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1. 发明授权

US5319118A Volatile barium precursor and use of precursor in OMCVD process 失效
标题翻译：挥发性钡前体和前体在OMCVD工艺中的应用
公开(公告)号：US5319118A
公开(公告)日：1994-06-07
申请号：US779435
申请日：1991-10-17
申请人： John A. T. Norman , Beth A. Muratore , Paul N. Dyer
发明人： John A. T. Norman , Beth A. Muratore , Paul N. Dyer
IPC分类号： C07C45/45 , C07C49/12 , C07C49/92 , C23C16/40 , C07F3/00
CPC分类号： C23C16/404 , C07C45/455 , C07C49/12 , C07C49/92
摘要： Novel volatile barium complexes are disclosed which are very stable and evaporate cleanly at elevated temperatures. Such complexes are highly suited for use as a barium source in OMCVD processes.
摘要翻译：公开了新的挥发性钡络合物，其在高温下非常稳定并蒸发干净。这种络合物非常适合用作OMCVD工艺中的钡源。

2. 发明授权

US5273775A Process for selectively depositing copper aluminum alloy onto a substrate 失效
标题翻译：将铜铝合金选择性沉积到基底上的工艺
公开(公告)号：US5273775A
公开(公告)日：1993-12-28
申请号：US867599
申请日：1992-04-13
申请人： Paul N. Dyer , Stephen M. Fine , John A. T. Norman
发明人： Paul N. Dyer , Stephen M. Fine , John A. T. Norman
IPC分类号： C23C16/02 , C23C14/16 , C23C16/04 , C23C16/18 , C23C16/20 , H01L21/285 , H01L21/3205 , C23C16/00
CPC分类号： H01L21/32051 , C23C14/16 , C23C16/04 , C23C16/18 , C23C16/20 , H01L21/28562
摘要： An improved method is provided for depositing a thin copper aluminum alloy film on a patterned silicon substrate. A copper base layer conforming to the existing pattern is initially formed on the surface of the substrate, followed by contact with vapors of an aminealane compound, which causes aluminum to be selectively deposited on the copper base layer portion of the substrate. Preferably, copper is applied to a diffusion barrier surface such as tungsten using chemical vapor deposition from a complex of copper (I) perfluoroalkyl-.beta.-diketonate and an olefin or silylolefin. The entire process of developing an alloy film can be carried out without exceeding 200.degree. C.
摘要翻译：提供了一种改进的方法，用于在图案化的硅衬底上沉积薄的铜铝合金膜。最初在衬底的表面上形成符合现有图案的铜基底层，然后与胺铝化合物的蒸气接触，这导致铝被选择性地沉积在基底的铜基底层部分上。优选地，使用化学气相沉积从铜（I）全氟烷基-β-二酮络合物和烯烃或甲硅烷基烯烃复合物将铜施加到扩散阻挡表面，例如钨。开发合金膜的整个过程可以不超过200℃进行。

3. 发明授权

US5098516A Processes for the chemical vapor deposition of copper and etching of copper 失效
标题翻译：铜的化学气相沉积和铜蚀刻的工艺
公开(公告)号：US5098516A
公开(公告)日：1992-03-24
申请号：US636316
申请日：1990-12-31
申请人： John A. T. Norman , Paul N. Dyer
发明人： John A. T. Norman , Paul N. Dyer
IPC分类号： C07F1/08 , C07C13/263 , C07C45/00 , C07C49/92 , C07F1/00 , C23C16/06 , C23C16/18 , C23F1/12 , H01L21/285 , H01L21/3213 , H01L21/768
CPC分类号： H01L21/32136 , C07F1/005 , C23C16/18 , C23F1/12 , H01L21/28562 , H01L21/76879
摘要： A process is provided for selectively depositing copper films on metallic or other electrically conducting portions of substrate surfaces by contacting the substrate at a temperature from 110.degree. to 190.degree. C. with a volatile organometallic copper complex, in the gas phase, represented by the structural formula: ##STR1## wherein R.sup.1 and R.sup.3 are each independently C.sub.1 -C.sub.8 perfluoroalkyl, R.sup.2 is H or C.sub.1 -C.sub.8 perfluoroalkyl and L is carbon monoxide, an isonitrile, or an unsaturated hydrocarbon ligand containing at least one non-aromatic unsaturation.

