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    • 3. 发明申请
    • METHOD AND APPARATUS FOR PREPARATION OF GRANULAR POLYSILICON
    • 用于制备颗粒聚硅氧烷的方法和装置
    • WO2008018760A1
    • 2008-02-14
    • PCT/KR2007/003827
    • 2007-08-09
    • KOREA RESEARCH INSTITUTE OF CHEMICAL TECHNOLOGYKIM, Hee YoungYOON, Kyung KooPARK, Yong KiCHOI, Won Choon
    • KIM, Hee YoungYOON, Kyung KooPARK, Yong KiCHOI, Won Choon
    • C30B29/06C30B25/00
    • C01B33/027C23C16/24C23C16/4401C23C16/442
    • A process for preparing granular polysilicon using a fluidized bed reactor is disclosed. The upper and lower spaces of the bed are defined as a reaction zone and a heating zone, respectively, with the height of the reaction gas outlet being selected as the reference height. The invention maximizes the reactor productivity by sufficiently providing the heat required and stably maintaining the reaction temperature in the reaction zone, without impairing the mechanical stability of the fluidized bed reactor. This is achieved through electrical resistance heating in the heating zone where an internal heater is installed in a space in between the reaction gas supplying means and the inner wall of the reactor tube, thereby heating the fluidizing gas and the silicon particles in the heating zone. The heat generated in the heating zone is transferred to the reaction zone by supplying the fluidizing gas at such a rate that the silicon particles can be intermixed between the reaction zone and the heating zone in a continuous, fluidized state.
    • 公开了一种使用流化床反应器制备颗粒状多晶硅的方法。 床的上部和下部空间分别被定义为反应区和加热区,反应气体出口的高度被选为参考高度。 本发明通过充分提供所需的热量并稳定地维持反应区域中的反应温度,而不损害流化床反应器的机械稳定性,使反应器生产率最大化。 这是通过加热区域中的电阻加热来实现的,其中内部加热器安装在反应气体供给装置和反应器管的内壁之间的空间中,从而加热流化气体和加热区域中的硅颗粒。 通过以使得硅颗粒能够以连续流化状态在反应区和加热区之间混合的速率供给流化气体,将加热区中产生的热转移到反应区。