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1. 发明申请

US20080207901A1 Process for the Preparation of Pulverulent Alkoxycarbonylaminotriazine 有权
标题翻译：制备粉末状烷氧基氨基三嗪的方法
公开(公告)号：US20080207901A1
公开(公告)日：2008-08-28
申请号：US11916747
申请日：2006-05-31
申请人： Joerg Schneider , Gunter Scherr , Rainer Erhardt , Andreas Eichfelder , Martin Reif , Stefan Hirsch , Georg Sieder , Thomas Holtmann , Jurgen Ciprian , Hermann Ascherl
发明人： Joerg Schneider , Gunter Scherr , Rainer Erhardt , Andreas Eichfelder , Martin Reif , Stefan Hirsch , Georg Sieder , Thomas Holtmann , Jurgen Ciprian , Hermann Ascherl
IPC分类号： C07D251/48
CPC分类号： C07D251/70
摘要： The invention relates to a process for preparing free-flowing, pulverulent alkoxycarbonylaminotriazine from an alkanolic reaction mixture which is obtained in the preparation of alkoxycarbonylaminotriazines and comprises at least one alkoxycarbonylaminotriazine, at least one cyclic and/or acyclic carbonic ester, at least one C1-C13-alkanol which optionally comprises one or two oxygen atoms in the form of ether bonds and is optionally substituted by C1-C4-alkyl and/or hydroxyl, and also at least one alkali metal or alkaline earth metal alkoxide, with or without melamine and with or without catalyst, by atomizing and drying the reaction mixture in a spray drier.
摘要翻译：本发明涉及一种从烷醇反应混合物中制备自由流动的粉末状烷氧基羰基氨基三嗪的方法，其在制备烷氧基羰基氨基三嗪时得到，并且包含至少一种烷氧基羰基氨基三嗪，至少一种环状和/或非环状碳酸酯，其任选地包含一个或两个醚键形式的氧原子，并且任选地被C 1 -C 3烷基取代，亚烷基和/或羟基，以及至少一种碱金属或碱土金属醇盐，具有或不具有三聚氰胺和有或没有催化剂，通过在喷雾干燥器中雾化和干燥反应混合物。

2. 发明申请

US20080306261A1 Process For Treating a Reaction Mixture Comprising Alkoxycarbonylaminotriazine 审中-公开
标题翻译：用于处理包含烷氧基氨基三嗪的反应混合物的方法
公开(公告)号：US20080306261A1
公开(公告)日：2008-12-11
申请号：US11916626
申请日：2006-06-02
申请人： Jörg Schneider , Gunter Scherr , Rainer Erhardt , Andreas Eichfelder , Martin Reif , Stefan Hirsch , Georg Sieder , Thomas Holtmann , Jurgen Ciprian , Hermann Ascherl
发明人： Jörg Schneider , Gunter Scherr , Rainer Erhardt , Andreas Eichfelder , Martin Reif , Stefan Hirsch , Georg Sieder , Thomas Holtmann , Jurgen Ciprian , Hermann Ascherl
IPC分类号： C07D251/48
CPC分类号： C07D251/70
摘要： Processes comprising: providing an alkanolic reaction mixture, the alkanolic reaction mixture comprising: at least one alkoxycarbonylaminotriazine; at least one carbonic ester; at least one C1-C13-alkanol, which alkanol may further comprise up to two ether-bound oxygen atoms and may further comprise a substituent selected from the group consisting of C1-C4-alkyls and hydroxyls; and at least one alkali metal alkoxide or alkaline earth metal alkoxide; and subjecting the alkanolic reaction mixture to extraction with a polar extractant such that at least a portion of polar/ionic components present in the reaction mixture are removed, wherein the polar extractant is less than entirely miscible with an organic phase of the reaction mixture, to form an alkanolic phase comprising the at least one alkoxycarbonylaminotriazine and a polar phase comprising the polar extractant and the portion of polar/ionic components; and wherein the extraction is carried out with one or more selected from the group consisting of mixer/settler units, columns, centrifugal field separation extractors, and combinations thereof.
摘要翻译：方法包括：提供烷醇反应混合物，所述链烷醇反应混合物包含：至少一种烷氧基羰基氨基三嗪; 至少一个碳酸酯; 至少一种C1-C13-链烷醇，该链烷醇还可包含至多两个醚结合的氧原子，并且还可包含选自C 1 -C 4 - 烷基和羟基的取代基; 和至少一种碱金属醇盐或碱土金属醇盐; 并用极性萃取剂对链烷醇反应混合物进行萃取，使得除去反应混合物中存在的至少一部分极性/离子组分，其中极性萃取剂与反应混合物的有机相完全混溶，至形成包含至少一种烷氧基羰基氨基三嗪和极性相的链烷醇相，所述极性相包含极性萃取剂和部分极性/离子组分; 并且其中所述萃取用选自混合器/沉降器单元，塔，离心场分离提取器及其组合的一种或多种进行。

