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1. 发明授权

US5789557A Reactive azo dyes with a coupler of the aminonaphthalene series 失效
标题翻译：反应性偶氮染料与氨基萘系列的偶合剂
公开(公告)号：US5789557A
公开(公告)日：1998-08-04
申请号：US809292
申请日：1997-03-27
申请人： Jurgen Dornhagen , Heike Kilburg , Manfred Patsch , Hermann Loffler , Ortwin Schaffer
发明人： Jurgen Dornhagen , Heike Kilburg , Manfred Patsch , Hermann Loffler , Ortwin Schaffer
IPC分类号： C09B62/513 , C07C309/47 , C07C309/50 , C09B62/08 , C09B62/44 , C09B62/507 , D06P1/38
CPC分类号： C09B62/08 , C07C309/47 , C07C309/50 , C09B62/4411 , C09B62/507
摘要： Reactive dyes of the formula ##STR1## where n is 1 or 2, R.sup.1 is hydrogen or hydroxysulfonyl, R.sup.2 is hydrogen or hydroxyl, R.sup.3 is substituted C.sub.1 -C.sub.4 -alkyl, C.sub.5 -C.sub.7 -cycloalkyl or substituted phenyl, R.sup.4 is hydrogen or R.sup.3 and R.sup.4, together with the nitrogen atom linking them, form a heterocyclic radical and D is a radical of a diazo or tetrazo component, each having at least one mechanism, their use for dyeing or printing hydroxyl-containing or nitrogen-containing organic substrates, and novel aminonaphthalenes.
摘要翻译： PCT No.PCT / EP95 / 03687 371日期1997年3月27日 102（e）1997年3月27日PCT PCT 1995年9月19日PCT公布。出版物WO96 / 10610 日期：1996年4月11日，其中n为1或2，R 1为氢或羟基磺酰基，R 2为氢或羟基，R 3为取代的C 1 -C 4 - 烷基，C 5 -C 7 - 环烷基或取代的苯基， R4是氢或R3和R4与连接它们的氮原子一起形成杂环基，D是重氮或双偶氮组分的基团，它们各自具有至少一种机理，它们用于染色或印刷含羟基或氮含有机基质和新型氨基萘。

2. 发明授权

US5681937A Reactive azo dyes with a coupling component from the aminonaphthalenesulfonic acid series 失效
标题翻译：活性偶氮染料与氨基萘磺酸系的偶联组分
公开(公告)号：US5681937A
公开(公告)日：1997-10-28
申请号：US622588
申请日：1996-03-26
申请人： Manfred Patsch , Heike Kilburg , Andrea Zamponi
发明人： Manfred Patsch , Heike Kilburg , Andrea Zamponi
IPC分类号： C09B62/507 , C09B62/096 , D06P1/38
CPC分类号： C09B62/507
摘要： Reactive dyes of the formula ##STR1## where n is 1 or 2 R.sup.1 is hydrogen or hydroxyl and D is the radical of a diazo or tetrazo component with, in each case, at least one anchor radical of the formula SO.sub.2 --Y where Y is vinyl or substituted ethyl, and the use thereof for dyeing or printing organic substrates having hydroxyl groups or nitrogen atoms are described.
摘要翻译：其中n为1或2个R 1的式（I）的活性染料是氢或羟基，D是重氮或双偶氮组分的基团，在每种情况下，至少一个式SO 2 -Y的锚基团其中Y是乙烯基或取代的乙基，并且描述了其用于染色或印刷具有羟基或氮原子的有机底物的用途。

3. 发明授权

US5424461A Preparation of 1-amino-4-hydroxyanthraquinone 失效
标题翻译： 1-氨基-4-羟基蒽醌的制备
公开(公告)号：US5424461A
公开(公告)日：1995-06-13
申请号：US165464
申请日：1993-12-13
申请人： Erwin Hahn , Manfred Patsch , Heike Kilburg
发明人： Erwin Hahn , Manfred Patsch , Heike Kilburg
IPC分类号： C07C221/00 , C07C225/36 , C09B1/503
CPC分类号： C09B1/5035
摘要： A process for preparing 1-amino-4-hydroxyanthraquinone by treating 1,4-dihydroxyanthraquinone with ammonia in an aqueous medium comprises treating with ammonia in the presence of a base and of a catalytic amount of a reducing agent at from 60.degree. to 150.degree. C. and at from 1 to 30 bar.
摘要翻译：在水性介质中用氨处理1,4-二羟基蒽醌制备1-氨基-4-羟基蒽醌的方法包括在碱存在下用氨和催化量的还原剂在60〜150℃下处理和1至30巴。

