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1. 发明专利

JPS58140045A LIQUID CRYSTAL COMPOUND, LIQUID CRYSTAL COMPOSITION AND LIQUID CRYSTAL DISPLAY ELEMENT 失效
公开(公告)号：JPS58140045A
公开(公告)日：1983-08-19
申请号：JP2108382
申请日：1982-02-15
申请人： KANTO KAGAKU , HITACHI LTD
发明人： FUJII TSUNENORI , SUZUKI KENJI , YOSHIDA MASAHIRO , OOKAWA HISASHI , KOTOU KAORU , OOMORI HIDEKI , YOKOKURA HISAO , OKABE YOSHIAKI , HATSUTORI SHINTAROU , KITAMURA TERUO , KOUBI AKIO , SATOU MIKIO
IPC分类号： C07C69/753 , C07C69/76 , C07C69/773 , C09K19/12 , C09K19/20 , C09K19/30 , C09K19/46 , C09K19/54 , G02F1/13
摘要： NEW MATERIAL:The liquid crystal compound of formulaI(R and R' are alkyl; X, X', Y and Y' are a group of formula II or formula III). EXAMPLE:(trans-4-Propylcyclohexyl)phenyl 4'-propylbiphenyl-4''-carboxylate. USE:A component of a liquid crystal composition. In improves especially an upper limit of the liquid crystal temperature range remarkably without too much increasing the viscosity of the composition, and improves the response of the liquid crystal display element. PROCESS:The compound of formulaIcan be prepared by the esterification of an acid chloride with an alcohol according to the reaction formula.

2. 发明专利

JPS58134052A LIQUID CRYSTAL COMPOUND AND LIQUID CRYSTAL COMPOSITION 失效
公开(公告)号：JPS58134052A
公开(公告)日：1983-08-10
申请号：JP1487382
申请日：1982-02-03
申请人： KANTO KAGAKU , HITACHI LTD
发明人： FUJII TSUNENORI , KOTOU KAORU , SUZUKI KENJI , YOSHIDA MASAHIRO , OOKAWA HISASHI , HIRAI YOUICHI , YOKOKURA HISAO , OKABE YOSHIAKI , HATSUTORI SHINTAROU , KITAMURA TERUO , KOUBI AKIO , SATOU MIKIO
IPC分类号： C07C69/76 , C07C69/757 , C07C69/773 , C09K19/12 , C09K19/20 , C09K19/30 , C09K19/46 , G02F1/13 , G09F9/00 , G09F9/35
摘要： NEW MATERIAL:A compound shown by the formulaI(R and R are alkyl; X -X are residues shown by the formula II and formula III). EXAMPLE:4-n-methoxymethyl-4''(propylphenyl)4'-cycloheyxylphenyl-carbox ylate. USE:A colorless and low-viscosity liquid crystal substance having a wide liquid crystal temperature range and improved chemical stability, capable of being blended with all types of liquid crystals, applicable by all display methods of liquid crystal. PROCESS:A compound shown by the formula X X COOH is reduced into a corresponding alcohol, which is esterified to give a compound shown by the formula X X CH2OR . This compound is acetylated to give a compound shown by the formula CH3OCX X CH2OR , which is hydrolyzed to give a compound shown by the formula HOOCX X CH2OR . This compound is halogenated to give ClOCX X CH2OR , which is reacted with a compound shown by the formula HOX R to give a compound shown by the formulaI.

3. 发明专利

JPS588782A COLORLESS LIQUID CRYSTAL MATERIAL, COLORLESS LIQUID CRYSTAL COMPOSITION AND LIQUID CRYSTAL DISPLAY ELEMENT 失效
公开(公告)号：JPS588782A
公开(公告)日：1983-01-18
申请号：JP10707481
申请日：1981-07-10
申请人： KANTO KAGAKU , HITACHI LTD
发明人： HIRAI YOUICHI , FUJII TSUNENORI , KOTOU KAORU , SUZUKI KENJI , YOSHIDA MASAHIRO , OOKAWA HISASHI , OKABE YOSHIAKI , KITAMURA TERUO , YOKOKURA HISAO , HATSUTORI SHINTAROU , KOUBI AKIO , SATOU MIKIO
IPC分类号： C07C69/75 , C09K19/30 , C09K19/46 , G02F1/13 , G09F9/00 , G09F9/35
摘要： PURPOSE:A colorless liquid crystal material with a liquid crystal temp. range capable of being extended to a low-temp. region, comprising a 4-alkyloxymethylphenyl-4'-alkylcyclohexylcarboxylate. CONSTITUTION:A 4-alkyloxymethylphenyl-4'alkylcyclohexyl-carboxylate is used as a colorless liquid crystal material. Said material is desirably a material of the formula (wherein m and n are each 1-8). It is possible to use the material as a component of a colorless liquid crystal composition. It is possible to constitute a liquid crystal display element by supporting as a liquid crystal layer the colorless liquid crystal composition between two base electrodes opposed to each other and to apply the display element to an optical instrument in which the liquid crystal layer is optically modulated by applying a voltage between said base electrodes. The liquid crystal display element is effective for a variety of display systems such as a phase transition type or guest/host type, not to speak of a TN type.

