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1. 发明申请

US20100179356A1 PROCESSES FOR PRODUCING ETHYLENE GLYCOL FROM OXALATE(S) 有权
标题翻译：用于生产乙酸甘油酯的方法（S）
公开(公告)号：US20100179356A1
公开(公告)日：2010-07-15
申请号：US12642621
申请日：2009-12-18
申请人： Juntao LIU , Weimin Yang , Fengxia Sun , Siqing Zhong , Wanmin Wang
发明人： Juntao LIU , Weimin Yang , Fengxia Sun , Siqing Zhong , Wanmin Wang
IPC分类号： C07C29/136
CPC分类号： B01J35/0006 , B01J21/08 , B01J23/72 , B01J23/745 , B01J23/78 , B01J23/80 , B01J23/868 , B01J23/8892 , B01J37/0201 , C07C29/149 , Y02P20/52 , C07C31/202
摘要： Provided are processes for producing ethylene glycol from oxalate(s), wherein two or more reaction zones in series are used, and oxalate feedstock is fed stagewise, or hydrogen feedstock and optionally a solvent are fed stagewise. The present processes achieve higher selectivity for the product and improved stability of catalysts.
摘要翻译：提供了从草酸生产乙二醇的方法，其中使用串联的两个或更多个反应区，并且草酸进料进料阶段，或者氢原料和任选的溶剂进料阶段进料。本发明方法对产物获得更高的选择性并提高催化剂的稳定性。

2. 发明授权

US08178734B2 Processes for producing ethylene glycol from oxalate(s) 有权
标题翻译：从草酸生产乙二醇的方法
公开(公告)号：US08178734B2
公开(公告)日：2012-05-15
申请号：US12642621
申请日：2009-12-18
申请人： Juntao Liu , Weimin Yang , Fengxia Sun , Siqing Zhong , Wanmin Wang
发明人： Juntao Liu , Weimin Yang , Fengxia Sun , Siqing Zhong , Wanmin Wang
IPC分类号： C07C27/04
CPC分类号： B01J35/0006 , B01J21/08 , B01J23/72 , B01J23/745 , B01J23/78 , B01J23/80 , B01J23/868 , B01J23/8892 , B01J37/0201 , C07C29/149 , Y02P20/52 , C07C31/202
摘要： Provided are processes for producing ethylene glycol from oxalate(s), wherein two or more reaction zones in series are used, and oxalate feedstock is fed stagewise, or hydrogen feedstock and optionally a solvent are fed stagewise. The present processes achieve higher selectivity for the product and improved stability of catalysts.
摘要翻译：提供了从草酸生产乙二醇的方法，其中使用串联的两个或更多个反应区，并且草酸进料进料阶段，或者氢原料和任选的溶剂进料阶段进料。本发明方法对产物获得更高的选择性并提高催化剂的稳定性。

3. 发明授权

US09084984B2 Method for selective hydrogenation of phenylacetylene in the presence of styrene 有权
标题翻译：在苯乙烯存在下苯乙炔的选择性氢化方法
公开(公告)号：US09084984B2
公开(公告)日：2015-07-21
申请号：US13140616
申请日：2009-12-17
申请人： Siqin Li , Juntao Liu , Fengxia Sun , Wanmin Wang , Yuanlin Cheng
发明人： Siqin Li , Juntao Liu , Fengxia Sun , Wanmin Wang , Yuanlin Cheng
IPC分类号： C10G35/09 , B01J29/46 , B01J23/44 , B01J23/755 , B01J23/89 , B01J37/08 , C07C7/167 , B01J21/04
CPC分类号： B01J29/46 , B01J21/04 , B01J23/44 , B01J23/755 , B01J23/892 , B01J37/084 , C07C7/167 , C07C15/46
摘要： The present invention discloses a process for the selective hydrogenation of phenylacetylene in the presence of styrene, comprising contacting a phenylacetylene and styrene-containing hydrocarbon fraction feedstock with a carbon-containing catalyst under hydrogenation reaction conditions, wherein the carbon-containing catalyst has a carbon content of from 0.02 to 8 wt % based on the weight of the catalyst.
摘要翻译：本发明公开了一种在苯乙烯存在下选择性氢化苯基乙炔的方法，包括在氢化反应条件下使苯基乙炔和含苯乙烯的烃馏分原料与含碳催化剂接触，其中含碳催化剂具有碳含量为0.02至8重量％，基于催化剂的重量。

4. 发明申请

US20110308999A1 METHOD FOR SELECTIVE HYDROGENATION OF PHENYLACETYLENE IN THE PRESENCE OF STYRENE 有权
标题翻译：苯乙烯存在下选择性加氢苯乙烯的方法
公开(公告)号：US20110308999A1
公开(公告)日：2011-12-22
申请号：US13140616
申请日：2009-12-17
申请人： Siqin Li , Juntao Liu , Fengxia Sun , Wanmin Wang , Yuanlin Cheng
发明人： Siqin Li , Juntao Liu , Fengxia Sun , Wanmin Wang , Yuanlin Cheng
IPC分类号： C10G35/09 , C10G35/085 , C10G35/06
CPC分类号： B01J29/46 , B01J21/04 , B01J23/44 , B01J23/755 , B01J23/892 , B01J37/084 , C07C7/167 , C07C15/46
摘要： The present invention discloses a process for the selective hydrogenation of phenylacetylene in the presence of styrene, comprising contacting a phenylacetylene and styrene-containing hydrocarbon fraction feedstock with a carbon-containing catalyst under hydrogenation reaction conditions, wherein the carbon-containing catalyst has a carbon content of from 0.02 to 8 wt % based on the weight of the catalyst.
摘要翻译：本发明公开了一种在苯乙烯存在下选择性氢化苯基乙炔的方法，包括在氢化反应条件下使苯基乙炔和含苯乙烯的烃馏分原料与含碳催化剂接触，其中含碳催化剂具有碳含量为0.02至8重量％，基于催化剂的重量。