4. 发明授权

US5264507A Azo dye polymers 失效
标题翻译：偶氮染料聚合物
公开(公告)号：US5264507A
公开(公告)日：1993-11-23
申请号：US949156
申请日：1992-09-23
申请人： Matthias Wiesenfeldt , Sabine Gruettner-Merten , Ruediger Sens , Karl-Heinz Etzbach , Heike Kilburg
发明人： Matthias Wiesenfeldt , Sabine Gruettner-Merten , Ruediger Sens , Karl-Heinz Etzbach , Heike Kilburg
IPC分类号： C08F20/34 , C08F220/34 , C08F246/00 , C09B69/10 , G02F1/361 , C08F228/06 , C08F220/18 , C08F226/02
CPC分类号： C08F220/34 , C08F20/34 , C08F246/00 , C09B69/106 , G02F1/3612 , G02F1/3614 , G02F1/3617
摘要： Azo dye polymers useful in nonlinear optics contain as characteristic monomer units radicals of the formulae I, II, III and IV ##STR1## where D is the radical of a heterocyclic diazo component,R.sup.1 and R.sup.2 are each hydrogen, C.sub.1 -C.sub.6 -alkyl or substituted or unsubstituted C.sub.1 -C.sub.6 -alkoxy, and R.sup.2 may also be C.sub.1 -C.sub.4 -alkanoylamino,R.sup.3 is hydrogen, C.sub.1 -C.sub.6 -alkyl, C.sub.5 -C.sub.7 -cycloalkyl or C.sub.3 -C.sub.4 -alkenyl,R.sup.4 is hydrogen, deuterium, methyl, trideuterated methyl or chlorine,R.sup.5 is hydrogen or deuterium,Y.sup.1 and Y.sup.2 are each substituted or unsubstituted C.sub.2 -C.sub.10 -alkylene,W is oxygen, imino or C.sub.1 -C.sub.4 -alkylimino, andX is hydroxyl, substituted or unsubstituted C.sub.1 -C.sub.6 -alkoxy, phenoxy, amino or mono- or di(C.sub.1 -C.sub.4 -alkyl)amino,and have an average molecular weight of from 1,000 to 100,000.
摘要翻译：可用于非线性光学的偶氮染料聚合物包含式I，II，III和IV的特征单体单元基团。其中D是式（I）杂环重氮组分的基团R 1和R 2各自为氢，C 1 -C 6烷基或取代或未取代的C 1 -C 6 - 烷氧基，R 2也可为C 1 -C 4 - 烷酰基氨基，R 3为氢，C 1 -C 6烷基 C 5 -C 7 - 环烷基或C 3 -C 4 - 烯基，R 4是氢，氘，甲基，三卤代甲基或氯，R 5是氢或氘，Y 1和Y 2各自是取代或未取代的C 2 -C 10亚烷基，W是氧，亚氨基或C1-C4烷基亚氨基，X是羟基，取代或未取代的C1-C6-烷氧基，苯氧基，氨基或单或二（C1-C4-烷基）氨基，平均分子量为1,000至100,000 。