3. 发明申请

US20080275236A1 Method For Removing Salts From A Reaction Mixture Containing Alkoxycarbonyl Amino Triazine 审中-公开
标题翻译：从含有烷氧基羰基氨基三嗪的反应混合物中除去盐的方法
公开(公告)号：US20080275236A1
公开(公告)日：2008-11-06
申请号：US11916564
申请日：2006-06-01
申请人： Jorg Schneider , Gunter Scherr , Rainer Erhardt , Andreas Eichfelder , Martin Reif , Stefan Hirsch , Georg Sieder , Thomas Holtmann , Juergen Ciprian , Hermann Ascherl
发明人： Jorg Schneider , Gunter Scherr , Rainer Erhardt , Andreas Eichfelder , Martin Reif , Stefan Hirsch , Georg Sieder , Thomas Holtmann , Juergen Ciprian , Hermann Ascherl
IPC分类号： C07D251/00
CPC分类号： C07D251/70 , C07D251/50 , C07D251/52
摘要： The invention relates to a process for removing salts from an alkanolic reaction mixture which is obtained in the preparation of alkoxycarbonylaminotriazines and comprises at least one alkoxycarbonylaminotriazine, at least one cyclic and/or acyclic carbonic ester, at least one C1-C13-alkanol which optionally comprises one or two oxygen atoms as ether bonds and is optionally substituted by C1-C4-alkyl and/or hydroxyl, and also at least one alkali metal alkoxide or alkaline earth metal alkoxide, with or without melamine and with or without catalyst, in which salts are removed from the reaction mixture by ion exchange over a cation exchanger and/or anion exchanger.
摘要翻译：本发明涉及一种从链烷醇反应混合物中除去盐的方法，其在烷氧基羰基氨基三嗪的制备中得到，并且包含至少一种烷氧基羰基氨基三嗪，至少一种环状和/或非环状碳酸酯，至少一个C 1〜其任选地包含一个或两个氧原子作为醚键，并且任选被C 1 -C 4 - 烷基和/或羟基，以及至少一种碱金属醇盐或碱土金属醇盐，其具有或不具有三聚氰胺和有或无催化剂，其中通过在阳离子交换剂和/或阴离子上离子交换从反应混合物中除去盐交换机。

4. 发明授权

US08030485B2 Process for the preparation of pulverulent alkoxycarbonylaminotriazine 有权
标题翻译：制备粉状烷氧基羰基氨基三嗪的方法
公开(公告)号：US08030485B2
公开(公告)日：2011-10-04
申请号：US11916747
申请日：2006-05-31
申请人： Joerg Schneider , Guenter Scherr , Rainer Erhardt , Andreas Eichfelder , Martin Reif , Stefan Hirsch , Georg Sieder , Thomas Holtmann , Juergen Ciprian , Hermann Ascherl
发明人： Joerg Schneider , Guenter Scherr , Rainer Erhardt , Andreas Eichfelder , Martin Reif , Stefan Hirsch , Georg Sieder , Thomas Holtmann , Juergen Ciprian , Hermann Ascherl
IPC分类号： C07D251/70 , C07D251/50 , C07D251/48 , C07D251/18
CPC分类号： C07D251/70
摘要： The invention relates to a process for preparing free-flowing, pulverulent alkoxycarbonylaminotriazine from an alkanolic reaction mixture which is obtained in the preparation of alkoxycarbonylaminotriazines and comprises at least one alkoxycarbonylaminotriazine, at least one cyclic and/or acyclic carbonic ester, at least one C1-C13-alkanol which optionally comprises one or two oxygen atoms in the form of ether bonds and is optionally substituted by C1-C4-alkyl and/or hydroxyl, and also at least one alkali metal or alkaline earth metal alkoxide, with or without melamine and with or without catalyst, by atomizing and drying the reaction mixture in a spray drier.
摘要翻译：本发明涉及一种从烷醇反应混合物中制备自由流动的粉末状烷氧基羰基氨基三嗪的方法，其在制备烷氧基羰基氨基三嗪时得到，并且包含至少一种烷氧基羰基氨基三嗪，至少一种环状和/或无环碳酸酯，至少一个C1- 任选地包含一个或两个醚键形式的氧原子并且任选被C 1 -C 4 - 烷基和/或羟基取代的C 13 - 链烷醇，以及至少一种具有或不具有三聚氰胺的碱金属或碱土金属醇盐，以及具有或不具有催化剂，通过在喷雾干燥器中雾化和干燥反应混合物。

