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    • 4. 发明授权
    • Process for producing alumina
    • 氧化铝生产工艺
    • US5122349A
    • 1992-06-16
    • US530085
    • 1990-05-29
    • Gyorgy BanvolgyiJozsef ZoldiPeter SiklosiTibor FerencziT. Anna CsordasIvan FeherIldiko Tassy nee VarjuIstvan Sajo
    • Gyorgy BanvolgyiJozsef ZoldiPeter SiklosiTibor FerencziT. Anna CsordasIvan FeherIldiko Tassy nee VarjuIstvan Sajo
    • C01F7/06
    • C01F7/062C01F7/0666
    • An improvement in the process for extracting alumina from gibbsitic bauxites, wherein the basic, known process comprises mixing the bauxites with a sodium hydroxide-sodium aluminate digestion liquor, digesting the bauxites at a temperature in the range of 100.degree.-180.degree. C., diluting the resulting slurry, separating the red mud therefrom, precipitating alumina hydrate by cooling and agitation of the sodium aluminate liquor, and calcining the alumina hydrate precipitate to obtain alumina, wherein the improvement is characterized by so controlling the process that, in the liquid phase of the slurry leaving the digestion reactor, the reactive hydroxide ion concentration is maintained below 6 g/l, and preferably between 0 and 2 g/l, where the reactive hydroxide ion concentration is defined by the following formula: ##EQU1## where: C.sub.Al.sbsb.2 O.sub.3,gi.sup.eq is the equilibrium solubility of Al.sub.2 O.sub.3 for gibbsite, in g/l.C.sub.Al.sbsb.2 O.sub.3 is the actual concentration of Al.sub.2 O.sub.3, in g/l andC.sub.SiO.sbsb.2 is the actual concentration of SiO.sub.2, in g/l.Desirably, control of the process is maintained by regulating the ratio of bauxite to digestion liquor.
    • 碱性已知方法包括将铝土矿与氢氧化钠 - 铝酸钠消化液混合,在100-180℃的温度下消化铝土矿, 稀释所得浆料,从中分离红泥,通过冷却和搅拌铝酸钠液体沉淀氧化铝水合物,并煅烧氧化铝水合物沉淀物以获得氧化铝,其中改进的特征在于控制在液相中 离开消解反应器的浆料中,反应性氢氧根离子浓度保持在6g / l以下,优选在0至2g / l之间,其中活性氢氧根离子浓度由下式定义:其中:CAl 2 O 3 gieq是三水铝矿的Al2O3平衡溶解度,单位为g / l。 CAl2O3是Al2O3的实际浓度,g / l,CSiO2是SiO2的实际浓度,单位为g / l。 理想地,通过调节铝土矿与消化液的比例来保持该方法的控制。
    • 5. 发明授权
    • Equipment for continuous heat treatment of tungsten filaments wound on
molybdenum cores
    • 用于连续热处理钨丝缠绕在钼芯上的设备
    • US4923529A
    • 1990-05-08
    • US258712
    • 1988-10-17
    • Tibor FerencziLaszlo KovacsAttila Szathmari
    • Tibor FerencziLaszlo KovacsAttila Szathmari
    • C21D11/00C22F1/18
    • C21D11/00C22F1/18
    • The invention relates to continuous heat treatment of coiled tungsten filaments wound onto molybdenum cores, in the course of which said filament is passed first through a humid hydrogen atmosphere of about 1300.degree. C. then through a dry hydrogen atmosphere of a temperature of about 1700.degree. to about 1850.degree. C. The method complying with the invention is characterized by transfer times of the coiled tungsten filaments to be heat-treated through heating zones lying in the range of about 3 to about 7 seconds, preferably about 5 seconds, but the duration of passing through the 1700.degree. to 1850.degree. C. high-temperature is at most 7 seconds. The invention also covers the equipment suitable for accomplishing the method, consisting of two high-melting metallic heating tubes, an inventing wheel, a spiral winding/unwinding device, and a temperature sensing and controlling unit. The equipment complying with the invention is also characterized by the tungsten spiral filaments passing in axial direction through heating tubes of low thermal inertia and made of some low-melting metal directly heated with electric current supplied by an electric power unit, temperature control of which is accomplished by electronically controlling the passed-through current, based on measuring the resistance of the heating tube.
    • 本发明涉及卷绕在钼芯上的卷绕的钨丝的连续热处理,其中所述长丝首先通过约1300℃的潮湿氢气氛,然后通过约1700℃的干燥氢气氛 约1850℃。符合本发明的方法的特征在于,通过加热区域进行热处理的螺旋钨丝的转移时间为约3至约7秒,优选约5秒,但持续时间 通过1700°C至1850°C,高温至多7秒。 本发明还包括适用于完成该方法的设备,包括两个高熔点金属加热管,发明轮,螺旋缠绕/退绕装置和温度感测和控制单元。 符合本发明的设备的特征还在于钨螺旋细丝沿轴向通过低热惯性的加热管,并由直接由电力单元提供的电流加热的一些低熔点金属制成,其温度控制是 通过电子控制通过电流,基于测量加热管的电阻来实现。