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1. 发明授权

US07829652B2 Polyarylether composition and membrane 有权
标题翻译：聚芳醚组成和膜
公开(公告)号：US07829652B2
公开(公告)日：2010-11-09
申请号：US12183488
申请日：2008-07-31
申请人： Joyce Hung , Daniel Joseph Brunelle , Marianne Elisabeth Harmon , David Roger Moore , Joshua James Stone , Hongyi Zhou , Joseph Anthony Suriano
发明人： Joyce Hung , Daniel Joseph Brunelle , Marianne Elisabeth Harmon , David Roger Moore , Joshua James Stone , Hongyi Zhou , Joseph Anthony Suriano
IPC分类号： C08G2/00
CPC分类号： C08F283/08 , C08F283/06 , C08G65/4075 , C08G65/48 , C08G75/23 , C08G81/00 , C08G2650/40 , C08J5/2256 , C08J2371/12 , C08J2381/06 , C08J2387/00 , C08L51/08 , C08L53/00 , C08L71/00 , C08L81/06 , C08L2205/05 , H01M8/1025 , H01M8/1027 , H01M2300/0082 , C08L2666/02 , C08L81/00 , C08L2666/22
摘要： A composition including a polyarylether copolymer is provided. The copolymer includes a polyarylether backbone; and a sulfonated oligomeric group bonded to the polyarylether suitable for use as a cation conducting membrane. Method of bonding a sulfonated oligomeric group to the polyarylether backbone to form a polyarylether copolymer. The membrane may be formed from the polyarylether copolymer composition. The chain length of the sulfonated oligomeric group may be controlled to affect or control the ion conductivity of the membrane.
摘要翻译：提供了包含聚芳醚基共聚物的组合物。共聚物包括聚芳醚基骨架; 和与适合用作阳离子导电膜的聚芳醚结合的磺化低聚基团。将磺化低聚基团键合到聚芳醚基骨架以形成聚芳醚基共聚物的方法。膜可以由聚芳醚醚共聚物组合物形成。可以控制磺化低聚基团的链长度以影响或控制膜的离子传导性。

2. 发明申请

US20100029864A1 POLYARYLETHER COMPOSITION AND MEMBRANE 有权
标题翻译：聚氨酯组合物和膜
公开(公告)号：US20100029864A1
公开(公告)日：2010-02-04
申请号：US12183488
申请日：2008-07-31
申请人： Joyce Hung , Daniel Joseph Brunelle , Marianne Elisabeth Harmon , David Roger Moore , Joshua James Stone , Hongyi Zhou , Joseph Anthony Suriano
发明人： Joyce Hung , Daniel Joseph Brunelle , Marianne Elisabeth Harmon , David Roger Moore , Joshua James Stone , Hongyi Zhou , Joseph Anthony Suriano
IPC分类号： C08F283/06
CPC分类号： C08F283/08 , C08F283/06 , C08G65/4075 , C08G65/48 , C08G75/23 , C08G81/00 , C08G2650/40 , C08J5/2256 , C08J2371/12 , C08J2381/06 , C08J2387/00 , C08L51/08 , C08L53/00 , C08L71/00 , C08L81/06 , C08L2205/05 , H01M8/1025 , H01M8/1027 , H01M2300/0082 , C08L2666/02 , C08L81/00 , C08L2666/22
摘要： A composition including a polyarylether copolymer is provided. The copolymer includes a polyarylether backbone; and a sulfonated oligomeric group bonded to the polyarylether suitable for use as a cation conducting membrane. Method of bonding a sulfonated oligomeric group to the polyarylether backbone to form a polyarylether copolymer. The membrane may be formed from the polyarylether copolymer composition. The chain length of the sulfonated oligomeric group may be controlled to affect or control the ion conductivity of the membrane.
摘要翻译：提供了包含聚芳醚基共聚物的组合物。共聚物包括聚芳醚基骨架; 和与适合用作阳离子导电膜的聚芳醚结合的磺化低聚基团。将磺化低聚基团键合到聚芳醚基骨架以形成聚芳醚基共聚物的方法。膜可以由聚芳醚醚共聚物组合物形成。可以控制磺化低聚基团的链长度以影响或控制膜的离子传导性。

