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1. 发明授权

US07351310B2 Rectificative separation of fluids comprising (meth) acrylic monomers 有权
标题翻译：包含（甲基）丙烯酸单体的流体的精馏分离
公开(公告)号：US07351310B2
公开(公告)日：2008-04-01
申请号：US10658257
申请日：2003-09-10
申请人： Joachim Thiel , Albrecht Dams , Juergen Schroeder
发明人： Joachim Thiel , Albrecht Dams , Juergen Schroeder
IPC分类号： B01D3/34 , B01D5/00 , C07C51/42
CPC分类号： C07C51/44 , B01D3/14 , B01D5/0063 , C07C45/81 , C07C45/82 , C07C51/43 , C07C67/54 , Y10S203/22 , C07C47/22 , C07C57/04 , C07C69/54
摘要： A process for rectificatively separating fluids including (meth)acrylic monomers in a rectification column by directly cooling the vapor including (meth)acrylic monomers rising to the top of the rectification column to form top condensate including (meth)acrylic monomers, the condensation space at the top of the column being separated from the region of the rectification column containing the separating internals only by at least one chimney tray from which the top condensate formed is removed from the rectification column, which includes effecting the direct cooling of the vapor in the condensation space in at least two spray zones which are spatially successive and are flowed through by vapor by spraying supercooled top condensate including added polymerization inhibitor, and the temperature of the sprayed supercooled top condensate becoming lower from spray zone to spray zone in the flown direction of the vapor.
摘要翻译：通过将上升到精馏塔顶部的（甲基）丙烯酸单体直接冷却的蒸汽直接冷却，形成精馏塔中的（甲基）丙烯酸单体，形成包含（甲基）丙烯酸单体的顶部缩合物，柱的顶部仅由至少一个烟囱式塔板从含有分离内部件的精馏塔的区域分离出，从该澄清塔中形成的顶部冷凝物从精馏塔从精馏塔排出，其中包括直接冷却冷凝物中的蒸气至少两个喷雾区的空间，其空间连续并通过喷雾通过喷雾过冷顶部冷凝物（包括加入的阻聚剂）而流过，并且喷射的过冷顶部冷凝物的温度从喷射区域向喷雾区域的流动方向变低汽。

2. 发明授权

US07279075B2 Thermal separating process between at least one gaseous and at least one liquid stream, of which at least one comprises (meth)acrylic monomers 有权
标题翻译：至少一种气态和至少一种液体物流之间的热分离过程，其中至少一种液体物流包含（甲基）丙烯酸单体
公开(公告)号：US07279075B2
公开(公告)日：2007-10-09
申请号：US10647241
申请日：2003-08-26
申请人： Joachim Thiel , Hugues Vandenmersch , Juergen Schroeder , Albrecht Dams
发明人： Joachim Thiel , Hugues Vandenmersch , Juergen Schroeder , Albrecht Dams
IPC分类号： B01D3/42 , C07C51/42
CPC分类号： C07C51/44 , C07C45/783 , C07C45/81 , C07C45/82 , C07C67/54 , Y10S203/11 , C07C57/04 , C07C69/54
摘要： In a thermal separating process between at least one gaseous and at least one liquid stream, of which at least one comprises (meth)acrylic monomers, in a separating column containing sieve trays as separating internals, at least some of the sieve trays are operated above an entrainment fraction of 10% by weight.
摘要翻译：在至少一种气态和至少一种液态物流之间的热分离过程中，至少一种液体物流在至少一种包含（甲基）丙烯酸类单体的分离塔中，该分离塔含有作为分离内部物质的筛板，至少一些筛板在上面操作 10％重量的夹带部分。