4. 发明授权

US5277987A High hardness fine grained beta tungsten carbide 失效
标题翻译：高硬度细粒度β碳化钨
公开(公告)号：US5277987A
公开(公告)日：1994-01-11
申请号：US649647
申请日：1991-02-01
申请人： Diwakar Garg , Paul N. Dyer , Robert E. Stevens , Christopher Ceccarelli
发明人： Diwakar Garg , Paul N. Dyer , Robert E. Stevens , Christopher Ceccarelli
IPC分类号： C04B41/50 , C04B41/52 , C04B41/87 , C04B41/89 , C23C16/14 , C23C16/32 , C23C30/00 , B05B15/04
CPC分类号： C04B41/009 , C04B41/5057 , C04B41/52 , C04B41/87 , C04B41/89 , C23C16/14 , C23C16/32 , C23C30/00 , Y10T428/31678
摘要： An extremely hard, fine grained tungsten carbide produced by thermochemical deposition is described. The tungsten carbide consists primarily of substantially pure tungsten carbide wherein the tungsten carbide consists of WC.sub.1-x, where x is 0 to about 0.4. The disclosed tungsten carbide is free of columnar grains and consists essentially of extremely fine, equiaxial crystals. Also disclosed is a method of producing the disclosed material.
摘要翻译：描述了通过热化学沉积产生的极硬的细晶碳化钨。碳化钨主要由基本上纯的碳化钨组成，其中碳化钨由WC1-x组成，其中x为0至约0.4。所公开的碳化钨不含柱状晶粒，并且基本上由极细的等轴晶体组成。还公开了制造所公开的材料的方法。

5. 发明授权

US5261932A Process for recovering oxygen from gaseous mixtures containing water or carbon dioxide which process employs ion transport membranes 失效
标题翻译：从含有水或二氧化碳的气态混合物中回收氧气的方法，该方法采用离子迁移膜
公开(公告)号：US5261932A
公开(公告)日：1993-11-16
申请号：US937767
申请日：1992-09-01
申请人： Michael F. Carolan , Paul N. Dyer , James M. LaBar, Sr. , Robert M. Thorogood
发明人： Michael F. Carolan , Paul N. Dyer , James M. LaBar, Sr. , Robert M. Thorogood
IPC分类号： B01D53/32 , B01D71/02 , C01B13/02 , C01B13/08 , B01D53/22
CPC分类号： C01B13/0255 , B01D53/326 , B01D71/024 , C01B2210/0051 , C01B2210/0062 , C01B2210/007 , Y10S505/701 , Y10S505/778 , Y10S505/785
摘要： The invention is a process for recovering oxygen from an oxygen-containing gaseous mixture containing one or more components selected from water, carbon dioxide or a volatile hydrocarbon which process utilizes ion transport membranes comprising a multicomponent metallic oxide containing strontium, calcium or magnesium. The process utilizes a temperature regime which overcomes problems associated with degradation of strontium-, calcium- and magnesium-containing multicomponent oxides caused by carbon dioxide.
摘要翻译：本发明是从含有一种或多种选自水，二氧化碳或挥发性烃的组分的含氧气体混合物中回收氧气的方法，该方法利用了包含含锶，钙或镁的多组分金属氧化物的离子迁移膜。该方法利用了克服由二氧化碳引起的含锶，钙和镁的多组分氧化物降解相关问题的温度状态。

6. 发明授权

US5147687A Hot filament CVD of thick, adherent and coherent polycrystalline diamond films 失效
标题翻译：厚丝，粘附和相干多晶金刚石薄膜的热丝CVD
公开(公告)号：US5147687A
公开(公告)日：1992-09-15
申请号：US707984
申请日：1991-05-22
申请人： Diwakar Garg , Sui-Yuan Lynn , Robert L. Iampietro , Ernest L. Wrecsics , Paul N. Dyer
发明人： Diwakar Garg , Sui-Yuan Lynn , Robert L. Iampietro , Ernest L. Wrecsics , Paul N. Dyer
IPC分类号： C23C16/27 , C23C16/54
CPC分类号： C23C16/54 , C23C16/271 , C23C16/279 , Y10T428/30
摘要： A thick, adherent and coherent polycrystalline diamond (PCD) coated substrate product is disclosed which comprises either a metallic or ceramic substrate and a plurality of separately deposited PCD layers of substantially uniform microstructure and having high electrical resistivity. The method for depositing multi-layers of PCD film onto the substrate comprises chemically depositing at least two separate polycrystalline diamond layers onto the substrate deposition conditions which are substantially different between cycles. The method enables one to deposit PCD films having a thickness of at least 12 microns for applications on flat as well as curved substrates having wide use in the electronics industry. Thick PCT films of this invention have been found to be ideal for dissipating heat from radio frequency (RF) and microwave (MW) devices.
摘要翻译：公开了一种厚的，粘附和一致的多晶金刚石（PCD）涂覆的基底产品，其包括金属或陶瓷基底和多个基本上均匀的微结构并且具有高电阻率的单独沉积的PCD层。将多层PCD膜沉积到衬底上的方法包括将至少两个单独的多晶金刚石层化学沉积到在循环之间基本不同的衬底沉积条件上。该方法使得能够沉积具有至少12微米厚度的PCD膜用于在电子工业中广泛使用的平面以及弯曲基板上的应用。已经发现本发明的PCT薄膜对于从射频（RF）和微波（MW）装置中散热是理想的。

