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1. 发明申请

US20140112860A1 SEPARATION OF TELLURIUM BY SOLVENT EXTRACTION METHOD 有权
标题翻译：通过溶剂萃取法分离细菌
公开(公告)号：US20140112860A1
公开(公告)日：2014-04-24
申请号：US13922380
申请日：2013-06-20
申请人： Recytec. Inc. , Korea Institute of Science and Technology
发明人： Hwa Young LEE , Joong Kee LEE , Jae Gyu JEE , Joon Chul CHOI
IPC分类号： C01B19/00
CPC分类号： C01B19/001 , C01B19/00 , Y02P20/129
摘要： A method for separating tellurium includes separating and recovering tellurium (Te) from a dissolved solution containing the tellurium using a solvent extraction by an extractant, which contains one selected from a group consisting of tributyl phosphate (TBP), tris(2-ethylhexyl) phosphate (TEHP) and a combination thereof. The method may separate and recover the tellurium as a high-priced metallic element from a material, such as a Bi2Te3-based waste thermoelectric material, which contains not only the tellurium but also other metallic elements, simply and economically using a solvent extraction, whereby the tellurium with high yield and high purity can be separated, recovered and recycled.
摘要翻译：用于分离碲的方法包括使用萃取剂的溶剂萃取从含有碲的溶解溶液中分离和回收碲（Te），所述萃取剂含有选自磷酸三丁酯（TBP），磷酸三（2-乙基己基）酯（TEHP）及其组合。该方法可以从诸如基于Bi2Te3的废热电材料的材料中分离和回收作为高价金属元素的碲，其不仅包含碲而且还包含其它金属元素，简单且经济地使用溶剂萃取，由此具有高产率和高纯度的碲可以分离，回收和再循环。

2. 发明申请

US20150151966A1 SEPARATION METHOD OF TELLURIUM AND SELENIUM, AND PREPARATION METHOD OF TELLURIUM USING THE SAME 审中-公开
标题翻译：碲和硒的分离方法及使用其的氧化锆的制备方法
公开(公告)号：US20150151966A1
公开(公告)日：2015-06-04
申请号：US14541799
申请日：2014-11-14
申请人： KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY , RECYTEC INC.
发明人： Hwa Young LEE , Joong Kee LEE , Jae Gyu JEE , Joon Chul CHOI
IPC分类号： C01B19/00 , C07C51/42
CPC分类号： C01B19/001 , C01B19/005 , C07C51/412 , C07C51/48 , Y02P20/129 , C07C55/07
摘要： The present invention relates to a method of separating tellurium (Te) and selenium (Se) by using a neutral extractant (for example, either one of TBP and TEHP, or in combination thereof) from a dissolved solution of tellurium, such as a waste thermoelectric material. When tellurium and selenium are separated by using the method of this invention from a dissolved solution in which a Bi2Te3-based waste thermoelectric material is dissolved, a recovery rate of 97% or more and a separation factor of 400 or more for tellurium may be achieved, and therefore, tellurium and selenium may be separated in a very effective and economic manner as compared to conventional methods. Further, the present invention is characterized in that environmental pollution issues may be significantly reduced as compared with conventional methods carried out in a strong acidic solution since the present separation and extraction is conducted under a relative weak acid atmosphere in a pH range of 1.0 to 1.5.
摘要翻译：本发明涉及通过使用中和提取剂（例如，TBP和TEHP中的任一种或其组合）从碲的溶解溶液（例如废物）分离碲（Te）和硒（Se）的方法热电材料。当使用本发明的方法从溶解有Bi 2 Te 3的废热电材料的溶解溶液中分离碲和硒时，可以实现97％以上的回收率和碲的分离系数为400以上。因此，与常规方法相比，碲和硒可以以非常有效和经济的方式分离。此外，本发明的特征在于，与在强酸性溶液中进行的常规方法相比，可以显着降低环境污染问题，因为在1.0至1.5的pH范围内的相对弱酸性气氛下进行本分离和萃取。

