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    • 2. 发明授权
    • NMR measuring system for weight and humidity of powders
    • 粉末重量和湿度的NMR测量系统
    • US07015693B2
    • 2006-03-21
    • US10836738
    • 2004-04-30
    • Jozef A. W. M. CorverPaul Stewart
    • Jozef A. W. M. CorverPaul Stewart
    • G01V3/00
    • G01N24/08G01N24/085
    • An improvement in a magnetic resonance method for determining the mass of samples wherein the samples include powdered solid materials, including applying a first magnetic field in a first direction in an interrogation zone for creating a net magnetisation within a sample located within the interrogation zone; applying an alternating magnetic field in a second direction in the interrogation zone for temporarily changing the net magnetisation of the sample; monitoring energy emitted by the sample as the net magnetisation of the sample returns to its original state and generating an output signal having a characteristic which is proportional to the energy emitted; comparing the output signal characteristic with like data obtained from at least one similar sample of known mass; and, determining the mass of the sample; the improvement being one of generating the static magnetic field having a field strength in the range of about 0.1 T to about 1.3 T, or disposing the samples within a distance of about 0.5 mm from the surface of the magnetic probe generating the static magnetic field; applying the alternating magnetic field to the sample; sensing the free induction decay energy of the sample and generating a corresponding output free induction decay signal.
    • 用于确定样品质量的磁共振方法的改进,其中样品包括粉末状固体材料,包括在询问区中沿第一方向施加第一磁场,以在位于询问区内的样品内产生净磁化; 在询问区中沿第二方向施加交变磁场,以暂时改变样品的净磁化; 当样品的净磁化返回到其初始状态并产生具有与发射的能量成比例的特性的输出信号时,监测由样品发射的能量; 将输出信号特性与从已知质量的至少一个相似样品获得的类似数据进行比较; 并确定样品的质量; 该改进是产生具有约0.1T至约1.3T范围内的场强的静态磁场之一,或者将样品设置在距产生静磁场的磁探针的表面约0.5mm的距离内; 将交变磁场施加到样品上; 感测样品的自由感应衰减能量并产生相应的输出自由感应衰减信号。
    • 3. 发明授权
    • NMR measuring system
    • NMR测量系统
    • US06946838B2
    • 2005-09-20
    • US10837108
    • 2004-04-30
    • Jozef A. W. M. CorverPaul Stewart
    • Jozef A. W. M. CorverPaul Stewart
    • G01N24/08G01R33/44G01V3/00
    • G01N24/08G01N24/085
    • An improvement in a magnetic resonance method for determining at least one property of multiple samples, including introducing multiple samples into the interrogation zone simultaneously; applying a gradient magnetic field to the interrogation zone wherein different positions within the interrogation zone are sensitive to different specific frequencies; monitoring energy emitted by the samples in the different positions and generating an output signal having a characteristic which is proportional to the energy emitted corresponding thereto in different frequency bands; and, attributing the signals to specific positions and samples, and comparing the output signal characteristics of the specific positions and samples with like data obtained from at least one similar sample to provide an indication of the corresponding property of the samples.
    • 用于确定多个样品的至少一个性质的磁共振方法的改进,包括同时将多个样品引入询问区; 向询问区施加梯度磁场,其中询问区内的不同位置对不同的特定频率敏感; 监测由不同位置的样本发射的能量,并产生具有与在不同频段对应的能量成比例的特性的输出信号; 以及将信号归因于特定位置和样本,并且将特定位置和样本的输出信号特征与从至少一个类似样本获得的相似数据进行比较,以提供样本的相应属性的指示。
    • 7. 发明授权
    • Freeze drying apparatus
    • 冷冻干燥装置
    • US06311409B1
    • 2001-11-06
    • US09255581
    • 1999-02-22
    • Nicholas V. CoppaPaul StewartErnesto Renzi
    • Nicholas V. CoppaPaul StewartErnesto Renzi
    • F26B506
    • F26B5/06
    • The present invention provides methods and apparatus for freeze drying in which a solution, which can be a radioactive salt dissolved within an acid, is frozen into a solid on vertical plates provided within a freeze drying chamber. The solid is sublimated into vapor and condensed in a cold condenser positioned above the freeze drying chamber and connected thereto by a conduit. The vertical positioning of the cold condenser relative to the freeze dryer helps to help prevent substances such as radioactive materials separated from the solution from contaminating the cold condenser. Additionally, the system can be charged with an inert gas to produce a down rush of gas into the freeze drying chamber to also help prevent such substances from contaminating the cold condenser.
    • 本发明提供了一种用于冷冻干燥的方法和装置,其中可将溶解在酸中的放射性盐的溶液在冷冻干燥室内的垂直板上冷冻成固体。 将固体升华成蒸汽并在位于冷冻干燥室上方的冷凝器中冷凝并通过导管与其连接。 冷凝器相对于冷冻干燥机的垂直定位有助于防止从溶液中分离的放射性物质等物质污染冷凝器。 此外,该系统可以带有惰性气体,以产生气体进入冷冻干燥室的下冲,也有助于防止这些物质污染冷凝器。
    • 8. 发明授权
    • Freeze drying method
    • 冷冻干燥方法
    • US5996248A
    • 1999-12-07
    • US716008
    • 1996-09-19
    • Nicholas V. CoppaPaul StewartErnesto Renzi
    • Nicholas V. CoppaPaul StewartErnesto Renzi
    • G21F9/08F26B5/06G21F9/14F26B5/04
    • F26B5/06
    • The present invention provides methods and apparatus for freeze drying in which a solution, which can be a radioactive salt dissolved within an acid, is frozen into a solid on vertical plates provided within a freeze drying chamber. The solid is sublimated into vapor and condensed in a cold condenser positioned above the freeze drying chamber and connected thereto by a conduit. The vertical positioning of the cold condenser relative to the freeze dryer helps to help prevent substances such as radioactive materials separated from the solution from contaminating the cold condenser. Additionally, the system can be charged with an inert gas to produce a down rush of gas into the freeze drying chamber to also help prevent such substances from contaminating the cold condenser.
    • 本发明提供了一种用于冷冻干燥的方法和装置,其中可将溶解在酸中的放射性盐的溶液在冷冻干燥室内的垂直板上冷冻成固体。 将固体升华成蒸汽并在位于冷冻干燥室上方的冷凝器中冷凝并通过导管与其连接。 冷凝器相对于冷冻干燥机的垂直定位有助于防止从溶液中分离的放射性物质等物质污染冷凝器。 此外,该系统可以带有惰性气体,以产生气体进入冷冻干燥室的下冲,也有助于防止这些物质污染冷凝器。