7. 发明授权

US4619910A Catalyst for selective conversion of synthesis gas and method of making the catalyst 失效
标题翻译：用于选择性转化合成气的催化剂和制备催化剂的方法
公开(公告)号：US4619910A
公开(公告)日：1986-10-28
申请号：US741403
申请日：1985-06-05
申请人： Paul N. Dyer , Ronald Pierantozzi
发明人： Paul N. Dyer , Ronald Pierantozzi
IPC分类号： B01J23/46 , B01J23/74 , B01J37/00 , B01J37/02 , C07C1/04 , C07C1/06 , B01J21/04 , B01J21/06
CPC分类号： B01J23/74 , B01J23/462 , B01J37/0203 , B01J37/0207 , C07C1/063 , C07C2521/04 , C07C2531/12 , C07C2531/20
摘要： A Fischer-Tropsch (F-T) catalyst, a method of making the catalyst and an F-T process utilizing the catalyst by which synthesis gas, particularly carbon-monoxide rich synthesis gas is selectively converted to higher hydrocarbons of relatively narrow carbon number range. In general, the selective and notably stable catalyst, consists of an inert carrier first treated with a Group IV B metal compound (such as zirconium or titanium), preferably an alkoxide compound, and subsequently treated with an organic compound of an F-T metal catalyst, such as cobalt, iron or ruthenium carbonyl. Reactions with air and water and calcination are specifically avoided in the catalyst preparation procedure.
摘要翻译：费 - 托（F-T）催化剂，制备催化剂的方法和利用催化剂的F-T方法，其中合成气，特别是一氧化碳浓度合成气选择性地转化为碳数范围相对较窄的高级烃。通常，选择性和特别稳定的催化剂由首先用ⅣB族金属化合物（例如锆或钛），优选醇盐化合物处理的惰性载体组成，随后用FT金属催化剂的有机化合物处理，例如钴，铁或羰基钌。在催化剂制备过程中特别避免了与空气和水的反应和煅烧。

8. 发明授权

US4336240A Method of manufacturing hydrogen peroxide 失效
标题翻译：制造过氧化氢的方法
公开(公告)号：US4336240A
公开(公告)日：1982-06-22
申请号：US256438
申请日：1981-04-22
申请人： Fred Moseley , Paul N. Dyer
发明人： Fred Moseley , Paul N. Dyer
IPC分类号： C01B15/029 , C01B15/02
CPC分类号： C01B15/029
摘要： A process for producing hydrogen peroxide wherein a gaseous mixture comprising hydrogen and oxygen is contacted with a catalyst in the presence of water and an organic solvent wherein:(i) the organic solvent is immiscible with water and unreactive with hydrogen peroxide under the contacting conditions;(ii) the distribution coefficient for hydrogen peroxide between the water and the organic solvent is greater than 1;(iii) the catalyst is of the formula L.sub.2 MX.sub.2 wherein L is a ligand represented by the formula A R.sub.1 R.sub.2 R.sub.3 wherein R.sub.1 R.sub.2 and R.sub.3 are alkyl, cycloalkyl or aryl groups, hydrogen or halogen, A is a Group 5b element selected from the group consisting of nitrogen, phosphorous and arsenic, M is a Group 8 metal and X is halogen, said catalyst being soluble in said organic solvent and insoluble in water; and(iv) the gaseous mixture is non-ignitable under the process conditionscharacterized in that the organic solvent is selected from the group consisting of fluorocarbons, halofluorocarbons and mixtures thereof.
摘要翻译：一种生产过氧化氢的方法，其中包含氢气和氧气的气体混合物在水和有机溶剂存在下与催化剂接触，其中：（i）有机溶剂与水不混溶，在接触条件下与过氧化氢不反应; （ii）水和有机溶剂之间的过氧化氢分配系数大于1; （iii）催化剂具有式L2MX2，其中L是由式A R1R2 R3表示的配体，其中R1R2和R3是烷基，环烷基或芳基，氢或卤素，A是选自组中的第5b族元素由氮，磷和砷组成，M是第8族金属，X是卤素，所述催化剂可溶于所述有机溶剂并且不溶于水; 和（iv）在工艺条件下气态混合物是不可燃的，其特征在于有机溶剂选自碳氟化合物，卤代氟烃及其混合物。

