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1. 发明授权

US07618300B2 Method of synthesizing small-diameter carbon nanotubes with electron field emission properties 有权
标题翻译：合成具有电子场发射特性的小直径碳纳米管的方法
公开(公告)号：US07618300B2
公开(公告)日：2009-11-17
申请号：US11012341
申请日：2004-12-16
申请人： Jie Liu , Chunsheng Du , Cheng Qian , Bo Gao , Qi Qiu , Otto Z. Zhou
发明人： Jie Liu , Chunsheng Du , Cheng Qian , Bo Gao , Qi Qiu , Otto Z. Zhou
IPC分类号： H01J1/304
CPC分类号： H01J9/025 , B82Y10/00 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/04 , C01B2202/36 , H01J1/304 , H01J2201/30469
摘要： Carbon nanotube material having an outer diameter less than 10 nm and a number of walls less than ten are disclosed. Also disclosed are an electron field emission device including a substrate, an optionally layer of adhesion-promoting layer, and a layer of electron field emission material. The electron field emission material includes a carbon nanotube having a number of concentric graphene shells per tube of from two to ten, an outer diameter from 2 to 8 nm, and a nanotube length greater than 0.1 microns. One method to fabricate carbon nanotubes includes the steps of (a) producing a catalyst containing Fe and Mo supported on MgO powder, (b) using a mixture of hydrogen and carbon containing gas as precursors, and (c) heating the catalyst to a temperature above 950° C. to produce a carbon nanotube. Another method of fabricating an electron field emission cathode includes the steps of (a) synthesizing electron field emission materials containing carbon nanotubes with a number of concentric graphene shells per tube from two to ten, an outer diameter of from 2 to 8 nm, and a length greater than 0.1 microns, (b) dispersing the electron field emission material in a suitable solvent, (c) depositing the electron field emission materials onto a substrate, and (d) annealing the substrate.
摘要翻译：公开了外径小于10nm，壁数小于10的碳纳米管材料。还公开了一种电子场发射器件，其包括衬底，任选层的粘附促进层和电子场发射材料层。电子场发射材料包括碳纳米管，每个管具有多至2个至10个，外径为2至8nm的多个同心石墨烯壳，纳米管长度大于0.1微米。一种制造碳纳米管的方法包括以下步骤：（a）制备负载在MgO粉末上的含有Fe和Mo的催化剂，（b）使用氢气和含碳气体的混合物作为前体，和（c）将催化剂加热至高于950℃以产生碳纳米管。制造电子场发射阴极的另一种方法包括以下步骤：（a）合成含有碳纳米管的电子场发射材料，每个管具有多个同心石墨烯，每个管数为2至10个，外径为2至8nm，长度大于0.1微米，（b）将电子场发射材料分散在合适的溶剂中，（c）将电子场发射材料沉积到衬底上，和（d）使衬底退火。

2. 发明申请

US20060055303A1 Method of synthesizing small-diameter carbon nanotubes with electron field emission properties 有权
公开(公告)号：US20060055303A1
公开(公告)日：2006-03-16
申请号：US11012341
申请日：2004-12-16
申请人： Jie Liu , Chunsheng Du , Cheng Qian , Bo Gao , Qi Qiu , Otto Zhou
发明人： Jie Liu , Chunsheng Du , Cheng Qian , Bo Gao , Qi Qiu , Otto Zhou
IPC分类号： H01J1/14 , H01J19/06 , H01K1/04
CPC分类号： H01J9/025 , B82Y10/00 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/04 , C01B2202/36 , H01J1/304 , H01J2201/30469
摘要： Carbon nanotube material having an outer diameter less than 10 nm and a number of walls less than ten are disclosed. Also disclosed are an electron field emission device including a substrate, an optionally layer of adhesion-promoting layer, and a layer of electron field emission material. The electron field emission material includes a carbon nanotube having a number of concentric graphene shells per tube of from two to ten, an outer diameter from 2 to 8 nm, and a nanotube length greater than 0.1 microns. One method to fabricate carbon nanotubes includes the steps of (a) producing a catalyst containing Fe and Mo supported on MgO powder, (b) using a mixture of hydrogen and carbon containing gas as precursors, and (c) heating the catalyst to a temperature above 950° C. to produce a carbon nanotube. Another method of fabricating an electron field emission cathode includes the steps of (a) synthesizing electron field emission materials containing carbon nanotubes with a number of concentric graphene shells per tube from two to ten, an outer diameter of from 2 to 8 nm, and a length greater than 0.1 microns, (b) dispersing the electron field emission material in a suitable solvent, (c) depositing the electron field emission materials onto a substrate, and (d) annealing the substrate.