3. 发明申请

US20150016024A1 CATHODE ACTIVE MATERIAL HAVING CORE-SHELL STRUCTURE AND PRODUCING METHOD THEREOF 审中-公开
标题翻译：具有核壳结构的阴极活性材料及其制备方法
公开(公告)号：US20150016024A1
公开(公告)日：2015-01-15
申请号：US14031239
申请日：2013-09-19
申请人： KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
发明人： Won Chang CHOI , Ji Hun PARK , Martin HALIM , Joong Kee LEE , Jung Sub KIM , Kyu-Ha LEE , Bong Jo KANG , A Young KIM , Hun Gi JUNG , Yu Jin CHAE , Joo Man WOO , Yong-Ho LEE , Tae Yong KIM
IPC分类号： H01G11/50 , H01G11/62 , H01G11/86 , H01G11/04
CPC分类号： H01G11/50 , H01G11/04 , H01G11/06 , H01G11/86 , Y02E60/13
摘要： Disclosed is a cathode active material having a core-shell structure. The core-shell cathode active material includes a core including a lithium transition metal oxide with excellent electrochemical properties and a shell formed by coating the surface of the core with a transition metal oxide. The formation of the shell by coating a transition metal oxide on the surface of the core comprising a lithium transition metal oxide prevents the structure of the lithium transition metal oxide from collapsing and inhibits the dissolution of manganese ions, enabling the fabrication of a hybrid capacitor with improved energy density and rate characteristics. Also disclosed is a method for producing the cathode active material.
摘要翻译：公开了具有核 - 壳结构的阴极活性材料。核 - 壳阴极活性材料包括具有优异的电化学性质的锂过渡金属氧化物的核和通过用过渡金属氧化物涂覆芯的表面形成的壳。通过在包含锂过渡金属氧化物的芯的表面上涂覆过渡金属氧化物来形成壳防止锂过渡金属氧化物的结构塌陷并抑制锰离子的溶解，使得能够制造具有改善能量密度和速率特征。还公开了一种用于制造正极活性物质的方法。

4. 发明申请

US20140349177A1 MAGNESIUM HYBRID BATTERY AND ITS FABRICATION METHOD 审中-公开
标题翻译：镁混合电池及其制造方法
公开(公告)号：US20140349177A1
公开(公告)日：2014-11-27
申请号：US14016549
申请日：2013-09-03
申请人： KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
发明人： Kyung Yoon CHUNG , Byung Won CHO , Joong Kee LEE , Hyung Sun KIM , Jae Hyun CHO , Won Young CHANG , Hwa Young LEE
IPC分类号： H01M10/0568 , H01M10/058 , H01M4/58 , H01M10/054 , H01M10/052
CPC分类号： H01M10/0568 , H01M4/381 , H01M4/466 , H01M10/052 , H01M10/054 , H01M10/058 , H01M2300/0025 , Y10T29/49108
摘要： The present disclosure relates to a magnesium hybrid battery and a method for fabricating same. The magnesium hybrid battery according to the present disclosure, which includes magnesium or magnesium alloy metal as an anode, a cathode including a cathode active material wherein not only magnesium ion but also one or more ion selected from lithium ion and sodium ion can be intercalated and deintercalated and an electrolyte including magnesium ion and further including one or more ion selected from lithium ion and sodium, can overcome the limitation of the existing magnesium secondary battery and provide improved battery capacity, output characteristics, cycle life, safety, etc.
摘要翻译：本发明涉及镁混合电池及其制造方法。根据本公开的镁混合电池，其包括镁或镁合金金属作为阳极，阴极包括正极活性材料，其中不仅可以插入镁离子而且还可以插入一种或多种选自锂离子和钠离子的离子，脱嵌和包含镁离子的电解质，并且还包括一种或多种选自锂离子和钠的离子，可以克服现有镁二次电池的限制，并提供改进的电池容量，输出特性，循环寿命，安全性等。