3. 发明申请

US20090163692A1 AROMATIC POLYETHERS 审中-公开
标题翻译：芳香聚醚
公开(公告)号：US20090163692A1
公开(公告)日：2009-06-25
申请号：US11962627
申请日：2007-12-21
申请人： David Roger Moore , Gary William Yeager , Daniel Joseph Brunelle , Marianne Elisabeth Harmon , Joyce Hung , Joseph Anthony Suriano , Hongyi Zhou
发明人： David Roger Moore , Gary William Yeager , Daniel Joseph Brunelle , Marianne Elisabeth Harmon , Joyce Hung , Joseph Anthony Suriano , Hongyi Zhou
IPC分类号： C08G75/02
CPC分类号： C08G65/40 , C07C317/14 , C07C317/22 , C07C317/44 , C08G65/4006 , C08G75/23
摘要： An aromatic polyether comprising structural units derived from a halosulfone sulfonate having structure (I): wherein R1 is a C3-C25 aromatic radical, a C3-C25 cycloaliphatic radical, or a C1-C10 aliphatic radical; M is hydrogen or a charge balancing cation; Y1 is independently at each occurrence a halogen; “t” is an integer having a value of 1 or 2; “s” is an integer having a value 0 to 3, “b” is an integer having a value 1 to 4; and “c” is an integer having a value 1 to 20. Also provided are methods of preparing the aromatic polyethers, and compositions including the aromatic polyethers.
摘要翻译：包含衍生自具有结构（I）的卤代磺酸盐的结构单元的芳族聚醚：其中R1是C3-C25芳族基团，C3-C25脂环族基团或C1-C10脂族基团; M是氢或电荷平衡阳离子; Y1在每次出现时独立地为卤素; “t”是1或2的整数; “s”为0〜3的整数，b为1〜4的整数， “c”是1至20的整数。还提供了制备芳族聚醚的方法和包括芳族聚醚的组合物。

4. 发明申请

US20080114149A1 Polymers comprising superacidic groups, and uses thereof 审中-公开
标题翻译：包含超酸基团的聚合物及其用途
公开(公告)号：US20080114149A1
公开(公告)日：2008-05-15
申请号：US11598948
申请日：2006-11-14
申请人： David Roger Moore , Hongyi Zhou , Daniel Joseph Brunelle , Marianne Elisabeth Harmon , Joyce Hung
发明人： David Roger Moore , Hongyi Zhou , Daniel Joseph Brunelle , Marianne Elisabeth Harmon , Joyce Hung
IPC分类号： C08G63/688
CPC分类号： C08G75/23 , C08G65/4025 , C08G65/4056
摘要： The invention relates generally to polymers derived from monomers having aromatic superacidic functional groups. The superacidic functional groups comprise fluorinated sulfonate moieties. Polymers provided by the present invention include polyethers, polyesters, polycarbonates, polyestercarbonates, polyetherketones, and polyethersulfones among others. The polymers provided by the present invention include block and random copolymers. In one embodiment, the present invention provides a polyetherketone-polyethersulfone block copolymer comprising superacidic functional groups. Polymers comprising superacidic functional groups are useful materials in membrane applications. The superacidic functional groups present in the new polymer compositions impart excellent proton conductivities. In one embodiment, the present invention provides polymers useful as materials for polymer electrolyte fuel cell membranes.
摘要翻译：本发明一般涉及衍生自具有芳族超酸官能团的单体的聚合物。超酸性官能团包括氟化磺酸盐部分。本发明提供的聚合物包括聚醚，聚酯，聚碳酸酯，聚酯碳酸酯，聚醚酮和聚醚砜等。本发明提供的聚合物包括嵌段和无规共聚物。在一个实施方案中，本发明提供了包含超酸官能团的聚醚酮 - 聚醚砜嵌段共聚物。包含超酸性官能团的聚合物是膜应用中的有用材料。存在于新聚合物组合物中的超酸性官能团赋予优异的质子导电性。在一个实施方案中，本发明提供了可用作聚合物电解质燃料电池膜的材料的聚合物。