3. 发明申请

US20110183203A1 Polymer supported electrodes 审中-公开
标题翻译：聚合物支撑电极
公开(公告)号：US20110183203A1
公开(公告)日：2011-07-28
申请号：US12931320
申请日：2011-01-27
申请人： Chunsheng Du , Clark Dong , Lawrence S. Pan , Shufu Peng
发明人： Chunsheng Du , Clark Dong , Lawrence S. Pan , Shufu Peng
IPC分类号： H01M4/62 , B05D5/12 , B82Y30/00
CPC分类号： H01M2/166 , B82Y30/00 , H01M2/1653 , H01M2/1686 , H01M4/0402 , H01M4/0419 , H01M4/131 , H01M4/133 , H01M4/1391 , H01M4/1393 , H01M4/583 , H01M4/625 , H01M10/052 , H01M10/4235
摘要： Methods and devices arising from the practice thereof for making and using battery electrodes formed onto ion permeable, electrically non-conductive substrates, preferably battery separators are disclosed herein. Electrodes are formed onto substrates using a variety of methods including, but not limited to, spray coating and electrophoretic deposition. Electrically conductive layers may be applied to the electrode coating layer side opposite or adjacent to the substrate to act as current collectors for the battery. Multilayer devices having alternating layers of conductive layers, electrode layers and substrates, wherein the conductive layers may be in electrical communication with other conductive layers to form a battery.
摘要翻译：本文公开了用于制造和使用形成在离子可渗透的非导电基底上的电池电极的实践的方法和装置，优选电池隔板。电极使用各种方法形成在基底上，包括但不限于喷涂和电泳沉积。可以将导电层施加到与基板相对或相邻的电极涂层侧，以用作电池的集流器。具有交替层的导电层，电极层和衬底的多层器件，其中导电层可以与其它导电层电连通以形成电池。

4. 发明申请

US20080010796A1 High power density supercapacitors with carbon nanotube electrodes 失效
标题翻译：具有碳纳米管电极的高功率密度超级电容器
公开(公告)号：US20080010796A1
公开(公告)日：2008-01-17
申请号：US11281325
申请日：2005-11-16
申请人： Ning Pan , Chunsheng Du
发明人： Ning Pan , Chunsheng Du
IPC分类号： H01G9/00
CPC分类号： H01G11/26 , H01G11/36 , H01G11/86 , H01M4/133 , H01M4/587 , Y02E60/13 , Y02T10/7022 , Y10T29/417
摘要： One embodiment of the present invention provides a process for fabricating an electrode for a capacitor using carbon nanotubes (CNTs), wherein the electrode comprises a metal substrate and a layer of active material (CNTs) coated onto the metal substrate. Specifically, the process starts by dispersing CNTs in a solvent to form a suspension. Next, the CNTs are charged in the suspension. The metal substrate is then immersed in the suspension. Next, the CNTs are deposited onto the metal substrate using electrophoretic deposition (EPD) to form the layer of active material on the metal substrate. In particular, the layer of active material is formed on the metal substrate without using a binder, which effectively reduces contact resistance between the active material and the metal substrate.
摘要翻译：本发明的一个实施例提供了一种使用碳纳米管（CNT）制造用于电容器的电极的方法，其中电极包括金属基底和涂覆在金属基底上的活性材料层（CNT）。具体地，该方法通过将CNT分散在溶剂中以形成悬浮液而开始。接下来，将CNT充入悬浮液中。然后将金属基材浸入悬浮液中。接下来，使用电泳沉积（EPD）将CNT沉积到金属基板上，以在金属基板上形成活性材料层。特别地，在金属基板上形成活性物质层，而不使用粘合剂，这有效地降低了活性材料和金属基底之间的接触电阻。

5. 发明授权

US07553341B2 High power density supercapacitors with carbon nanotube electrodes 失效
标题翻译：具有碳纳米管电极的高功率密度超级电容器
公开(公告)号：US07553341B2
公开(公告)日：2009-06-30
申请号：US11281325
申请日：2005-11-16
申请人： Ning Pan , Chunsheng Du
发明人： Ning Pan , Chunsheng Du
IPC分类号： H01G9/00
CPC分类号： H01G11/26 , H01G11/36 , H01G11/86 , H01M4/133 , H01M4/587 , Y02E60/13 , Y02T10/7022 , Y10T29/417
摘要： One embodiment of the present invention provides a process for fabricating an electrode for a capacitor using carbon nanotubes (CNTs), wherein the electrode comprises a metal substrate and a layer of active material (CNTs) coated onto the metal substrate. Specifically, the process starts by dispersing CNTs in a solvent to form a suspension. Next, the CNTs are charged in the suspension. The metal substrate is then immersed in the suspension. Next, the CNTs are deposited onto the metal substrate using electrophoretic deposition (EPD) to form the layer of active material on the metal substrate. In particular, the layer of active material is formed on the metal substrate without using a binder, which effectively reduces contact resistance between the active material and the metal substrate.
摘要翻译：本发明的一个实施例提供了一种使用碳纳米管（CNT）制造用于电容器的电极的方法，其中电极包括金属基底和涂覆在金属基底上的活性材料层（CNT）。具体地，该方法通过将CNT分散在溶剂中以形成悬浮液而开始。接下来，将CNT充入悬浮液中。然后将金属基材浸入悬浮液中。接下来，使用电泳沉积（EPD）将CNT沉积到金属基板上，以在金属基板上形成活性材料层。特别地，在金属基板上形成活性物质层，而不使用粘合剂，这有效地降低了活性材料和金属基底之间的接触电阻。

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