9. 发明授权

US4128627A Synthesis of hydrogen peroxide 失效
标题翻译：合成过氧化氢
公开(公告)号：US4128627A
公开(公告)日：1978-12-05
申请号：US774577
申请日：1977-03-04
申请人： Paul N. Dyer , Fred Moseley
发明人： Paul N. Dyer , Fred Moseley
IPC分类号： B01J31/16 , B01J31/18 , B01J31/24 , C01B15/029 , C01B15/02
CPC分类号： C01B15/029 , B01J31/1895 , B01J31/2404 , B01J2531/824
摘要： Hydrogen peroxide is synthesized by reacting hydrogen and oxygen in a two phase mixture of water and an organic. The mixture contains a catalyst which is insoluble in water but dissolves in the organic. The hydrogen peroxide is extracted in the water.The catalyst is L.sub.2 MX.sub.2 where:L is a ligand containing a Group 5b element (preferably phosphorous);M is a Group 8 metal (preferably palladium); andX is a halogen (preferably chlorine).
摘要翻译：过氧化氢通过氢和氧在水和有机物的两相混合物中反应来合成。该混合物含有不溶于水但溶于有机物的催化剂。过氧化氢在水中提取。

10. 发明授权

US5599383A Tubular solid-state membrane module 失效
标题翻译：管状固态膜组件
公开(公告)号：US5599383A
公开(公告)日：1997-02-04
申请号：US403050
申请日：1995-03-13
申请人： Paul N. Dyer , Jeffrey D. Bright , Michael F. Carolan , Eric Minford , Robin E. Richards , Steven L. Russek , Dale M. Taylor , Merrill A. Wilson
发明人： Paul N. Dyer , Jeffrey D. Bright , Michael F. Carolan , Eric Minford , Robin E. Richards , Steven L. Russek , Dale M. Taylor , Merrill A. Wilson
IPC分类号： B01D53/22 , C01B13/02 , B01D63/06 , B01D71/02
CPC分类号： B01D53/22 , B01D53/228 , B01D63/06 , B28B1/008 , B28B19/0053 , C01B13/0251 , C01B13/0255 , C04B35/01 , C04B35/2633 , C04B35/2641 , C04B35/6262 , C04B37/025 , C04B37/026 , C04B38/0003 , B01D2313/42 , B01D2319/02 , B29L2023/00 , C01B2210/0046 , C04B2111/00801 , C04B2235/3215 , C04B2235/3227 , C04B2235/3272 , C04B2235/3275 , C04B2235/3281 , C04B2235/6021 , C04B2235/6025 , C04B2235/6027 , C04B2235/768 , C04B2235/96 , C04B2237/10 , C04B2237/12 , C04B2237/34 , C04B2237/405 , C04B2237/76
摘要： Tubular solid-state membrane modules for separating oxygen from an oxygen-containing gaseous mixture which provide improved pneumatic and structural integrity and ease of manifolding. The modules are formed from a plurality of tubular membrane units, each membrane unit which comprises a channel-free porous support having connected through porosity which is in contact with a contiguous dense mixed conducting oxide layer having no connected through porosity. The dense mixed conducting oxide layer is placed in flow communication with the oxygen-containing gaseous mixture to be separated and the channel-free porous support of each membrane unit is placed in flow communication with one or more manifolds or conduits for discharging oxygen which has been separated from the oxygen-containing gaseous mixture by permeation through the dense mixed conducting oxide layer of each membrane unit and passage into the manifolds or conduits via the channel-free porous support of each membrane unit.
摘要翻译：用于从含氧气体混合物中分离氧的管状固态膜组件，其提供改善的气动和结构完整性以及易于歧管。模块由多个管状膜单元形成，每个膜单元包括无通孔的多孔载体，该多孔载体通过孔隙率连接，该多孔载体与没有连通孔隙的连续密集的混合导电氧化物层接触。密集混合的导电氧化物层与要分离的含氧气体混合物流动连通，并且每个膜单元的无通道多孔载体被放置成与一个或多个歧管或导管连通，用于排出氧气通过渗透通过每个膜单元的致密混合导电氧化物层并从每个膜单元的无通道多孔载体通入歧管或管道而与含氧气体混合物分离。

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