5. 发明授权

US07595373B2 Sulfonated polyaryletherketone-polyethersulfone block copolymers 失效
标题翻译：磺化聚芳醚酮 - 聚醚砜嵌段共聚物
公开(公告)号：US07595373B2
公开(公告)日：2009-09-29
申请号：US11314877
申请日：2005-12-20
申请人： Joyce Hung , Hongyi Zhou , Marianne Elisabeth Harmon , Daniel Joseph Brunelle , Hongwei Liu , David Roger Moore , Daniel Steiger
发明人： Joyce Hung , Hongyi Zhou , Marianne Elisabeth Harmon , Daniel Joseph Brunelle , Hongwei Liu , David Roger Moore , Daniel Steiger
IPC分类号： C08G2/00
CPC分类号： C08G75/23
摘要： Sulfonated block copolymer suitable for use as proton exchange membranes for fuel cells comprise sulfonated polyaryletherketone blocks and polyethersulfone blocks. The sulfonated polyaryletherketone blocks comprise structural units of formula the polyethersulfone blocks comprising structural units of formula wherein R1, R2, R3 and R4 are independently C1-C10 alkyl, C3-C12 cycloalkyl, C6-C14 aryl, allyl, alkenyl, alkoxy,halo, or cyano; Z and Z1 are independently a direct bond or O, S, (CH2)r; (CF2)r, C(CH3)2, C(CF3)2, or a combination thereof; M is H, a metal cation, a non-metallic inorganic cation, an organic cation or a mixture thereof a is 0 or an integer from 1 to 3; b, c and d are independently 0 or an integer from 1 to 4; m and n are independently 0 or 1; and r is an integer from 1 to 5.
摘要翻译：适用于燃料电池质子交换膜的磺化嵌段共聚物包括磺化聚芳醚酮嵌段和聚醚砜嵌段。所述磺化聚芳醚酮嵌段包含结构式的结构单元，所述结构单元包括结构单元，其中R 1，R 2，R 3和R 4独立地为C 1 -C 10烷基，C 3 -C 12环烷基，C 6 -C 14芳基，烯丙基，烯基，烷氧基，或氰基; Z和Z1独立地是直接键或O，S，（CH 2）r; （CF 2）r，C（CH 3）2，C（CF 3）2或其组合; M为H，金属阳离子，非金属无机阳离子，有机阳离子或其混合物a为0或1〜3的整数; b，c和d独立地为0或1〜4的整数; m和n独立地为0或1; r为1〜5的整数。

6. 发明授权

US07547756B2 Benzimidazole-containing sulfonated polyethersulfones 失效
标题翻译：含苯并咪唑的磺化聚醚砜
公开(公告)号：US07547756B2
公开(公告)日：2009-06-16
申请号：US11263166
申请日：2005-10-31
申请人： Joyce Hung , Hongyi Zhou , Daniel Joseph Brunelle , Marianne Elisabeth Harmon , Daniel Steiger , Hongwei Liu , David Roger Moore
发明人： Joyce Hung , Hongyi Zhou , Daniel Joseph Brunelle , Marianne Elisabeth Harmon , Daniel Steiger , Hongwei Liu , David Roger Moore
IPC分类号： C08G75/23 , C08G75/20
CPC分类号： C08G65/4037 , C08G65/4043 , C08G65/4056 , C08L79/04
摘要： Sulfonated polyethersulfones and polymer compositions comprising sulfonated polyethersulfones and at least one inorganic heteropolyacid are useful as proton exchange membranes for fuel cells. The polyethersulfones include structural units derived from at least one biphenol monomer and a monomer of formula I wherein X is O, S or NR1; Y is N or CR5; R1, R2, R3 and R4 are independently hydrogen, alkyl, substituted alkyl, aryl, substituted aryl, alkylaryl, substituted alkylaryl, arylalkyl or substituted arylalkyl, or R3 and R4, taken together, form a 5- or 6-membered substituted or unsubstituted aliphatic or aromatic ring; R5 is hydrogen, alkyl, substituted alkyl, aryl, substituted aryl, alkylaryl, substituted alkylaryl, arylalkyl or substituted arylalkyl; and L is a direct bond or a divalent aromatic linker containing 6-12 carbons.
摘要翻译：包含磺化聚醚砜和至少一种无机杂多酸的磺化聚醚砜和聚合物组合物可用作燃料电池的质子交换膜。聚醚砜包括衍生自至少一种联苯酚单体的结构单元和式I的单体，其中X是O，S或NR1; Y为N或CR5; R 1，R 2，R 3和R 4独立地为氢，烷基，取代的烷基，芳基，取代的芳基，烷基芳基，取代的烷基芳基，芳烷基或取代的芳基烷基，或者R 3和R 4一起形成5-或6-元取代或未取代的脂肪族或芳香环; R5是氢，烷基，取代的烷基，芳基，取代的芳基，烷基芳基，取代的烷基芳基，芳基烷基或取代的芳基烷基; L是直接键或含有6-12个碳原子的二价芳族连接体。