4. 发明专利

JPS5936634A Liquid crystal compound 失效
标题翻译：液晶化合物
公开(公告)号：JPS5936634A
公开(公告)日：1984-02-28
申请号：JP14665982
申请日：1982-08-23
申请人： Hitachi Ltd , Kanto Kagaku Kk
发明人： HIRAI YOUICHI , FUJII TSUNENORI , KOTOU KAORU , SUZUKI KENJI , YOSHIDA MASAHIRO , OOKAWA HISASHI , OKABE YOSHIAKI , KITAMURA TERUO , YOKOKURA HISAO , HATSUTORI SHINTAROU , KOUBI AKIO , SATOU MIKIO
IPC分类号： C07C43/164 , C07C41/00 , C07C43/168 , C07C43/205 , C07C67/00 , C09K19/30 , G02F1/13 , G09F9/00
摘要： NEW MATERIAL:A compound expressed by formula I (R
1 and R
2 are alkyl; n is 0, 1 or 2).
EXAMPLE: The compound expressed by formula II.
USE: A component for liquid crystal compositions capable of extending the liquid crystal temperature, reducing the viscosity and improving the operating temperature range and response characteristics of liquid crystal display elements.
PROCESS: A solution of a compound expressed by formula III in ethanol is prepared, and a small amount of Na [BH
4 ] is added to the resultant solution under cooling with ice and stirring. Acetic acid is then added thereto to produce a compound expressed by formula IV, which is then reacted with SOCl
2 to give a compound expressed by formula V. Sodium is dissolved in propyl alcohol, and a solution of the compound expressed by formula V in dimethylformamide is added to the resultant solution and reacted under heating to obtain the compound expressed by formula I , e.g. the compound expressed by formula II.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：新材料：由式I表示的化合物（R1和R2是烷基; n是0,1或2）。实施例：由式II表示的化合物。用途：能够延长液晶温度，降低粘度，提高液晶显示元件的工作温度范围和响应特性的液晶组合物成分。方法：制备由式III表示的化合物在乙醇中的溶液，并在冰冷却并搅拌下向所得溶液中加入少量Na [BH4]。然后向其中加入乙酸以产生由式IV表示的化合物，然后与SOCl 2反应，得到式V表示的化合物。将钠溶于丙醇中，将式V化合物在二甲基甲酰胺中的溶液为加入到所得溶液中并加热反应，得到由式I表示的化合物，例如由式II表示的化合物。

5. 发明专利

JPS58134051A LIQUID CRYSTAL COMPOUND, LIQUID CRYSTAL COMPOSITION, AND DISPLAY ELEMENT OF LIQUID CRYSTAL 失效
公开(公告)号：JPS58134051A
公开(公告)日：1983-08-10
申请号：JP1487482
申请日：1982-02-03
申请人： KANTO KAGAKU , HITACHI LTD
发明人： FUJII TSUNENORI , SUZUKI KENJI , YOSHIDA MASAHIRO , OOKAWA HISASHI , KOTOU KAORU , HIRAI YOUICHI , OKABE YOSHIAKI , YOKOKURA HISAO , HATSUTORI SHINTAROU , KITAMURA TERUO , KOUBI AKIO , SATOU MIKIO
IPC分类号： C09K19/32 , C07C69/753 , C09K19/46 , G02F1/13 , G09F9/00 , G09F9/35
摘要： NEW MATERIAL:A compound shown by the formulaI(R and R are alkyl; n is integer of 1-6). EXAMPLE:4-(alpha-Propoxymethyl)phenyl-4'-pentylbicyclo(2,2,2) oetanecarboxylate. USE:A low-viscosity and colorless liquid crystal substance useful for preparing a display element of liquid crystal capable of being operated in a wide temperature range and having improved response properties, having a wide phase transition temperature. PROCESS:A compound shown by the formula R CH2COCH3 is condensed with cyanoethylene to give a compound shown by the formula II. The CN of the compound is hydrolyzed into COOH with an alkali, and the resulting compound is heated in acetic anhydride to give a compound shown by the formula III. This compound is heated in the presence of an alkali, to give a compound shown by the formula IV. This compond is reduced with hydrazine, treated with phosphorus oxybromide, treated with formic acid in an acidic medium, and treated with thionyl chloride successively, to give a compound shown by the formula V. This compound is further esterified with a compound shown by the formula VI, to give a compound shown by the formulaI.

