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1. 发明授权

US5852088A Nanoporous ceramics with catalytic functionality 失效
标题翻译：具有催化功能的纳米多孔陶瓷
公开(公告)号：US5852088A
公开(公告)日：1998-12-22
申请号：US578084
申请日：1995-12-27
申请人： John P. Dismukes , Jack Wayne Johnson , John Stewart Bradley
发明人： John P. Dismukes , Jack Wayne Johnson , John Stewart Bradley
IPC分类号： B01J35/10 , C04B38/00 , C08K5/00
CPC分类号： C04B38/0022 , B01J35/1014 , B01J35/1019 , B01J35/1038 , B01J35/1057 , C04B2111/00801 , C04B2111/0081
摘要： The present invention provides for amorphous, nanoporous, catalytic metal-containing ceramic material having a surface area in excess of 70 m.sup.2 /gm and characterized by a high content of open microporous cell structure wherein the micropores have a mean width of less than 20 Angstroms and wherein said microporous structure comprises a volume of greater than about 0.03 cm.sup.3 /gm of the ceramic. The invention also provides for a preceramic composite intermediate composition comprising a mixture of a ceramic precursor and from about 0.5 up to about 65 wt % of an organometallic compound containing a metal of Group IB, II, III, IV, IV, V, VIB, VIIA or VIII of the Periodic Table, including rare earth metals, whose pyrolysis product in ammonia or an inert atmosphere at temperatures of up to less than about 1100.degree. C. gives rise to the nanoporous catalytic ceramics of the invention. Also provided is a process for the preparation of the nanoporous ceramics of the invention involving pyrolysis of the ceramic intermediate under controlled conditions of heating up to temperatures of less than about 1100.degree. C. to form a nanoporous ceramic product useful in catalytic and membrane separation processes.
摘要翻译：本发明提供了具有超过70m 2 / gm的表面积的无定形，纳米孔，催化含金属的陶瓷材料，其特征在于高含量的开孔微孔孔结构，其中微孔的平均宽度小于20埃，其中所述微孔结构包括大于约0.03cm 3 / gm的陶瓷体积。本发明还提供了一种预陶瓷复合中间体组合物，其包含陶瓷前体和约0.5至约65重量％的含有IB，II，III，IV，IV，V，VIB族金属的金属的有机金属化合物的混合物，包括稀土金属的元素周期表VIIA或VIII，它们的热解产物在氨或惰性气氛中，温度高达约1100℃，产生本发明的纳米多孔催化陶瓷。还提供了制备本发明的纳米多孔陶瓷的方法，其包括在加热到低于约1100℃的温度的受控条件下陶瓷中间体的热解，以形成可用于催化和膜分离过程的纳米多孔陶瓷产物。

2. 发明授权

US5952421A Synthesis of preceramic polymer-stabilized metal colloids and their conversion to microporous ceramics 失效
标题翻译：合成前陶瓷聚合物稳定金属胶体及其转化为微孔陶瓷
公开(公告)号：US5952421A
公开(公告)日：1999-09-14
申请号：US579444
申请日：1995-12-27
申请人： John Stewart Bradley , Ernestine Williams Hill , John P. Dismukes , Paul James Tindall
发明人： John Stewart Bradley , Ernestine Williams Hill , John P. Dismukes , Paul James Tindall
IPC分类号： B01D71/02 , B01J37/08 , C04B38/00 , C08G77/06
CPC分类号： B01D67/0072 , B01D67/0044 , B01D67/0067 , B01D71/02 , B01J37/082 , C04B38/0022 , B01D2323/08 , B01D2323/18 , B01D2325/02
摘要： The present invention provides for microporous ceramic materials having a surface area in excess of 70 m.sup.2 /gm and an open microporous cell structure wherein the micropores have a mean width of less than 20 Angstroms and wherein said microporous structure comprises a volume of greater than about 0.03 cm.sup.3 /gm of the ceramic. The invention also provides for a preceramic composite intermediate composition comprising a mixture of a ceramic precursor and nanoscale size metallic particles, whose pyrolysis product in inert atmosphere or in an ammonia atmosphere at temperatures of up to less than about 1100.degree. C. gives rise to the microporous ceramics of the invention. Also provided is a process for the preparation of the microporous ceramics of the invention involving pyrolysis of the composite intermediate under controlled conditions of heating up to temperatures of less than about 1100.degree. C. to form a microporous ceramic product.
摘要翻译：本发明提供了具有超过70m 2 / gm的表面积的微孔陶瓷材料和一种开孔微孔孔结构，其中微孔具有小于20埃的平均宽度，其中所述微孔结构包括大于约0.03的体积 cm3 / gm的陶瓷。本发明还提供了一种预陶瓷复合中间体组合物，其包含陶瓷前体和纳米尺寸金属颗粒的混合物，其在惰性气氛中或在氨气氛中的热解产物在高至少于约1100℃的温度下产生本发明的微孔陶瓷。还提供了一种制备本发明的微孔陶瓷的方法，包括在加热至少于约1100℃的温度的受控条件下复合中间体的热解，以形成微孔陶瓷产物。