5. 发明申请

US20140141324A1 ELECTROLYTE FOR MAGNESIUM SECONDARY BATTERY AND PREPARATION METHOD THEREOF 有权
标题翻译：用于镁二次电池的电解液及其制备方法
公开(公告)号：US20140141324A1
公开(公告)日：2014-05-22
申请号：US13870439
申请日：2013-04-25
申请人： KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
发明人： Kyung Yoon CHUNG , Byung Won CHO , Joong Kee LEE , Jae Hyun CHO , Sang Hoon LEE , Won Young CHANG
IPC分类号： H01M10/0567 , H01M10/054
CPC分类号： H01M10/0567 , H01M10/054 , H01M10/0568
摘要： Provided are an electrolyte for a magnesium secondary battery having improved ion conductivity and stability, and a method for preparing the same. The electrolyte for a magnesium secondary battery shows higher ion conductivity as compared to the electrolyte according to the related art, increases the dissociation degree of a magnesium halide electrolyte salt, and provides stable electrochemical characteristics. In addition, after determining the capacity, output characteristics and cycle life of the magnesium secondary battery including the electrolyte, the battery provides significantly higher discharge capacity after 100 cycles, as compared to the electrolyte according to the related art. Therefore, the electrolyte may be useful for an electrolyte solution of a magnesium secondary battery.
摘要翻译：提供一种具有改善的离子传导性和稳定性的用于镁二次电池的电解质及其制备方法。与现有技术的电解液相比，镁二次电池用电解液的离子传导性高，卤化镁电解质盐的解离度提高，电化学性能稳定。此外，在确定包括电解质的镁二次电池的容量，输出特性和循环寿命之后，与根据现有技术的电解液相比，电池在100次循环后提供显着更高的放电容量。因此，电解质可用于镁二次电池的电解液。

6. 发明申请

US20160028117A1 ELECTROLYTE FOR MAGNESIUM RECHARGEABLE BATTERY AND PREPARATION METHOD THEREOF 有权
标题翻译：用于镁可充电电池的电解液及其制备方法
公开(公告)号：US20160028117A1
公开(公告)日：2016-01-28
申请号：US14633807
申请日：2015-02-27
申请人： KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
发明人： Si Hyoung OH , Byung Won CHO , Kyung Yoon CHUNG , Joong Kee LEE , Won Young CHANG , Jae Hyun CHO , Junghoon HA
IPC分类号： H01M10/0567 , H01M10/0568 , H01M10/054
CPC分类号： H01M10/0567 , H01M10/054 , H01M10/0568 , H01M10/0569 , H01M2300/0025
摘要： Disclosed is an electrolyte solution for a magnesium rechargeable battery with a high ionic conductivity and a wide electrochemical window compared to the conventional electrolyte solution. The electrolyte solution is prepared by dissolving magnesium metal into the ethereal solution using combinations of metal chloride catalysts. The electrolyte solution can be applied to fabricate magnesium rechargeable batteries and magnesium hybrid batteries with a markedly increased reversible capacity, rate capability, and cycle life compared to those batteries employing the conventional electrolyte solution. Also disclosed is a method for preparing the electrolyte.
摘要翻译：公开了与常规电解质溶液相比，具有高离子电导率和宽电化学窗口的镁可充电电池的电解液。通过使用金属氯化物催化剂的组合将镁金属溶解在醚溶液中来制备电解质溶液。与使用常规电解质溶液的电池相比，电解质溶液可用于制造镁可充电电池和镁混合电池，其具有显着增加的可逆容量，速率能力和循环寿命。还公开了一种制备电解质的方法。

7. 发明申请

US20140219891A1 SEPARATION METHOD OF ZIRCONIUM AND HAFNIUM BY SOLVENT EXTRACTION PROCESS 失效
标题翻译：通过溶剂萃取方法分离锆和铪的方法
公开(公告)号：US20140219891A1
公开(公告)日：2014-08-07
申请号：US13852143
申请日：2013-03-28
申请人： KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY , POSCO M-TECH
发明人： Hwa Young LEE , Byung Won CHO , Joong Kee LEE
IPC分类号： C22B3/26
CPC分类号： C22B3/0005 , Y02P10/234
摘要： A separation method of zirconium and hafnium is described which includes an extraction process of agitating an undiluted aqueous solution containing zirconium, hafnium, and sulfuric acid with a first stirring solution containing an acidic extractant to produce a first extract solution in which the hafnium is extracted by the acidic extractant; and a recovery process of agitating the first extract solution with a second stirring solution containing a citric acid solution to produce a citric acid solution after extraction in which zirconium is reverse-extracted from the first extract solution to the citric acid solution so as to recover zirconium contained in the first extract solution. The method may reduce the amount of extractant while greatly enhancing the separation effect of zirconium and hafnium, and increase zirconium recovery rate by more than 97% through an additional zirconium recovery process while reducing a hafnium content in zirconium by less than 50 ppm.
摘要翻译：描述了锆和铪的分离方法，其包括使用含有酸性萃取剂的第一搅拌溶液搅拌未稀释的含有锆，铪和硫酸的水溶液的提取方法，以产生其中铪被提取的第一提取溶液酸性提取剂; 以及回收方法，用含有柠檬酸溶液的第二搅拌溶液搅拌第一提取溶液，以在提取后产生柠檬酸溶液，其中将锆从第一提取溶液反萃取至柠檬酸溶液，以回收锆包含在第一提取物溶液中。该方法可以减少萃取剂的量，同时大大提高锆和铪的分离效果，并且通过另外的锆回收方法将锆回收率提高97％以上，同时将锆中的铪含量降低到低于50ppm。