5. 再颁专利

USRE35407E Azo dye polymers 失效
公开(公告)号：USRE35407E
公开(公告)日：1996-12-17
申请号：US223852
申请日：1994-04-06
申请人： Matthias Wiesenfeldt , Sabine Gruettner-Merten , Ruediger Sens , Karl-Heinz Etzbach , Heike Kilburg
发明人： Matthias Wiesenfeldt , Sabine Gruettner-Merten , Ruediger Sens , Karl-Heinz Etzbach , Heike Kilburg
IPC分类号： C08F20/34 , C08F220/34 , C08F246/00 , C09B69/10 , G02F1/361 , C08F228/06 , C08F212/06 , C08F220/18 , C08F226/02
CPC分类号： C08F220/34 , C08F20/34 , C08F246/00 , C09B69/106 , G02F1/3612 , G02F1/3614 , G02F1/3617
摘要： Azo dye polymers useful in nonlinear optics contain as characteristic monomer units radicals of the formulae I, II, III and IV ##STR1## where D is the radical of a heterocyclic diazo component,R.sup.1 and R.sup.2 are each hydrogen, C.sub.1 -C.sub.6 -alkyl or substituted or unsubstituted C.sub.1 -C.sub.6 -alkoxy, and R.sup.2 may also be C.sub.1 -C.sub.4 -alkanoylamino,R.sup.3 is hydrogen, C.sub.1 -C.sub.6 -alkyl, C.sub.5 -C.sub.7 -cycloalkyl or C.sub.3 -C.sub.4 -alkenyl,R.sup.4 is hydrogen, deuterium, methyl, trideuterated methyl or chlorine,R.sup.5 is hydrogen or deuterium,Y.sup.1 and Y.sup.2 are each substituted or unsubstituted C.sub.2 -C.sub.10 -alkylene,W is oxygen, imino or C.sub.1 -C.sub.4 -alkylimino, andX is hydroxyl, substituted or unsubstituted C.sub.1 -C.sub.6 -alkoxy, phenoxy, amino or mono- or di(C.sub.1 -C.sub.4 -alkyl)amino,and have an average molecular weight of from 1,000 to 100,000.

6. 发明授权

US5525743A Preparation of anthraquinone imide compounds 失效
标题翻译：蒽醌酰亚胺化合物的制备
公开(公告)号：US5525743A
公开(公告)日：1996-06-11
申请号：US328948
申请日：1994-10-21
申请人： Udo Bergmann , Helmut Hoch , Heike Kilburg , Reinhold Kohlhaupt , Matthias Niedenbrueck
发明人： Udo Bergmann , Helmut Hoch , Heike Kilburg , Reinhold Kohlhaupt , Matthias Niedenbrueck
IPC分类号： C09B1/32 , C07C221/00 , C07C225/34 , C09B1/48 , C09B3/10 , C09B3/12 , C09B3/48 , C09B1/00 , C07C103/76
CPC分类号： C07C221/00 , C07C225/34 , C07C2103/24 , C07C2103/40 , C07C2103/52 , C07C2103/54
摘要： The preparation of anthraquinone imide compounds by condensation of anthraquinone compounds containing at least one primary amino group with halogenized aromatics or by condensation of halogenized anthraquinone compounds with primary aromatic amines, in the presence of a vat-dyeing catalyst and an acid-binding agent in an organic solvent, in which the organic solvent used is an alkyl benzoate.
摘要翻译：通过将含有至少一个伯氨基的蒽醌化合物与卤化的芳族化合物缩合或通过卤化的蒽醌化合物与伯芳基胺的缩合，在还原染色催化剂和酸结合剂的存在下制备蒽醌酰亚胺化合物有机溶剂，其中所用的有机溶剂是苯甲酸烷基酯。

7. 发明授权

US5393645A Production of structured polymer layers having nonlinear optical properties 失效
标题翻译：具有非线性光学特性的结构化聚合物层的制备
公开(公告)号：US5393645A
公开(公告)日：1995-02-28
申请号：US167064
申请日：1993-12-16
申请人： Karl-Heinz Etzbach , Heike Kilburg , Hans-Joachim Lorkowski , Karl Pfeiffer
发明人： Karl-Heinz Etzbach , Heike Kilburg , Hans-Joachim Lorkowski , Karl Pfeiffer
IPC分类号： C08J3/28 , G02F1/35 , G02F1/355 , G02F1/361 , G03F7/027 , G03F7/40
CPC分类号： G02F1/3617 , G02F1/3611 , G02F1/3614 , G03F7/027 , G03F7/40
摘要： Structured polymer layers having nonlinear optical properties are produced by a process wherein either organic compounds containing ethylenically unsaturated groups are subjected to free radical copolymerization (A) with stilbene, azo or azomethine compounds containing ethylenically unsaturated groups and donor and acceptor groups, or organic compounds containing ethylenically unsaturated groups are subjected to free radical polymerization and are mixed (B) with stilbene, azo or azomethine compounds containing ethylenically unsaturated groups and donor and acceptor groups, the copolymers (A) or mixtures (B) thus obtained are exposed imagewise to high-energy radiation, the unexposed parts are removed and the structured polymer layers thus obtained are polarized in an electric field for orientation of the chromophoric structural units in the region of the glass transition temperature of the polymer and crosslinked in an applied electric field.Such structured polymer layers are suitable for the production of polymeric waveguides in communications technology.
摘要翻译：具有非线性光学性质的结构化聚合物层通过一种方法制备，其中含有烯键式不饱和基团的有机化合物与含有烯属不饱和基团和供体和受体基团的二苯乙烯，偶氮或偶氮甲碱化合物或含有烯键式不饱和基团进行自由基聚合，并与（B）与含有烯键式不饱和基团和供体和受体基团的二苯乙烯，偶氮或偶氮甲碱化合物混合（B），由此获得的共聚物（A）或混合物（B）能量辐射，去除未曝光部分，并且由此获得的结构化聚合物层在电场中极化，以在聚合物的玻璃化转变温度区域内发色团结构单元的取向并在施加的电场中交联。这种结构化聚合物层适用于在通信技术中生产聚合物波导。

