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1. 发明申请

US20130005918A1 METHOD FOR PRODUCING POLYMERIC POLYAMINES 审中-公开
标题翻译：生产聚合聚氨酯的方法
公开(公告)号：US20130005918A1
公开(公告)日：2013-01-03
申请号：US13612052
申请日：2012-09-12
申请人： Jiang-Jen Lin , Wei-Cheng Tsai , Yen-Chi Hsu , Wen-Hsin Chang
发明人： Jiang-Jen Lin , Wei-Cheng Tsai , Yen-Chi Hsu , Wen-Hsin Chang
IPC分类号： C07C231/02 , C08F8/32
CPC分类号： C08F26/00
摘要： Polymeric polyamine is produced by polymerizing polyoxyalkylene-amine and a linker. The polyoxyalkylene-amine has a structural formula H2N—R—NH2, wherein R is selected from the group consisting of dianhydride, diacid, epoxy, diisocyanate and poly(styrene-co-maleic anhydride) copolymers (SMA). The linker can be anhydride, carboxylic acid, epoxy, isocyanate or poly(styrene-co-maleic anhydride) copolymers (SMA). The polymeric polyamine so produced can be used as a stabilizer or dispersant of the Ag nanoparticles.
摘要翻译：聚合多胺通过聚合聚氧亚烷基 - 胺和接头来制备。聚氧化烯胺具有结构式H2N-R-NH2，其中R选自二酐，二酸，环氧，二异氰酸酯和聚（苯乙烯 - 共 - 马来酸酐）共聚物（SMA）。接头可以是酐，羧酸，环氧，异氰酸酯或聚（苯乙烯 - 共 - 马来酸酐）共聚物（SMA）。如此生产的聚合多胺可用作Ag纳米颗粒的稳定剂或分散剂。

2. 发明申请

US20110288239A1 POLYMERIC POLYAMINES AND METHOD FOR PRODUCING THE SAME 审中-公开
标题翻译：聚合物聚氨酯及其制造方法
公开(公告)号：US20110288239A1
公开(公告)日：2011-11-24
申请号：US13195022
申请日：2011-08-01
申请人： Jiang-Jen Lin , Wei-Cheng Tsai , Yen-Chi Hsu , Wen-Hsin Chang
发明人： Jiang-Jen Lin , Wei-Cheng Tsai , Yen-Chi Hsu , Wen-Hsin Chang
IPC分类号： C08F8/32 , C07D403/12 , C08F220/08 , C07D307/60 , C07C275/24 , C07C235/84 , C07C235/78
CPC分类号： C08F26/00
摘要： The present invention discloses a polymeric polyamine which can be produced by polymerizing polyoxyalkylene-amine and a linker. The linker can be anhydride, carboxylic acid, epoxy, isocyanate or poly(styrene-co-maleic anhydride) copolymers (SMA). The present invention also discloses a method for stabilizing the Ag nanoparticles with polymeric polyamine. The polymeric polyamine serving as a stabilizer or dispersant is mixed with a water solution of silver salt and then a reducer is provided to reduce the silver ions and form an organic or a water solution of Ag nanoparticles. Water or solvent of this solution can be further removed through a heating, freezing or decompression process, and thus solid content of the solution can be increased. The concentrated solution also can be diluted to obtain a stable dispersion without aggregation.
摘要翻译：本发明公开了一种聚合多胺，其可通过聚合聚氧亚烷基 - 胺和连接体而制备。接头可以是酐，羧酸，环氧，异氰酸酯或聚（苯乙烯 - 共 - 马来酸酐）共聚物（SMA）。本发明还公开了一种用聚合多胺稳定Ag纳米颗粒的方法。用作稳定剂或分散剂的聚合多胺与银盐水溶液混合，然后提供还原剂以还原银离子并形成Ag纳米颗粒的有机或水溶液。该溶液的水或溶剂可以通过加热，冷冻或减压方法进一步除去，从而可以提高溶液的固体含量。浓缩溶液也可以稀释以获得稳定的分散体而不凝聚。