5. 发明申请

US20090121181A1 ETHERIFIED MELAMINE/FORMALDEHYDE CONDENSATES HAVING A HIGH SOLID CONTENT AND LOW VISCOSITY 有权
标题翻译：具有高固体含量和低粘度的乙烯/甲醛冷凝物
公开(公告)号：US20090121181A1
公开(公告)日：2009-05-14
申请号：US12096502
申请日：2006-12-07
申请人： Andreas Eichfelder , Rainer Erhardt , Martin Reif , Eva Ruba , Gunter Scherr , Jorg Schneider , Dieter Weilacher
发明人： Andreas Eichfelder , Rainer Erhardt , Martin Reif , Eva Ruba , Gunter Scherr , Jorg Schneider , Dieter Weilacher
IPC分类号： C09K3/00
CPC分类号： C08G12/427
摘要： Process for the preparation of etherified melamine/formaldehyde condensates, in which first a methylolation of melamine with a formaldehyde component in the molar ratio of from 1:6 to 1:15, preferably at a pH of >7, is carried out. This is followed by an etherification of the resulting hydroxymethylation intermediate in the presence of a C1-C20-alkyl, preferably of a C1-C6-alcohol, particularly preferably of a C1-C4-alcohol, at a pH of 9.5 being established before, during and/or after the distillation. According to the invention, a plurality of hydroxymethylation, etherification and distillation steps follow in order to achieve an etherified melamine/formaldehyde condensate which is distinguished by a high degree of hydroxymethylation, a high solids content and a low viscosity.
摘要翻译：用于制备醚化的三聚氰胺/甲醛缩合物的方法，其中首先以摩尔比为1:6至1:15，优选pH为> 7的三聚氰胺与甲醛组分的羟甲基化反应。然后在pH <4.5的情况下在所得羟甲基化中间体在C1-C20烷基，优选C1-C6醇，特别优选C1-C4-醇的存在下进行醚化，随后通过至少一个蒸馏步骤以从体系中除去特别是甲醇，在蒸馏之前，期间和/或之后建立pH> 9.5。根据本发明，为了实现醚化的三聚氰胺/甲醛缩合物，通过高度羟甲基化，高固体含量和低粘度来区分多个羟甲基化，醚化和蒸馏步骤。

6. 发明授权

US08034929B2 Continuous method for producing highly methylolated melamine and etherified melamine formaldehyde resins 有权
标题翻译：用于生产高度羟甲基化的三聚氰胺和醚化的三聚氰胺甲醛树脂的连续方法
公开(公告)号：US08034929B2
公开(公告)日：2011-10-11
申请号：US10586580
申请日：2005-01-13
申请人： Jörg Schneider , Günter Scherr , Rainer Erhardt , Andreas Eichfelder , Martin Reif , Stefan Hirsch , Hans Schupp , Christel Hittinger , Alain Robert
发明人： Jörg Schneider , Günter Scherr , Rainer Erhardt , Andreas Eichfelder , Martin Reif , Stefan Hirsch , Hans Schupp , Christel Hittinger , Alain Robert
IPC分类号： C07D251/64
CPC分类号： C07D251/64
摘要： The invention relates to a process for preparing polymethylolated melamine and polymethylolated melamine compounds polyetherified with alkanol, wherein the methylolation reaction is carried out in a kneading reactor.
摘要翻译：本发明涉及一种制备多羟基化三聚氰胺和用链烷醇多醚化的多羟甲基化三聚氰胺化合物的方法，其中甲基化反应在捏合反应器中进行。