3. 发明授权

US5696217A Synthesis of microporous ceramics by ammonia pyrolysis of ceramic precursors 失效
标题翻译：通过陶瓷前体的氨热解合成微孔陶瓷
公开(公告)号：US5696217A
公开(公告)日：1997-12-09
申请号：US385299
申请日：1995-02-10
申请人： John Pickett Dismukes , John Stewart Bradley , Jack Wayne Johnson , Edward William Corcoran, Jr.
发明人： John Pickett Dismukes , John Stewart Bradley , Jack Wayne Johnson , Edward William Corcoran, Jr.
IPC分类号： C04B35/58 , B01D71/02 , C04B35/56 , C04B38/00 , C08G77/60 , C08G77/62 , C08G77/00 , C04B35/52
CPC分类号： B01D67/0067 , B01D67/0074 , B01D71/02 , C04B38/0022 , B01D2323/08 , B01D2325/02
摘要： The present invention provides for microporous ceramic materials having a surface area in excess of 100 m.sup.2 /gm and an open microporous cell structure wherein the micropores have a mean width of less than 20 Angstroms and wherein said microporous structure comprises a volume of greater than about 0.05 cm.sup.3 /gm of the ceramic. The pyrolysis product of ceramic precursor oligomers or polymers having a number average molecular weight in the range of from about 200 to about 100,000 g/mole in an ammonia atmosphere at temperatures of up to less than about 1200.degree. C. gives rise to the microporous ceramics of the invention. Also provided is a process for the preparation of the microporous ceramics of the invention involving pyrolysis of the ceramic precursor under controlled conditions of heating and with intermediate hold times, up to temperatures of less than 1200.degree. C., preferably less than 1000.degree. C., to form a microporous ceramic product.
摘要翻译：本发明提供了具有超过100m 2 / gm的表面积的微孔陶瓷材料和开放的微孔孔结构，其中微孔具有小于20埃的平均宽度，并且其中所述微孔结构包括大于约0.05的体积 cm3 / gm的陶瓷。陶瓷前体低聚物或聚合物的热解产物，其数均分子量在约200至约100,000克/摩尔的范围内，在氨气氛中在高于约1200℃的温度下产生微孔陶瓷的本发明。还提供了制备本发明的微孔陶瓷的方法，其包括在受控的加热条件下和中间保持时间下高达1200℃，优选小于1000℃的陶瓷前体的热解。，以形成微孔陶瓷产品。