3. 发明授权

US07393436B2 Thermal separating process for removing at least one stream containing enriched (meth) acrylic monomers 有权
标题翻译：用于除去至少一种含有富含（甲基）丙烯酸单体的物流的热分离方法
公开(公告)号：US07393436B2
公开(公告)日：2008-07-01
申请号：US10888933
申请日：2004-07-12
申请人： Bernd Eck , Ulrich Hammon , Klaus Joachim Mueller-Engel , Juergen Schroeder , Joachim Thiel , Hans Martan
发明人： Bernd Eck , Ulrich Hammon , Klaus Joachim Mueller-Engel , Juergen Schroeder , Joachim Thiel , Hans Martan
IPC分类号： B01D3/14 , B01D3/42 , C07C51/43
CPC分类号： C07C51/43 , B01D3/14 , B01D3/225 , B01D3/322 , C07C51/215 , C07C51/252 , C07C51/44 , Y10S203/22 , C07C57/04
摘要： A thermal separating process for removing a stream containing enriched (meth)acrylic monomers from a mixture containing (meth)acrylic monomers, in which the liquid phases retained in the separating space at high temperature and high (meth)acrylic monomer content are minimized.
摘要翻译：一种用于从含有（甲基）丙烯酸单体的混合物中除去含有富含（甲基）丙烯酸单体的物流的热分离方法，其中在高温和高（甲基）丙烯酸单体含量保留在分离空间中的液相被最小化。

4. 发明申请

US20050090628A1 Thermal separating process for removing at least one stream containing enriched (meth) acrylic monomers 有权
标题翻译：用于除去至少一种含有富含（甲基）丙烯酸单体的物流的热分离方法
公开(公告)号：US20050090628A1
公开(公告)日：2005-04-28
申请号：US10888933
申请日：2004-07-12
申请人： Bernd Eck , Ulrich Hammon , Klaus Mueller-Engel , Juergen Schroeder , Joachim Thiel , Hans Martan
发明人： Bernd Eck , Ulrich Hammon , Klaus Mueller-Engel , Juergen Schroeder , Joachim Thiel , Hans Martan
IPC分类号： B01D3/14 , B01D3/32 , C07C51/215 , C07C51/25 , C07C51/43 , C07C51/44 , C08F2/00
CPC分类号： C07C51/43 , B01D3/14 , B01D3/225 , B01D3/322 , C07C51/215 , C07C51/252 , C07C51/44 , Y10S203/22 , C07C57/04
摘要： A thermal separating process for removing a stream containing enriched (meth)acrylic monomers from a mixture containing (meth)acrylic monomers, in which the liquid phases retained in the separating space at high temperature and high (meth)acrylic monomer content are minimized.
摘要翻译：一种用于从含有（甲基）丙烯酸单体的混合物中除去含有富含（甲基）丙烯酸单体的物流的热分离方法，其中在高温和高（甲基）丙烯酸单体含量保留在分离空间中的液相被最小化。

5. 发明授权

US07306204B2 Column comprising dual flow plates 有权
标题翻译：柱包括双流板
公开(公告)号：US07306204B2
公开(公告)日：2007-12-11
申请号：US10494032
申请日：2002-11-21
申请人： Joachim Thiel , Juergen Schroeder
发明人： Joachim Thiel , Juergen Schroeder
IPC分类号： B01F3/04
CPC分类号： B01D3/225 , B01D3/22
摘要： A column for the thermal treatment of mixtures which contain one or more polymerizable compounds is proposed, which column has dual-flow trays with openings whose diameter is constant within a dual-flow tray, the dual-flow trays having openings of decreasing diameter with increasing distance from the feed of the mixture to be treated.
摘要翻译：提出了一种用于热处理含有一种或多种可聚合化合物的混合物的柱，该柱具有双流塔板，其双向流动塔板具有在双流托盘内直径不变的开口，双流托盘具有随着直径减小的开口而增加距离要处理的混合物的进料。