7. 发明申请

US20100113693A1 Continuous method for producing highly methylolated melamine and etherified melamine formaldehyde resins 有权
标题翻译：用于生产高度羟甲基化的三聚氰胺和醚化的三聚氰胺甲醛树脂的连续方法
公开(公告)号：US20100113693A1
公开(公告)日：2010-05-06
申请号：US10586580
申请日：2005-01-13
申请人： Jörg Schneider , Günter Scherr , Rainer Erhardt , Andreas Eichfelder , Martin Reif , Stefan Hirsch , Hans Schupp , Christel Hittinger , Alain Robert
发明人： Jörg Schneider , Günter Scherr , Rainer Erhardt , Andreas Eichfelder , Martin Reif , Stefan Hirsch , Hans Schupp , Christel Hittinger , Alain Robert
IPC分类号： C08G8/28 , C08G12/32 , C08G63/91
CPC分类号： C07D251/64
摘要： The invention relates to a process for preparing polymethylolated melamine and polymethylolated melamine compounds polyetherified with alkanol, wherein the methylolation reaction is carried out in a kneading reactor.
摘要翻译：本发明涉及一种制备多羟基化三聚氰胺和用链烷醇多醚化的多羟甲基化三聚氰胺化合物的方法，其中甲基化反应在捏合反应器中进行。

8. 发明授权

US09039927B2 Etherified melamine/formaldehyde condensates having a high solid content and low viscosity 有权
标题翻译：具有高固体含量和低粘度的醚化三聚氰胺/甲醛缩合物
公开(公告)号：US09039927B2
公开(公告)日：2015-05-26
申请号：US12096502
申请日：2006-12-07
申请人： Andreas Eichfelder , Rainer Erhardt , Martin Reif , Eva Ruba , Günter Scherr , Jörg Schneider , Dieter Weilacher
发明人： Andreas Eichfelder , Rainer Erhardt , Martin Reif , Eva Ruba , Günter Scherr , Jörg Schneider , Dieter Weilacher
IPC分类号： C09K3/00 , C08F2/00 , C08G12/42
CPC分类号： C08G12/427
摘要： Process for the preparation of etherified melamine/formaldehyde condensates, in which first a methylolation of melamine with a formaldehyde component in the molar ratio of from 1:6 to 1:15, preferably at a pH of >7, is carried out. This is followed by an etherification of the resulting hydroxymethylation intermediate in the presence of a C1-C20-alkyl, preferably of a C1-C6-alcohol, particularly preferably of a C1-C4-alcohol, at a pH of 9.5 being established before, during and/or after the distillation. According to the invention, a plurality of hydroxymethylation, etherification and distillation steps follow in order to achieve an etherified melamine/formaldehyde condensate which is distinguished by a high degree of hydroxymethylation, a high solids content and a low viscosity.
摘要翻译：用于制备醚化的三聚氰胺/甲醛缩合物的方法，其中首先以摩尔比为1:6至1:15，优选pH为> 7的三聚氰胺与甲醛组分的羟甲基化反应。然后在pH <4.5的情况下在所得羟甲基化中间体在C1-C20烷基，优选C1-C6醇，特别优选C1-C4-醇的存在下进行醚化，随后通过至少一个蒸馏步骤以从体系中除去特别是甲醇，在蒸馏之前，期间和/或之后建立pH> 9.5。根据本发明，为了实现醚化的三聚氰胺/甲醛缩合物，通过高度羟甲基化，高固体含量和低粘度来区分多个羟甲基化，醚化和蒸馏步骤。