6. 发明专利

JPS5885842A COLORLESS LIQUID CRYSTAL SUBSTANCE 失效
公开(公告)号：JPS5885842A
公开(公告)日：1983-05-23
申请号：JP18376481
申请日：1981-11-18
申请人： KANTO KAGAKU , HITACHI LTD
发明人： FUJII TSUNENORI , SUZUKI KENJI , YOSHIDA MASAHIRO , OOKAWA HISASHI , KOTOU KAORU , HIRAI YOUICHI , OKABE YOSHIAKI , YOKOKURA HISAO , HATSUTORI SHINTAROU , KITAMURA TERUO , KOUBI AKIO , SATOU MIKIO
IPC分类号： C07C69/753 , C07C69/773 , C09K19/20 , C09K19/30 , C09K19/46 , G02F1/13 , G09F9/00
摘要： NEW MATERIAL:A compound of formulaI(R and R' are

7. 发明专利

JPS57140737A COLORLESS LIQUID CRYSTAL SUBSTANCE, COLORLESS LIQUID CRYSTAL COMPOSITION, AND DISPLAY ELEMENT OF LIQUID CRYSTAL 失效
公开(公告)号：JPS57140737A
公开(公告)日：1982-08-31
申请号：JP2550281
申请日：1981-02-25
申请人： KANTO KAGAKU , HITACHI LTD
发明人： HIRAI YOUICHI , FUJII TSUNENORI , KOTOU KAORU , SUZUKI KENJI , YOSHIDA MASAHIRO , OOKAWA HISASHI , KITAMURA TERUO , YOKOKURA HISAO , OKABE YOSHIAKI , HATSUTORI SHINTAROU , KOUBI AKIO , SATOU MIKIO
IPC分类号： C07C43/14 , C07C41/00 , C07C43/164 , C07C43/168 , C07C43/20 , C07C67/00 , C07C255/54 , C07D239/26 , C09K19/12 , C09K19/30 , C09K19/34 , C09K19/44 , G02F1/13 , G09F9/00 , G09F9/35
摘要： NEW MATERIAL:A colorless liquid crystal substance represented by the compound shown by the formula R1-A-B-R2[R1 is -(CH2O)nCmH2m+1(n is 1-4; m is 1-8) or -(CH2)OCmH2m+1, etc.; R2 is alkyl, alkoxyalkoxy-carbonyl, etc.; A and B are groups shown by the formulasI, II, III, etc.]or shown by the formula R1-A-X-B-R2 (X is -COO-, -OCO-, -CH=CH-, etc.), having a 6-membered ring having one or more carbon atoms wherein one carbon atom is linked through a methylene group to a noncyclic terminal alkoxy group. USE:A display element of liquid crystal. Having a wide range of liquid crystal temperature, colorless. PROCESS:For example, a compound shown by the formula IV is reacted with lithium aluminum hydride, and with diluted hydrochloric acid, to give a compound shown by the formula V. This compound is reacted with thionyl chloride, and with n-propyl sodium alcolate, to give a compound shown by the formula VI.

8. 发明专利

JPS5885825A COLORLESS LIQUID CRYSTAL SUBSTANCE, LIQUID CRYSTAL COMPOSITION AND LIQUID CRYSTAL DISPLAY ELEMENT 失效
公开(公告)号：JPS5885825A
公开(公告)日：1983-05-23
申请号：JP18376381
申请日：1981-11-18
申请人： KANTO KAGAKU , HITACHI LTD
发明人： FUJII TSUNENORI , SUZUKI KENJI , YOSHIDA MASAHIRO , OOKAWA HISASHI , KOTOU KAORU , HIRAI YOUICHI , OKABE YOSHIAKI , YOKOKURA HISAO , HATSUTORI SHINTAROU , KITAMURA TERUO , KOUBI AKIO , SATOU MIKIO
IPC分类号： C07C69/75 , C07C2/00 , C07C13/28 , C07C43/168 , C07C69/76 , C09K19/30 , C09K19/46 , G02F1/13 , G09F9/00 , G09F9/35
摘要： NEW MATERIAL:A compound of formulaI(R and R' are

