会员体验
专利管家(专利管理)
工作空间(专利管理)
风险监控(情报监控)
数据分析(专利分析)
侵权分析(诉讼无效)
联系我们
交流群
官方交流:
QQ群: 891211   
微信请扫码    >>>
现在联系顾问~
热词
    • 2. 发明授权
    • Process for the production of triethylenediamine
    • 三亚乙基二胺生产工艺
    • US5756741A
    • 1998-05-26
    • US751142
    • 1996-11-15
    • John Nelson ArmorJose Guadalupe SantiestebanHong-Xin Li
    • John Nelson ArmorJose Guadalupe SantiestebanHong-Xin Li
    • B01J29/40C07B61/00C07C209/60C07C209/62C07C211/09C07D487/08
    • C07D487/08
    • A process for preparing triethylenediamine by passing an amine compound over a catalyst at elevated temperature to afford a reaction product containing triethylenediamine and piperazine, the amine compound having, in the molecule, a moiety represented by the following general formula ##STR1## where R.sup.1, R.sup.2, R.sup.3 and R.sup.4 are independently a hydrogen atom or an alkyl group having 1 to 4 carbon atoms and X is oxygen or nitrogen characterized by adding an ethylating compound containing at least one nitrogen and/or oxygen atom to the reaction product and contacting the reaction product, under conditions sufficient to produce triethylenediamine from the ethylating compound and piperazine, with a condensation/cyclization shape-selective zeolite catalyst demonstrating a triethylenediamine/piperazine weight ratio uptake value of at least 6:1.
    • 一种通过使胺化合物在升高的温度下通过催化剂制备三亚乙基二胺的方法,得到含有三亚乙基二胺和哌嗪的反应产物,所述胺化合物在分子中具有由以下通式表示的部分,其中R1,R2 R 3和R 4独立地是氢原子或具有1至4个碳原子的烷基,X是氧或氮,其特征在于向反应产物中加入含有至少一个氮原子和/或氧原子的乙基化合物,并使反应产物 在足以从乙基化合物和哌嗪产生三亚乙基二胺的条件下,使用缩合/环化形状选择性沸石催化剂,证明三亚乙基二胺/哌嗪的重量比吸收值至少为6:1。