9. 发明申请

US20050043479A1 Preparation of polysiloxane-containing compositions and their use for imparting water repellency to or refatting materials having a fibrous structure 审中-公开
标题翻译：制备含聚硅氧烷的组合物及其对具有纤维结构的材料赋予拒水性或改性材料的用途
公开(公告)号：US20050043479A1
公开(公告)日：2005-02-24
申请号：US10909286
申请日：2004-08-03
申请人： Rainer Erhardt , Gunter Scherr , Gunther Pabst , Ralph Lunkwitz
发明人： Rainer Erhardt , Gunter Scherr , Gunther Pabst , Ralph Lunkwitz
IPC分类号： C08L83/08 , C09D183/08 , C14C11/00 , D06M15/643
CPC分类号： C14C11/003 , C08L83/08 , C09D183/08 , D06M15/643 , D06M2200/12
摘要： Compositions comprising the following components: (A) at least one carboxyl-containing polysiloxane which has at least one structural element of the formula Ia, Ib or Ic per molecule, (B1) at least one aprotic substance which is liquid at room temperature or (B2) at least one organic solvent, (C) up to 2% by weight, based on the weight of the composition, of water, the variables being defined as follows: R1 is hydrogen, hydroxyl, C1-C6-alkyl, C6-C14-aryl or C1-C4-alkoxy, R2 is hydrogen or C1-C6-alkyl, Z1 is C2-C25-alkylene, C3-C10-cycloalkylene, C6-C14-arylene, —[(CH2)n—NR2—(CH2)m]p, n and m are integers which are identical or different and are from 1 to 10, p is an integer from 1 to 5, A1 is C2-C20-alkylene, unsubstituted or substituted by R3 and/or R4, —CH═CR3—, R3 and R4 are identical or different and are selected from hydrogen, C1-C20-alkyl, C2-C20-alkenyl, C6-C14-aryl and C1-C4-alkoxy; it being possible for R3 and R4 to be linked to one another with formation of a mono- or bicyclic system, M are identical or different and are selected from hydrogen, alkali metal and ammonium, which may be substituted or cyclic, are prepared by a process wherein at least one amino-containing polysiloxane which has at least one structural element of the formula IIa, IIb or IIc per molecule is reacted, in the presence or absence of component (B1), with at least one dicarboxylic anhydride of the formula IIIa or at least one dicarboxylic acid derivative of the formula IIIb X being a leaving group and Z2 being C2-C25-alkylene, C3-C10-cycloalkylene, C6-C14-arylene or —[(CH2)n—NR2—(CH2)m]p, and then, if required, component (B1) or (B2) is added.
摘要翻译：包含以下组分的组合物：（A）至少一种含有羧基的聚硅氧烷，其每分子具有至少一个式Ia，Ib或Ic的结构元件，（B1）至少一种在室温下为液体的非质子性物质（或 B2）至少一种有机溶剂，（C）至多2重量％，基于组合物的重量，水，变量定义如下：R 1是氢，羟基，C 1 -C 6 - 烷基，C 6 -C 14 - 芳基或C 1 -C 4 - 烷氧基，R 2是氢或C 1 -C 6烷基，Z 1是C 2 -C 25 - 亚烷基，C 3 -C 10 - 亚环烷基，C 6 -C 14 - 亚芳基 - [（CH 2）n -NR 2 - （CH 2）m] p，n和m是相同或不同且为1至10的整数，p为1至5的整数，A 1为C 2 未取代或被R 3和/或R 4取代的-C 20 - 亚烷基，-CH = CR 3 - ，R 3和R 4相同或不同，并且选自氢，C1 C 20 - 烷基，C 2 -C 20 - 烯基，C 6 -C 14 - 芳基和C 1 -C 4 - 烷氧基; R 3和R 4可以彼此连接形成单环或双环体系，M相同或不同，并且可以选自氢，碱金属和铵，其可被取代或通过一种方法制备，其中至少一种含有至少一种分子式IIa，IIb或IIc结构元件的含氨基聚硅氧烷在组分（B1）存在或不存在下与至少一种二羧酸酐或式IIIb的至少一种二羧酸衍生物，其为离去基团，Z 2为C 2 -C 25 - 亚烷基，C 3 -C 10 - 亚环烷基，C 6 -C 14 - 亚芳基或 - [（CH 2））n-NR <

10. 发明授权

US07517474B2 Carbamate-functional triazine derivatives 有权
标题翻译：氨基甲酸酯官能的三嗪衍生物
公开(公告)号：US07517474B2
公开(公告)日：2009-04-14
申请号：US11547476
申请日：2005-04-08
申请人： Eva Wagner , Reinhold Schwalm , Joerg Schneider , Rainer Erhardt , Carl Jokisch , Heinz-Peter Rink
发明人： Eva Wagner , Reinhold Schwalm , Joerg Schneider , Rainer Erhardt , Carl Jokisch , Heinz-Peter Rink
IPC分类号： C07D251/54 , C07D251/70 , C09D175/04
CPC分类号： C07D251/54
摘要： New triazine derivatives containing carbamate groups, processes for preparing them, and their use.
摘要翻译：含有氨基甲酸酯基团的新型三嗪衍生物，其制备方法及其用途。

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