6. 发明授权

US07109374B2 Method for the continuous extraction of (meth)acrylic acid 失效
标题翻译：连续萃取（甲基）丙烯酸的方法
公开(公告)号：US07109374B2
公开(公告)日：2006-09-19
申请号：US10473102
申请日：2002-03-28
申请人： Otto Machhammer , Christoph Adami , Claus Hechler , Juergen Schroeder , Volker Schliephake , Joachim Thiel , Volker Diehl
发明人： Otto Machhammer , Christoph Adami , Claus Hechler , Juergen Schroeder , Volker Schliephake , Joachim Thiel , Volker Diehl
IPC分类号： C07C51/42
CPC分类号： C07C51/44 , B01D3/225 , C07C51/48 , C07C57/04
摘要： A process for the continuous recovery of (meth)acrylic acid from the reaction gas of a catalytic gas-phase oxidation comprising the following process stages is proposed: I quenching of the reaction gas by evaporative cooling using a high-boiling solvent, II separation of the (meth)acrylic acid from the quenched reaction gas by absorption into the high-boiling solvent, III separation of the solvent laden with (meth)acrylic acid by rectification into a first part-stream IIIA), which contains predominantly (meth)acrylic acid, and into a second part-stream IIIB) which contains predominantly the solvent, IV recycling of the stream IIIB) to process stage II and V distillative production of (meth)acrylic acid from stream IIIA), all liquid residual streams obtained in process stage V being recycled to process stage I.
摘要翻译：提出了从包括以下工艺步骤的催化气相氧化反应气体连续回收（甲基）丙烯酸的方法：I通过使用高沸点溶剂的蒸发冷却来淬灭反应气体，II分离（甲基）丙烯酸通过吸收进入高沸点溶剂从淬灭的反应气体中分离，III分离含有（甲基）丙烯酸的溶剂通过精馏分离成第一部分流IIIA），其主要含有（甲基）丙烯酸酸，并且进入第二部分流IIIB），其主要包含溶剂，IVB流的再循环），以处理从流IIIA进行的步骤II和V蒸馏生产（甲基）丙烯酸），所有在过程中获得的液体残余流第五阶段被回收到处理阶段I.

7. 发明授权

US07520964B2 Method for the rectifying separation of fluids containing (meth)acryl monomers 有权
标题翻译：含有（甲基）丙烯酸单体的流体的精馏分离方法
公开(公告)号：US07520964B2
公开(公告)日：2009-04-21
申请号：US10515639
申请日：2003-07-02
申请人： Ulrich Hammon , Joachim Thiel , Volker Schliephake , Juergen Schroeder
发明人： Ulrich Hammon , Joachim Thiel , Volker Schliephake , Juergen Schroeder
IPC分类号： B01D3/22 , B01D3/32
CPC分类号： B01D3/22 , B01D3/225 , C07C51/44 , Y10S203/11 , Y10S203/22 , C07C57/04
摘要： A process for rectificatively separating at least one (meth)acrylic monomer-containing fluid by feeding the fluid into a rectification column containing at least one sieve tray without a runoff segment, wherein an elementary cell is obtained from a number of centers of passages in a sieve tray, and the cell shifts regularly and repeatedly along its edges, the lengths of two shifting vectors being the lengths of the edges of the cell along which the shifting is effected; an arrangement of the centers is such that the positions of an ideal center and a real center are separated by ≦1% of half of the sum of the lengths of the two shifting vectors; and an arrangement of the passages is such that the sum of non-overlapping surface areas of an ideal passage with a real passage and vice versa is ≦1% of the surface area of the ideal passage.
摘要翻译：将含有至少一种（甲基）丙烯酸系单体的流体通过将流体供给至含有至少一个不具有径流段的多孔塔的精馏塔的方法，其中从多个通道中心获得基本单元，筛板，并且单元沿其边缘规则地且重复地移动，两个移动向量的长度是实现移位的单元的边缘的长度; 中心的布置使得理想中心和实心的位置被两个移位矢量的长度之和的一半的<= 1％分开; 并且通道的布置使得理想通道的非重叠表面面积与实际通道的总和相反，<=理想通道的表面积的1％。

