkanol. SOLUTION: The method for producing a cyclohexyl alkanol represented by formula (III) (wherein R 1 is a 2-4C hydrocarbon; R 4 is a 1-4C hydrocarbon group, provided that when R 1 is an isopropyl group, R 4 is always a methyl; and R 5 is hydrogen or a 1-4C hydrocarbon) comprises obtaining a carbonyl compound represented by formula (II) [wherein R 1 and R 4 are the same as defined above and R 2 is hydrogen, a 1-4C hydrocarbon group or OR 3 (wherein R 3 is hydrogen or a 1-10C hydrocarbon group)] with the use of a carbonyl compound represented by formula (I) (wherein R 1 and R 2 are the same as defined above) and thereafter reducing the carbonyl compound. The perfume composition contains the cyclohexyl alkanol. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：提供一种生产环己基链烷醇的方法，其可以赋予天然花所具有的具有奶油甜度的花香，并且包括顺式异构体和含有环己基链烷醇的香料组合物。解决方案：由式（III）表示的环己基链烷醇的制备方法（其中R 1 为2-4C烃; R 4 为1-4C 烃基，条件是当R 1是异丙基时，R SP 4总是甲基; R 5是氢或1- 4C烃）包括获得由式（II）表示的羰基化合物[其中R 1和R 2与上述定义相同，并且R 2 SP / >为氢，1-4C烃基或OR 3，其中R 3为氢或1-10C烃基）]，其中使用代表的羰基化合物通过式（I）（其中R 1 和R 2 与上述定义相同），然后还原羰基化合物。香料组合物含有环己基链烷醇。版权所有（C）2010，JPO＆INPIT

3. 发明专利

JP2008094731A Ester compound 有权
标题翻译： ESTER化合物
公开(公告)号：JP2008094731A
公开(公告)日：2008-04-24
申请号：JP2006275446
申请日：2006-10-06
申请人： Kao Corp , 花王株式会社
发明人： KOTACHI SHINJI , FUKUDA KAZUYUKI , ONO SATORU
IPC分类号： C07C67/08 , C07B61/00 , C07C69/24
摘要： PROBLEM TO BE SOLVED: To provide an ester compound which has a refreshing, fruity green-like floral fragrance, and is useful as a perfuming ingredient for compound perfume raw materials, flavoring agents, and the like, and to provide a method for producing the same. SOLUTION: The ester compound is represented by general formula (I) (R 1 and R 2 are each independently a 1-4C alkyl). COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供具有清爽，果香绿色花香味的酯化合物，并且可用作复合香料原料，调味剂等的加香成分，并提供方法为了生产相同。溶剂：酯化合物由通式（I）表示（R 1 SP＆gt;和R 2 SP 2各自独立地为1-4C烷基）。版权所有（C）2008，JPO＆INPIT

4. 发明专利

JP2009149811A Aldehyde compound 有权
标题翻译：醛类化合物
公开(公告)号：JP2009149811A
公开(公告)日：2009-07-09
申请号：JP2007330309
申请日：2007-12-21
申请人： Kao Corp , 花王株式会社
发明人： TOKI NAOTOSHI , KOTACHI SHINJI
IPC分类号： C11B9/00 , C07B61/00 , C07C45/68 , C07C47/32
摘要： PROBLEM TO BE SOLVED: To provide an aldehyde compound which does not have a strong aldehyde scent, which may limit its use as a perfume raw material, but has fresh sweetness and floral aroma, and a process of its production, and to provide a perfume composition containing the aldehyde compound.
SOLUTION: A perfume composition comprises an aldehyde compound expressed by general formula (I), wherein R
1 represents a 1C-4C hydrocarbon group, R
2 represents a 2C-4C saturated hydrocarbon group. R
1 and R
2 are bonded to the 2, 3 or 4 position of the aldehyde compound on a cyclohexane ring.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：待解决的问题：为了提供不具有强醛香味的醛化合物，其可能限制其作为香料原料的用途，但具有新鲜的甜味和花香香气，以及其生产方法，以及提供含有醛化合物的香料组合物。解决方案：香料组合物包含由通式（I）表示的醛化合物，其中R 1 SP 1表示1C-4C烃基，R SP 2表示2C -4C饱和烃基。 R 1 和R 2 键合在醛化合物的2,3或4位上环己烷环上。版权所有（C）2009，JPO＆INPIT