9. 发明专利

JPS59182880A Liquid crystal composition 失效
标题翻译：液晶组合物
公开(公告)号：JPS59182880A
公开(公告)日：1984-10-17
申请号：JP5832483
申请日：1983-04-01
申请人： Hitachi Ltd , Mitsubishi Chem Ind Ltd
发明人： IMAZEKI SHIYUUJI , KOUBI AKIO , SATOU MIKIO , KANEKO MASAHARU , OZAWA TETSUO , YONEYAMA TOMIO
IPC分类号： C09K19/60 , C09B1/02 , C09B1/14 , C09B1/22 , C09B1/503 , C09B1/54 , C09B1/56 , C09B6/00 , G02F1/137 , G09F9/00
摘要： PURPOSE: To obtain a liquid crystal composition capable of providing a clear display having high contrast using a polychromatic dye having excellent order- parameter, solubility, and stability to light, heat and electricity, by using an anthraquinone dye of a specific formula as a component.
CONSTITUTION: The objective liquid crystal composition contains the anthraquinone dye of formula I {R
1 is group of formula II (R
2 is H or cycloalkyl which may be substituted with 1W18C alkyl, 1W18C alkoxy, etc.) or group of formula III [R
3 is H, 1W18C alkyl which may be substituted with alkoxy, 1W18C alkoxy, group of formula IV (R
4 is H, 1W18C alkyl which may be substituted with alkoxy, etc.), halogen, cyano or dialkylamino]; Y
1 WY
4 are H, amino, hydroxy, -O-R
5 , or -NHR
5 (R
5 is alkoxyl, allyl, cycloalkyl, alkyl which may be substituted with furfuryl, etc.); Z is H, halogen, alkyl which may be substituted with alkoxy, -O-R
1 , -S-R
1 , etc.; X is -CH
2 -, O or S}.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：通过使用具有特定的式的蒽醌染料作为组分，获得能够提供具有高对比度的清晰显示的液晶组合物，该多色染料具有优异的参数，溶解度和对光，热和电的稳定性。构成：目标液晶组合物含有式I的蒽醌染料（R 1为式II基团（R 2为H或可被1-18C烷基，1-18C烷氧基等取代的环烷基））或式III的基团[R 3是H，可以被烷氧基取代的1-18C烷基，1-18C烷氧基，式IV基团（R 4是H，可被取代的1-18C烷基）与烷氧基等），卤素，氰基或二烷基氨基]; Y 1 -Y 4是H，氨基，羟基，-OR 5或-NHR 5（R 5是烷氧基，烯丙基，环烷基，可被糠基取代的烷基等））; Z是H，卤素，可被烷氧基取代的烷基，-O-R 1，-S-R 1等; X是-CH 2 - ，O或S}。

10. 发明专利

JPS59182877A Guest-host liquid crystal composition 失效
标题翻译：顾客液体水晶组合物
公开(公告)号：JPS59182877A
公开(公告)日：1984-10-17
申请号：JP5832183
申请日：1983-04-01
申请人： Hitachi Ltd , Mitsubishi Chem Ind Ltd
发明人： IMAZEKI SHIYUUJI , KOUBI AKIO , SATOU MIKIO , KANEKO MASAHARU , OZAWA TETSUO , YONEYAMA TOMIO
IPC分类号： C09K19/60 , C09B69/00 , G02F1/137 , G09F9/00
摘要： PURPOSE: To provide a guest-host liquid crystal composition having excellent display contrast and stability, by dissolving a polychromatic dye containing a dye having trans-4-substituted-cyclohexyl group as a guest substance in a host liquid crystal constituting the matrix.
CONSTITUTION: The objective liquid crystal composition can be prepared by dissolving (A) a polychromatic dye containing a dye having preferably ≥70mol% of trans-4-substituted-cyclohexyl group (preferably anthraquinone dye, azo dye, azomethine dye, quinophthalone dye, perynone dye, thioindigo dye, naphthalimide dye or oxazine dye) in (B) a host liquid crystal constituting the matrix. The dye having trans-4-substituted-cyclohexyl group is preferably the one represented by formula I [W is trans-4-substituted-cyclohexyl; D is group of organic dye free of ionic group; B is -COX
1 - (X
1 is O, S, -CH
2 -, etc.), CH
2 X
1 -, or group of formula II(m is 1W3)].
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：提供具有优异的显示对比度和稳定性的客体主体液晶组合物，通过将含有反式-4-取代的环己基的染料的多色染料作为客体物质溶解在构成基质的主液晶中。构成：目的液晶组合物可以通过将（A）含有优选≥70mol％的反式-4-取代的环己基（优选蒽醌染料，偶氮染料，偶氮甲碱染料，喹酞酮染料，紫罗兰染料，萘二甲酰亚胺染料或恶嗪染料）（B）构成基质的主体液晶。具有反式-4-取代的环己基的染料优选为由式I表示的染料[W为反式-4-取代的环己基; D是不含离子基团的有机染料组; B是-COX 1 - （X 1是O，S，-CH 2 - 等），CH 2 X 1 - 或式II的基团（m是1-3）]。

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