8. 发明授权

US5231140A Preparation of polymers with side groups with NLO activity, and the use thereof 失效
标题翻译：具有NLO活性的聚合物聚合物的制备及其使用
公开(公告)号：US5231140A
公开(公告)日：1993-07-27
申请号：US886918
申请日：1992-05-22
申请人： Heike Kilburg , Karl-Heinz Etzbach , Karin H. Beck , Peter Strohriegl , Harry Mueller , Oskar Nuyken
发明人： Heike Kilburg , Karl-Heinz Etzbach , Karin H. Beck , Peter Strohriegl , Harry Mueller , Oskar Nuyken
IPC分类号： C08F20/30 , C08F8/00 , C08F20/26 , C08F20/34 , G02F1/361
CPC分类号： G02F1/3617 , C08F8/00
摘要： The invention relates to a process for the preparation of (meth)acrylate polymers with side-chain, non-linear optical chromophores and molecular weights of from 5000 to 5000000, which comprises reacting polymers of (meth)acryloyl chloride in solution with D-.omega.-hydroxyalkyl chromophores of the formula (I) or the alcoholates thereof ##STR1## where D is an electron donor,A is an electron acceptor,X is CH and/or N, and m is from 2 to 11.The polymers can be used in optical components.
摘要翻译：本发明涉及一种制备具有侧链，非线性光学发色团和分子量为5000至5000000的（甲基）丙烯酸酯聚合物的方法，其包括将（甲基）丙烯酰氯在溶液中的聚合物与D- （I）的羟烷基发色团或其醇化物，其中D是电子给体，A是电子受体，X是CH和/或N，m是2至11。聚合物可用于光学元件。

9. 发明授权

US5461131A Azo dye polymers 失效
标题翻译：偶氮染料聚合物
公开(公告)号：US5461131A
公开(公告)日：1995-10-24
申请号：US393491
申请日：1995-02-24
申请人： Matthias Wiesenfeldt , Sabine Gruettner-Merten , Ruediger Sens , Karl-Heinz Etzbach , Heike Kilburg
发明人： Matthias Wiesenfeldt , Sabine Gruettner-Merten , Ruediger Sens , Karl-Heinz Etzbach , Heike Kilburg
IPC分类号： C08F20/34 , C08F220/34 , C08F246/00 , C09B69/10 , G02F1/361 , C08F228/06 , C08F220/18 , C08F226/02
CPC分类号： C08F220/34 , C08F20/34 , C08F246/00 , C09B69/106 , G02F1/3612 , G02F1/3614 , G02F1/3617
摘要： Azo dye polymers useful in nonlinear optics contain as characteristic monomer units radicals of the formulae I, II, III and IV ##STR1## where D is the radical of a heterocyclic diazo component,R.sup.1 and R.sup.2 are each hydrogen, C.sub.1 -C.sub.6 -alkyl or substituted or unsubstituted C.sub.1 -C.sub.6 -alkoxy, and R.sup.2 may also be C.sub.1 -C.sub.4 -alkanoylamino,R.sup.3 is hydrogen, C.sub.1 -C.sub.6 -alkyl, C.sub.5 -C.sub.7 -cycloalkyl or C.sub.3 -C.sub.4 -alkenyl,R.sup.4 is hydrogen, deuterium, methyl, trideuterated methyl or chlorine,R.sup.5 is hydrogen or deuterium,Y.sup.1 and Y.sup.2 are each substituted or unsubstituted C.sub.2 -C.sub.10 -alkylene,W is oxygen, imino or C.sub.1 -C.sub.4 -alkylimino, andX is hydroxyl, substituted or unsubstituted C.sub.1 -C.sub.6 -alkoxy, phenoxy, amino or mono- or di(C.sub.1 -C.sub.4 -alkyl)amino,and have an average molecular weight of from 1,000 to 100,000.
摘要翻译：可用于非线性光学的偶氮染料聚合物包含式I，II，III和IV的特征单体单元基团。其中D是式（I）杂环重氮组分的基团R 1和R 2各自为氢，C 1 -C 6烷基或取代或未取代的C 1 -C 6 - 烷氧基，R 2也可为C 1 -C 4 - 烷酰基氨基，R 3为氢，C 1 -C 6烷基 C 5 -C 7 - 环烷基或C 3 -C 4 - 烯基，R 4是氢，氘，甲基，三卤代甲基或氯，R 5是氢或氘，Y 1和Y 2各自是取代或未取代的C 2 -C 10亚烷基，W是氧，亚氨基或C1-C4烷基亚氨基，X是羟基，取代或未取代的C1-C6-烷氧基，苯氧基，氨基或单或二（C1-C4-烷基）氨基，平均分子量为1,000至100,000 。