5. 发明专利

JP2003055312A Optically active ester 有权
标题翻译：光学有效的ESTER
公开(公告)号：JP2003055312A
公开(公告)日：2003-02-26
申请号：JP2001243845
申请日：2001-08-10
申请人： Kao Corp , 花王株式会社
发明人： KOTACHI SHINJI , ONO SATORU , ETSUNO JIYUNJI
IPC分类号： C07C69/14 , C07C69/24 , C11B9/00
摘要： PROBLEM TO BE SOLVED: To provide a fragrant material having intense fragrance with more characteristic fragrant quality as a fragrance to be used in fragrant products including toiletries and cosmetics, and to provide a fragrant composition containing the above material.
SOLUTION: This fragrant material is an optically active ester, i.e., a (1R,2 R)-2-tert-butylcyclohexanol fatty acid ester selected from the group consisting of (1R,2R)-2-tert-butylcyclohexyl formate, (1R,2R)-2-tert-butylcyclohexyl acetate, (1R,2R)-2-tert-butylcyclohexyl propionate, (1R,2R)-2-tert-butylcyclohexyl butyrate and (1R,2R)-2-tert-butylcyclohexyl pentanoate.
COPYRIGHT: (C)2003,JPO
摘要翻译：要解决的问题：提供一种具有强烈香味的芳香物质，具有更加特征的香味，作为用于包括化妆品和化妆品的芳香产品中的香料，并提供含有上述材料的芳香组合物。解决方案：该香料为光学活性酯，即选自（1R，2R）-2-叔丁基环己基甲酸酯的（1R，2R）-2-叔丁基环己醇脂肪酸酯，（1R ，2R）-2-叔丁基环己基乙酸酯，（1R，2R）-2-叔丁基环己基丙酸酯，（1R，2R）-2-叔丁基环己基丁酸酯和（1R，2R）-2-叔丁基环己基戊酸酯。

6. 发明专利

JP2012140536A Perfume composition 有权
标题翻译： PERFUME组合物
公开(公告)号：JP2012140536A
公开(公告)日：2012-07-26
申请号：JP2010294146
申请日：2010-12-28
申请人： Kao Corp , 花王株式会社
发明人： MUROI MAKIKO , KOTACHI SHINJI , TOKI NAOTOSHI
IPC分类号： C11B9/00 , A61K8/34 , A61Q13/00
摘要： PROBLEM TO BE SOLVED: To provide a perfume composition including a compound having an excellent harmonic content with other various perfumes, and allowing impartment of a stronger fruity green feeling or fresh feeling by compounding, and to provide the use of the compound as a perfuming ingredient.SOLUTION: There are provided the perfume composition including the compound represented by general formula (I) (wherein, Rand Rrepresent each mutually independently methyl or ethyl); and the use of the compound as the perfuming ingredient.
摘要翻译：要解决的问题：提供一种香料组合物，其包含与其它各种香料具有优异的谐波含量的化合物，并且通过配混可以赋予更强的果香绿色感或新鲜感，并提供化合物的用途，作为一种加香成分。提供了包含通式（I）表示的化合物的香料组合物（其中，R 1 和R 2 < / SP>各自相互独立地表示甲基或乙基）; 以及使用该化合物作为加香成分。版权所有（C）2012，JPO＆INPIT

7. 发明专利

JP2009209326A Fragrance composition 有权
标题翻译： FRAGRANCE组成
公开(公告)号：JP2009209326A
公开(公告)日：2009-09-17
申请号：JP2008056542
申请日：2008-03-06
申请人： Kao Corp , 花王株式会社
发明人： KOTACHI SHINJI , NAGASAWA SHINYA , ONO SATORU
IPC分类号： C11B9/00
CPC分类号： C11B9/0034
摘要： PROBLEM TO BE SOLVED: To provide a fragrance composition as a fruity fragrance material, having a characteristic nuance of a fresh tree, a flower or a leaf not known conventionally, and capable of changing an odor of a blended fragrance to polished one while blended with various fragrances. SOLUTION: This fragrance composition contains a compound expressed by General Formula (I), where R 1 , R 2 represent independently 1C-4C hydrocarbon groups, and R 3 represents a 2C-4C hydrocarbon group. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：提供一种作为水果香料的香料组合物，其具有通常不知道的新鲜树，花或叶的特征，并且能够将混合香料的气味改变成抛光的一种同时与各种香水混合。解决方案：该香料组合物含有由通式（I）表示的化合物，其中R 1和R 2独立地代表C 1 -C 4烃基， SP> 3 表示2C-4C烃基。版权所有（C）2009，JPO＆INPIT