8. 发明授权

US08067593B2 Process for preparing aminocrotonylamino-substituted quinazoline derivatives 有权
公开(公告)号：US08067593B2
公开(公告)日：2011-11-29
申请号：US13101198
申请日：2011-05-05
申请人： Juergen Schroeder , Georg Dziewas
发明人： Juergen Schroeder , Georg Dziewas
IPC分类号： C07D239/94
CPC分类号： C07D293/04
摘要： The invention relates to an improved process for preparing aminocrotonylamino-substituted quinazoline derivatives of general formula (I) wherein the groups Ra, Rb, Rc and Rd have the meanings given in the claims, as well as sulphonyl derivatives of formula and the use thereof as synthesis components for preparing quinazolines of formula (I). The quinazoline derivatives of formula (I) are inhibitors of signal transduction mediated by tyrosinekinases and by the Epidermal Growth Factor-Receptor (EGF-R) and are therefore particularly suitable for the treatment of tumoral diseases.

9. 发明授权

US07294240B2 Method for producing (meth)acrylic acid esters 有权
标题翻译：（甲基）丙烯酸酯的制造方法
公开(公告)号：US07294240B2
公开(公告)日：2007-11-13
申请号：US10479962
申请日：2002-05-28
申请人： Matthias Geisendoerfer , Gerhard Nestler , Juergen Schroeder , Hugues Vandenmersch
发明人： Matthias Geisendoerfer , Gerhard Nestler , Juergen Schroeder , Hugues Vandenmersch
IPC分类号： B01D3/34 , C07C213/06 , C07C213/10 , C07C51/44 , C07C67/54
CPC分类号： C07C213/06 , C07C213/10 , Y02P20/582 , Y10S203/20 , Y10S203/22 , Y10S203/90 , C07C219/08
摘要： Basic (meth)acrylates IV are prepared by transesterification of alkyl (meth)acrylates I in the presence of a catalyst and working-up of the reaction mixture by distillation, by a process in which a gas or gas mixture which is inert under the reaction conditions is passed through the reaction zone and/or heat exchanger.
摘要翻译：碱性（甲基）丙烯酸酯IV通过烷基（甲基）丙烯酸烷基酯I在催化剂存在下进行酯交换和通过蒸馏处理反应混合物，通过其中反应惰性气体或气体混合物条件通过反应区和/或热交换器。

10. 发明授权

US07150809B2 Thermal separating process 有权
标题翻译：热分离过程
公开(公告)号：US07150809B2
公开(公告)日：2006-12-19
申请号：US10823672
申请日：2004-04-14
申请人： Volker Diehl , Ulrich Jaeger , Ulrich Hammon , Juergen Schroeder , Steffen Rissel
发明人： Volker Diehl , Ulrich Jaeger , Ulrich Hammon , Juergen Schroeder , Steffen Rissel
IPC分类号： B01D3/00
CPC分类号： B01D3/326 , B01D3/324 , C07C51/44 , Y10S203/11 , Y10S203/22 , C07C57/04
摘要： (Meth)acrylic monomers are separated by a thermal separation process by ascending at least one ascending gaseous stream in a separating column containing a sequence of mass transfer trays and a liquid stream that contains dissolved polymerization inhibitor which descends in the separating column, and in at least one of the streams being (meth)acrylic monomers; and spraying the inner surface of the separating column with the descending liquid stream that contains the dissolved polymerization inhibitor, and the separating column having internals, certain areas of which are shadow regions of the sprayed descending liquid stream; and which shadow regions are equipped by covering means which prevent contact of the shadow regions with (meth)acrylic monomers and consequently undesired polymerization of monomer.
摘要翻译：（Meth）丙烯酸单体通过在含有一系列质量转移塔的分离塔中的至少一个上升气流上升和含有在分离塔中下降的溶解聚合抑制剂的液体流在热分离过程中分离，至少一种物流是（甲基）丙烯酸单体; 并且用含有溶解的阻聚剂的下降液体流喷射分离塔的内表面，并且分离柱具有内部，其某些区域是喷射的下降液体流的阴影区域; 并且哪些阴影区域通过防止阴影区域与（甲基）丙烯酸单体接触的覆盖装置并因此单体的不希望的聚合来配备。

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