5. 发明申请

US20130197265A1 PROCESS OF PRODUCING OXALATE BY CO GAS PHASE METHOD 有权
标题翻译：通过气相法制备氧化铝的方法
公开(公告)号：US20130197265A1
公开(公告)日：2013-08-01
申请号：US13641457
申请日：2011-04-13
申请人： Juntao Liu , Fengxia Sun , Jun Kuai
发明人： Juntao Liu , Fengxia Sun , Jun Kuai
IPC分类号： C07C67/18
CPC分类号： C07C67/18 , B01J21/04 , B01J21/063 , B01J23/6562 , B01J23/8926 , B01J23/894 , B01J23/8946 , B01J23/8973 , C07C67/36 , C07C69/38
摘要： The present invention relates to a process of producing oxalate by CO gas phase method for chiefly solving the technical problem of the low utilization efficiency of nitrogen oxides or nitrous acid esters in the prior art. The present invention solves the problem in a better way by using the following steps including: a gas phase stream V containing NO and methanol and oxygen enter a supergravity rotating bed reactor II and are subjected to the oxidative esterification reaction to produce an effluent VI containing methyl nitrite; a methyl nitrite effluent VII obtained from separating said effluent VI together with a CO gas II enter a coupling reactor II and is contacted with a catalyst II to react to form a dimethyl oxalate effluent VIII and a gas phase effluent IX containing NO; the resultant dimethyl oxalate effluent VIII is separated to obtain a dimethyl oxalate product I; optionally, the gas phase effluent IX containing NO is returned to the step above so as to be mixed with the gas phase stream V containing NO for being recycled. Therefore, the process is applicable to the industrial production of oxalate by CO gas phase method.
摘要翻译：本发明涉及一种通过CO气相法生产草酸盐的方法，主要解决现有技术中氮氧化物或亚硝酸酯利用率低的技术问题。本发明通过使用以下步骤更好地解决了该问题，包括：含有NO和甲醇和氧的气相流V进入超重力旋转床反应器II，并进行氧化酯化反应以产生含有甲基亚硝酸盐通过将CO 2气体II与所述流出物VI分离而获得的亚硝酸甲酯流出物VII进入偶联反应器II，并与催化剂II接触以进行反应以形成草酸二乙酯流出物VIII和含有NO的气相流出物IX; 将得到的草酸二甲酯流出物VIII分离得到草酸二甲酯产物I; 任选地，将含有NO的气相流出物IX返回到上述步骤，以与含有NO的气相物流V混合以进行再循环。因此，该方法适用于CO气相法工业生产草酸盐。

6. 发明授权

US08871968B2 Process of producing oxalate by CO gas phase method 有权
标题翻译：通过CO气相法生产草酸盐的方法
公开(公告)号：US08871968B2
公开(公告)日：2014-10-28
申请号：US13641457
申请日：2011-04-13
申请人： Juntao Liu , Fengxia Sun , Jun Kuai
发明人： Juntao Liu , Fengxia Sun , Jun Kuai
IPC分类号： C07C67/18 , C07C67/36 , B01J23/89 , B01J23/656 , B01J21/04 , B01J21/06
CPC分类号： C07C67/18 , B01J21/04 , B01J21/063 , B01J23/6562 , B01J23/8926 , B01J23/894 , B01J23/8946 , B01J23/8973 , C07C67/36 , C07C69/38
摘要： The present invention relates to a process of producing oxalate by CO gas phase method for chiefly solving the technical problem of the low utilization efficiency of nitrogen oxides or nitrous acid esters in the prior art. The present invention solves the problem in a better way by using the following steps including: a gas phase stream V containing NO and methanol and oxygen enter a supergravity rotating bed reactor II and are subjected to the oxidative esterification reaction to produce an effluent VI containing methyl nitrite; a methyl nitrite effluent VII obtained from separating said effluent VI together with a CO gas II enter a coupling reactor II and is contacted with a catalyst II to react to form a dimethyl oxalate effluent VIII and a gas phase effluent IX containing NO; the resultant dimethyl oxalate effluent VIII is separated to obtain a dimethyl oxalate product I; optionally, the gas phase effluent IX containing NO is returned to the step above so as to be mixed with the gas phase stream V containing NO for being recycled. Therefore, the process is applicable to the industrial production of oxalate by CO gas phase method.
摘要翻译：本发明涉及一种通过CO气相法生产草酸盐的方法，主要解决现有技术中氮氧化物或亚硝酸酯利用率低的技术问题。本发明通过使用以下步骤更好地解决了该问题，包括：含有NO和甲醇和氧的气相流V进入超重力旋转床反应器II，并进行氧化酯化反应以产生含有甲基亚硝酸盐通过将CO 2气体II与所述流出物VI分离而获得的亚硝酸甲酯流出物VII进入偶联反应器II，并与催化剂II接触以进行反应以形成草酸二乙酯流出物VIII和含有NO的气相流出物IX; 将得到的草酸二甲酯流出物VIII分离得到草酸二甲酯产物I; 任选地，将含有NO的气相流出物IX返回到上述步骤，以与含有NO的气相物流V混合以进行再循环。因此，该方法适用于CO气相法工业生产草酸盐。

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