8. 发明专利

JP2008179603A Method for purifying acetal compound 有权
标题翻译：净化乙醇化合物的方法
公开(公告)号：JP2008179603A
公开(公告)日：2008-08-07
申请号：JP2007277386
申请日：2007-10-25
申请人： Kao Corp , 花王株式会社
发明人： KOTACHI SHINJI , FUKUDA KAZUYUKI
IPC分类号： C07D319/06 , A61K8/49 , A61Q13/00 , C11B9/00
CPC分类号： C07D319/06 , C11B9/0034
摘要： PROBLEM TO BE SOLVED: To provide a method for producing and purifying an acetal compound having floral flavor with sweetness, through suppressing offensive odor emitting in distilling the acetal compound at a high temperature under a high vacuum, and to provide a fragrance composition containing the acetal compound.
SOLUTION: The method for purifying the acetal compound comprises a step of distilling a feedstock containing the acetal compound represented by general formula (I) (wherein, R
1 is H, methyl or ethyl; R
2 is n-propyl or i-propyl; R
3 is H, n-propyl or i-propyl) at 80-170°C in the presence of an antioxidant.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：待解决的问题：提供一种生产和纯化具有甜味的花香味的缩醛化合物的方法，通过抑制在高真空下蒸馏缩醛化合物时发出的恶臭，并提供香料组合物含有缩醛化合物。解决方案：用于纯化缩醛化合物的方法包括蒸馏含有由通式（I）表示的缩醛化合物的原料（其中R 1为H，甲基或乙基; R 在抗氧化剂存在下，在80-170℃下， 2 是正丙基或异丙基; R 3是H，正丙基或异丙基。版权所有（C）2008，JPO＆INPIT

9. 发明专利

JP2008001667A Alcohol-based compound 有权
标题翻译：基于酒精的化合物
公开(公告)号：JP2008001667A
公开(公告)日：2008-01-10
申请号：JP2006174994
申请日：2006-06-26
申请人： Kao Corp , 花王株式会社
发明人： KOTACHI SHINJI , TANAKA SHIGEYOSHI , ONO SATORU
IPC分类号： C07C31/135 , A61K8/34 , A61Q13/00 , C07B61/00 , C07C29/17
CPC分类号： C07C33/14 , A61K8/34 , A61Q13/00 , C11B9/0034
摘要： PROBLEM TO BE SOLVED: To provide an alcohol-based compound having a natural aroma of Convallaria keiskei and almost without having a woody aroma which limits the utilization as a formulated aromatizing agent material, and a method for producing the same.
SOLUTION: This alcohol-based compound is expressed by general formula (I) [wherein, R
1 is H or a 1-4C hydrocarbon group; and any one of broken lines is a double bond and remaining 3 positions are each a single bond].
COPYRIGHT: (C)2008,JPO&INPIT

10. 发明专利

JP2006104192A Preparation method of salicylic ester 审中-公开
标题翻译：油菜籽的制备方法
公开(公告)号：JP2006104192A
公开(公告)日：2006-04-20
申请号：JP2005256816
申请日：2005-09-05
申请人： Kao Corp , 花王株式会社
发明人： TANAKA SHIGEYOSHI , UEHARA TAKEFUMI , ONO SATORU , KOTACHI SHINJI
IPC分类号： C07C67/03 , C07B61/00 , C07C69/94 , C11B9/00
摘要： PROBLEM TO BE SOLVED: To provide a novel preparation method which prepares a salicylic ester in a high yield, does not cause such a problem in handling as the occurrence of deposition in a distillation residue after reaction, and enables the reutilization of a catalyst used.
SOLUTION: In the method for preparing a salicylic ester for a perfume, a lower alkyl ester of salicylic acid is subjected to transesterification with an alcohol of which at least one carbon atom adjacent to a carbon atom having a hydroxy group has at least one hydrogen atom.
COPYRIGHT: (C)2006,JPO&NCIPI

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