8. 发明申请

US20140097094A1 RECOVERY METHOD OF NICKEL FROM SPENT ELECTROLESS NICKEL PLATING SOLUTIONS BY ELECTROLYSIS 有权
标题翻译：通过电解法从电极电镀镍溶液中回收镍的方法
公开(公告)号：US20140097094A1
公开(公告)日：2014-04-10
申请号：US13670869
申请日：2012-11-07
申请人： KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
发明人： Hwa Young LEE , Byung Won CHO , Joong Kee LEE
IPC分类号： C25C1/08
CPC分类号： C25C1/08 , C23C18/1617 , C23C18/32
摘要： A recovery method of nickel according to the present invention comprises pretreatment step to prepare a solution for electrolysis by adding hexanesulfonate salt to a treatment solution including nickel, and nickel recovery step to recover nickel in a metal form by electrolysis of the above solution for electrolysis. The present invention can produce nickel in high purity with simple process with low cost, and can recover and reproduce nickel in a metal form with at least 99.5% of high purity and at least 90% of recovery rate.
摘要翻译：根据本发明的镍的回收方法包括预处理步骤，通过向包含镍的处理溶液中加入己磺酸盐来制备电解溶液，以及镍回收步骤，通过电解上述电解溶液来回收金属形式的镍。本发明可以以低成本的简单工艺生产高纯度的镍，并且可以以至少99.5％的高纯度和至少90％的回收率回收和再现金属形式的镍。

9. 发明申请

US20130136996A1 ASYMMETRIC HYBRID LITHIUM SECONDARY BATTERY HAVING BUNDLE TYPE SILICON NANO-ROD 审中-公开
标题翻译：不对称混合锂离子二次电池
公开(公告)号：US20130136996A1
公开(公告)日：2013-05-30
申请号：US13681560
申请日：2012-11-20
申请人： Korea Institute of Science and Technology
发明人： Joong Kee LEE , Byung Won CHO , Hwa Young LEE , Byoung Sung AHN , Joo Man WOO , Sang Ok KIM , Ji Hun PARK , Jung Sub KIM , Nguyen Si HIEU
IPC分类号： H01M4/38 , H01M4/04 , H01M4/583
CPC分类号： H01M4/386 , B82Y30/00 , H01M4/04 , H01M4/0428 , H01M4/049 , H01M4/134 , H01M4/1395 , H01M4/405 , H01M4/583
摘要： Disclosed are a metallic nano-structure material in which an energy storage capacity based on electrochemical reaction with lithium is improved by 10 times or more compared to a conventional graphite material and power characteristics are excellent, an electrode composed of the metallic nano-structure material, and a lithium ion asymmetric secondary battery including the electrode as an anode. When using the electrode for the lithium ion asymmetric secondary battery, energy larger than with the graphite material can be stored with very thin thickness due to the high-capacity feature of the metallic material and the high-power feature can be achieved by the nano structure, such that energy density can be innovatively improved in the same weight condition when compared to a conventional lithium ion capacitor, and the lithium ion asymmetric secondary battery including the electrode can be used for renewable energy storage, ubiquitous power supply, heavy machinery, vehicle power source, etc.
摘要翻译：公开了一种金属纳米结构材料，其中与常规石墨材料相比，基于与锂的电化学反应的能量存储容量提高10倍以上，功率特性优异，由金属纳米结构材料构成的电极，以及包含该电极作为阳极的锂离子不对称二次电池。当使用电极作为锂离子不对称二次电池时，由于金属材料的高容量特性，能够比石墨材料大的能量可以非常薄的厚度储存，并且可通过纳米结构实现高功率特征与以往的锂离子电容器相比，能够在与重量相同的条件下进行能量密度的创新改善，并且包含电极的锂离子不对称二次电池可用于可再生能源储存，普遍存在的电力供应，重型机械，车辆动力来源等

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