7. 发明授权

US07635744B2 Trifluorovinyloxy monomers and polymers 失效
标题翻译：三氟乙烯基氧基单体和聚合物
公开(公告)号：US07635744B2
公开(公告)日：2009-12-22
申请号：US11397109
申请日：2006-04-05
申请人： David Roger Moore , Hongyi Zhou , Christoph Georg Erben , Marianne Elisabeth Harmon , Joyce Hung , Hongwei Liu , Daniel Steiger , Daniel Joseph Brunelle
发明人： David Roger Moore , Hongyi Zhou , Christoph Georg Erben , Marianne Elisabeth Harmon , Joyce Hung , Hongwei Liu , Daniel Steiger , Daniel Joseph Brunelle
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： C08G75/23
摘要： Reactive monomers containing the trifluorovinyloxy group may be copolymerized to form polymers useful as membranes, especially polymer electrolyte membranes for fuel cells. The monomers have the formula ((CF2CFO(R1)p)nArX2 wherein Ar is a trivalent, tetravalent or pentavalent, substituted or unsubstituted, aromatic or heteroaromatic, monocyclic or polycyclic group having from 5 to 50 carbon atoms; X is OH, SH, NR2aR2b, F or Br; p is 0 or 1; n is 1, 2 or 3; R1 is substituted or unsubstituted phenyl and R2a and R2b are independently H, C1-C8 alkyl or C1-C8 perfluoroalkyl.
摘要翻译：含有三氟乙烯基氧基的反应性单体可以共聚以形成可用作膜的聚合物，特别是用于燃料电池的聚合物电解质膜。单体具有式（（CF 2 CFO（R 1）p）nArX 2，其中Ar是具有5至50个碳原子的三价，四价或五价，取代或未取代的芳族或杂芳族单环或多环基团; X是OH，SH， NR2aR2b，F或Br; p是0或1; n是1,2或3; R1是取代或未取代的苯基，R2a和R2b独立地是H，C1-C8烷基或C1-C8全氟烷基。

8. 发明授权

US07598337B2 Mixed-sulfonation block copolymers 失效
标题翻译：混合磺化嵌段共聚物
公开(公告)号：US07598337B2
公开(公告)日：2009-10-06
申请号：US11314337
申请日：2005-12-20
申请人： Joyce Hung , Hongyi Zhou , David Roger Moore , Marianne Elisabeth Harmon , Daniel Joseph Brunelle , Hongwei Liu
发明人： Joyce Hung , Hongyi Zhou , David Roger Moore , Marianne Elisabeth Harmon , Daniel Joseph Brunelle , Hongwei Liu
IPC分类号： C08G2/00
CPC分类号： C08G65/4012 , C08G65/48 , C08G75/23
摘要： Sulfonated block copolymers that may be used as membranes for fuel cells include sulfonated polyaryletherketone blocks and lightly sulfonated polyethersulfone blocks.The sulfonated polyaryletherketone blocks include structural units of formula and the lightly sulfonated polyethersulfone blocks include structural units of formula wherein R1, R2, R3, R4, R5 and R6 are independently C1-C10 alkyl, C3-C12 cycloalkyl, C6-C14 aryl, allyl, alkenyl, alkoxy, halo, or cyano; Z, Z1 and Z2 are independently a direct bond or O, S, (CH2)r, (CF2)r, C(CH3)2, C(CF3)2, or a combination thereof; M is H, a metal cation, a non-metallic inorganic cation, an organic cation or a mixture thereof; a and e are independently 0 or an integer from 1 to 3; b, c, d, and f are independently 0 or an integer from 1 to 4; m, n and p are independently 0 or 1; and r is an integer from 1 to 5.
摘要翻译：可用作燃料电池膜的磺化嵌段共聚物包括磺化聚芳醚酮嵌段和轻质磺化聚醚砜嵌段。磺化的聚芳醚酮嵌段包括式的结构单元，轻度磺化的聚醚砜嵌段包括下式的结构单元：其中R1，R2，R3，R4，R5和R6独立地为C1-C10烷基，C3-C12环烷基，C6-C14芳基，烯丙基，烯基，烷氧基，卤素或氰基; Z，Z 1和Z 2独立地为直接键或O，S，（CH 2）r，（CF 2）r，C（CH 3）2，C（CF 3） M是H，金属阳离子，非金属无机阳离子，有机阳离子或其混合物; a和e独立地为0或1〜3的整数; b，c，d和f独立地为0或1〜4的整数; m，n和p独立地为0或1; r为1〜5的整数。