4. 发明申请

US20100202939A1 NOVEL NANOPOROUS MATERIALS 审中-公开
标题翻译：新型纳米材料
公开(公告)号：US20100202939A1
公开(公告)日：2010-08-12
申请号：US12764468
申请日：2010-04-21
申请人： John Stewart Bradley , Fei Cheng , Stephen Malcolm Kelly
发明人： John Stewart Bradley , Fei Cheng , Stephen Malcolm Kelly
IPC分类号： B01J8/02 , B01D24/00 , B01D50/00 , B01J27/24
CPC分类号： B01D71/02 , B01D53/885 , B01D67/0048 , B01D67/0067 , B01D67/0093 , B01D69/10 , B01D69/145 , B01D71/022 , B01D2325/02 , B01D2325/10 , B01D2325/22 , B01D2325/46 , B01J23/44 , B01J27/24 , B01J35/10 , B01J35/1061 , C01B21/068 , C01P2006/12 , C01P2006/16 , C01P2006/17 , C04B38/0045 , C04B41/009 , C04B41/5066 , C04B41/87 , C04B2111/00793 , G01N27/40 , Y10T428/249978 , C04B41/4537 , C04B41/4582 , C04B35/584 , C04B35/597 , C04B38/0054 , C04B35/10
摘要： The invention provides a nanoporous non-oxide material which comprises a modified derivative of silicon nitride and comprises a plurality of nanoscale pores. The nanoporous non-oxide material is preferably prepared by means of a sol-gel procedure and preferably comprises a metal-containing derivative of silicon nitride [SiN4], silicon oxynitride [Si2N2O] or silicon imidonitride [Si3N4−2x(NH)3x] which contains a Group III metal or a transition metal. The nanoporous non-oxide material also additionally comprises surface modifications. The invention also provides for the use of the nanoporous non-oxide material in the manufacture of selective gas filters for solid state gas sensors and catalysts for chemical reactions.
摘要翻译：本发明提供一种纳米多孔非氧化物材料，其包含氮化硅的改性衍生物并且包含多个纳米级孔。纳米多孔非氧化物材料优选通过溶胶 - 凝胶法制备，并且优选包含氮化硅[SiN 4]，氮氧化硅[Si 2 N 2 O]或亚氨基氮化硅[Si 3 N 4 -2 x（NH）3 x]的含金属衍生物，其中含有III族金属或过渡金属。纳米多孔非氧化物材料还包括表面改性。本发明还提供了纳米多孔非氧化物材料在固态气体传感器选择性气体过滤器和用于化学反应的催化剂的制造中的应用。

5. 发明申请

US20090131248A1 NOVEL NANOPOROUS MATERIALS 审中-公开
标题翻译：新型纳米材料
公开(公告)号：US20090131248A1
公开(公告)日：2009-05-21
申请号：US11577881
申请日：2005-10-21
申请人： John Stewart Bradley , Fei Cheng , Stephen Malcolm Kelly
发明人： John Stewart Bradley , Fei Cheng , Stephen Malcolm Kelly
IPC分类号： B32B5/18 , B01J21/06 , C01B21/068 , B01D53/22
CPC分类号： B01D71/02 , B01D53/885 , B01D67/0048 , B01D67/0067 , B01D67/0093 , B01D69/10 , B01D69/145 , B01D71/022 , B01D2325/02 , B01D2325/10 , B01D2325/22 , B01D2325/46 , B01J23/44 , B01J27/24 , B01J35/10 , B01J35/1061 , C01B21/068 , C01P2006/12 , C01P2006/16 , C01P2006/17 , C04B38/0045 , C04B41/009 , C04B41/5066 , C04B41/87 , C04B2111/00793 , G01N27/40 , Y10T428/249978 , C04B41/4537 , C04B41/4582 , C04B35/584 , C04B35/597 , C04B38/0054 , C04B35/10
摘要： The invention provides a nanoporous non-oxide material which comprises a modified derivative of silicon nitride and comprises a plurality of nanoscale pores. The nanoporous non-oxide material is preferably prepared by means of a sol-gel procedure and preferably comprises a metal-containing derivative of silicon nitride [SiN4], silicon oxynitride [Si2N2O] or silicon imidonitride [Si3N4-2x(NH)3x] which contains a Group III metal or a transition metal. The nanoporous non-oxide material also additionally comprises surface modifications. The invention also provides for the use of the nanoporous non-oxide material in the manufacture of selective gas filters for solid state gas sensors and catalysts for chemical reactions.
摘要翻译：本发明提供一种纳米多孔非氧化物材料，其包含氮化硅的改性衍生物并且包含多个纳米级孔。纳米多孔非氧化物材料优选通过溶胶 - 凝胶法制备，并且优选包含氮化硅[SiN 4]，氮氧化硅[Si 2 N 2 O]或亚氨基氮化硅[Si 3 N 4 -2 x（NH）3 x]的含金属衍生物，其中含有III族金属或过渡金属。纳米多孔非氧化物材料还包括表面改性。本发明还提供了纳米多孔非氧化物材料在固态气体传感器选择性气体过滤器和用于化学反应的催化剂的制造中的应用。

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