10. 发明授权

US5436306A Methine or azamethine dye polymers 失效
标题翻译：甲基或azamethine染料聚合物
公开(公告)号：US5436306A
公开(公告)日：1995-07-25
申请号：US267543
申请日：1994-06-29
申请人： Karl-Heinz Etzbach , Ruediger Sens , Heike Kilburg
发明人： Karl-Heinz Etzbach , Ruediger Sens , Heike Kilburg
IPC分类号： C08F20/34 , C08F20/38 , C08F246/00 , C09B69/10 , G02F1/35 , G02F1/355 , G02F1/361 , G03C1/12 , C08F228/06 , C08F220/42 , C08F224/00 , C08F226/06
CPC分类号： C08F20/38 , C08F20/34 , C08F246/00 , C09B69/105 , G02F1/3617
摘要： Methine or azamethine dye polymers useful in nonlinear optics contain as characteristic monomer units radicals of the formulae I, II, III and IV ##STR1## where G is a divalent organic radical,Z is nitrogen or CH,R.sup.1 and R.sup.2 are each hydrogen, C.sub.1 -C.sub.6 -alkyl or substituted or unsubstituted C.sub.1 -C.sub.6 -alkoxy,R.sup.3 is hydrogen, C.sub.1 -C.sub.6 -alkyl, C.sub.5 -C.sub.7 -cycloalkyl or C.sub.3 -C.sub.4 -alkenyl,R.sup.4 is hydrogen, deuterium, methyl, trideuterated methyl or chlorine,R.sup.5 is hydrogen or deuterium,Y.sup.1 and Y.sup.2 are each C.sub.2 -C.sub.10 -alkylene,E is oxygen, imino or C.sub.1 -C.sub.4 -alkylimino, andX is hydroxyl, substituted or unsubstituted C.sub.1 -C.sub.6 -alkoxy, phenoxy, amino or C.sub.1 -C.sub.4 -mono- or -dialkylamino, andthe ring A can be benzofused, and have an average molecular weight of from 1,000 to 100,000.
摘要翻译：可用于非线性光学的甲基或氮杂的日染料染料聚合物含有作为特征单体单元的式I，II，III和IV的自由基。其中（I）（II） G是二价有机基团，Z是氮或CH，R 1和R 2各自是氢，C 1 -C 6烷基或取代或未取代的C 1 -C 6 - 烷氧基，R 3是氢，C 1 -C 6烷基，C 5 -C 7 - 环烷基或C 3 -C 4 - 烯基，R 4是氢，氘，甲基，三卤代甲基或氯，R 5是氢或氘，Y 1和Y 2各自是C 2 -C 10亚烷基，E是氧，亚氨基或C 1 -C 4烷基亚氨基， X是羟基，取代或未取代的C 1 -C 6 - 烷氧基，苯氧基，氨基或C 1 -C 4 - 单 - 或二烷基氨基，并且环A可以是苯并稠合的，并且平均分子量为1,000至100,000。

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