9. 发明授权

US07393914B2 Polyethersulfone compositions 失效
标题翻译：聚醚砜组合物
公开(公告)号：US07393914B2
公开(公告)日：2008-07-01
申请号：US11193552
申请日：2005-07-29
申请人： David Roger Moore , Hongyi Zhou , Daniel Steiger , Joyce Hung , Daniel Joseph Brunelle , Hongwei Liu , Marianne Elisabeth Harmon
发明人： David Roger Moore , Hongyi Zhou , Daniel Steiger , Joyce Hung , Daniel Joseph Brunelle , Hongwei Liu , Marianne Elisabeth Harmon
IPC分类号： C08G75/00 , C08G8/02
CPC分类号： G11B7/22 , G11B7/1356 , G11B7/1362 , G11B2007/0006
摘要： Novel polyethersulfone compositions have been discovered which incorporate structural subunits derived from sulfonated bis(halophenyl)sulfones, dihydroxy terphenyls, and/or bis(hydroxyphenyl)pyridines. The sulfonated polyethersulfones show promise as materials for use in polymer electrolyte membranes (PEMs) in fuel cells owing to their high proton conductivities (0.02-0.07 S/cm at 20° C. and 100 percent humidity). In addition, a novel unsulfonated thermoplastic polyethersulfone comprising structural subunits derived from a non-sulfonated bis(halophenyl)sulfone bis4-fluorophenyl)sulfone and 4,4′-dihydroxyphenyl-2,6-pyridine (CAS No. 171820-16-9) is disclosed.
摘要翻译：已经发现新的聚醚砜组合物掺入衍生自磺化双（卤代苯基）砜，二羟基三联苯和/或双（羟基苯基）吡啶的结构亚单位。磺化聚醚砜由于其高质子电导率（在20℃和100％湿度下为0.02-0.07S / cm），在燃料电池中用作聚合物电解质膜（PEM）的材料显示出希望。另外，包含衍生自非磺化双（卤代苯基）砜双-4-氟苯基）砜和4,4'-二羟基苯基-2,6-吡啶（CAS号171820-16-9）的结构亚单位的新型未磺化热塑性聚醚砜，被披露。

10. 发明申请

US20080004443A1 Sulfonated polyaryletherketone-block-polyethersulfone copolymers 审中-公开
标题翻译：磺化聚芳醚酮 - 嵌段 - 聚醚砜共聚物
公开(公告)号：US20080004443A1
公开(公告)日：2008-01-03
申请号：US11479202
申请日：2006-07-03
申请人： Daniel Joseph Brunelle , Hongyi Zhou , Hongwei Liu , Joyce Hung , Marianne Elisabeth Harmon , David Roger Moore
发明人： Daniel Joseph Brunelle , Hongyi Zhou , Hongwei Liu , Joyce Hung , Marianne Elisabeth Harmon , David Roger Moore
IPC分类号： C07D295/00
CPC分类号： H01M8/1025 , C08G65/4012 , C08G65/48 , C08G75/23 , C08J5/2256 , C08J2371/12 , H01M8/1027 , H01M2300/0082
摘要： Sulfonated block copolymer suitable for use as proton exchange membranes for fuel cells comprise sulfonated polyaryletherketone blocks and polyethersulfone blocks. The sulfonated polyaryletherketone blocks comprise structural units of formula I wherein R1 is C1-C10 alkyl, C3-C12 cycloalkyl, C6-C14 aryl, allyl, alkenyl, alkoxy, halo, or cyano; Ar1 and Ar2 are each independently C6-C20 aromatic radicals, or Ar1 and Ar2, taken together with an intervening carbon atom, form a bicyclic C6-C20 aromatic radical or a tricyclic C6-C20 aromatic radical; M is H, a metal cation, a non-metallic inorganic cation, an organic cation or a mixture thereof; and a is 0 or an integer from 1 to 4.
摘要翻译：适用于燃料电池质子交换膜的磺化嵌段共聚物包括磺化聚芳醚酮嵌段和聚醚砜嵌段。磺化的聚芳醚酮嵌段包含式I的结构单元，其中R 1是C 1 -C 10烷基，C 3〜 -C 12 -C 12环烷基，C 6 -C 14芳基，烯丙基，烯基，烷氧基，卤素或氰基; Ar 1和Ar 2各自独立地为C 6 -C 20芳族基团或Ar 1 与其间插入的碳原子一起形成双环C 6 -C 20芳族基团或三环C 1 -C 20芳族基团 C 6 -C 20芳族基团; M是H，金属阳离子，非金属无机阳离子，有机阳离子或其混合物; a为0或1〜4的整数。

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