3. 发明申请

US20090149583A1 POLYMERIC POLYAMINES AND METHOD FOR STABILIZING SILVER NANOPARTICLE BY EMPLOYING THE SAME 有权
标题翻译：聚合物聚氨酯和通过使用其来稳定银纳米颗粒的方法
公开(公告)号：US20090149583A1
公开(公告)日：2009-06-11
申请号：US12140507
申请日：2008-06-17
申请人： Jiang-Jen Lin , Wei-Cheng Tsai , Yen-Chi Hsu , Wen-Hsin Chang
发明人： Jiang-Jen Lin , Wei-Cheng Tsai , Yen-Chi Hsu , Wen-Hsin Chang
IPC分类号： C08K3/08 , C08F26/00 , C08K5/3415 , C08K5/20 , C08K5/107 , C08K5/05
CPC分类号： C08F26/00
摘要： The present invention discloses a polymeric polyamine which can be produced by polymerizing polyoxyalkylene-amine and a linker. The linker can be anhydride, carboxylic acid, epoxy, isocyanate or poly(styrene-co-maleic anhydride) copolymers (SMA). The present invention also discloses a method for stabilizing the Ag nanoparticles with polymeric polyamine. The polymeric polyamine serving as a stabilizer or dispersant is mixed with a water solution of silver salt and then a reducer is provided to reduce the silver ions and form an organic or a water solution of Ag nanoparticles. Water or solvent of this solution can be further removed through a heating, freezing or decompression process, and thus solid content of the solution can be increased. The concentrated solution also can be diluted to obtain a stable dispersion without aggregation.
摘要翻译：本发明公开了一种聚合多胺，其可通过聚合聚氧亚烷基 - 胺和连接体而制备。接头可以是酐，羧酸，环氧，异氰酸酯或聚（苯乙烯 - 共 - 马来酸酐）共聚物（SMA）。本发明还公开了一种用聚合多胺稳定Ag纳米颗粒的方法。用作稳定剂或分散剂的聚合多胺与银盐水溶液混合，然后提供还原剂以还原银离子并形成Ag纳米颗粒的有机或水溶液。该溶液的水或溶剂可以通过加热，冷冻或减压方法进一步除去，从而可以提高溶液的固体含量。浓缩溶液也可以稀释以获得稳定的分散体而不凝聚。

4. 发明授权

US08013048B2 Polymeric polyamines and method for stabilizing silver nanoparticle by employing the same 有权
标题翻译：聚合多胺及其使用方法稳定银纳米颗粒
公开(公告)号：US08013048B2
公开(公告)日：2011-09-06
申请号：US12140507
申请日：2008-06-17
申请人： Jiang-Jen Lin , Wei-Cheng Tsai , Yen-Chi Hsu , Wen-Hsin Chang
发明人： Jiang-Jen Lin , Wei-Cheng Tsai , Yen-Chi Hsu , Wen-Hsin Chang
IPC分类号： C08K3/08 , C08K5/3415 , C08K5/20 , C08K5/107 , C08K5/05 , C08F26/00
CPC分类号： C08F26/00
摘要： The present invention discloses a polymeric polyamine which can be produced by polymerizing polyoxyalkylene-amine and a linker. The linker can be anhydride, carboxylic acid, epoxy, isocyanate or poly(styrene-co-maleic anhydride) copolymers (SMA). The present invention also discloses a method for stabilizing the Ag nanoparticles with polymeric polyamine. The polymeric polyamine serving as a stabilizer or dispersant is mixed with a water solution of silver salt and then a reducer is provided to reduce the silver ions and form an organic or a water solution of Ag nanoparticles. Water or solvent of this solution can be further removed through a heating, freezing or decompression process, and thus solid content of the solution can be increased. The concentrated solution also can be diluted to obtain a stable dispersion without aggregation.
摘要翻译：本发明公开了一种聚合多胺，其可通过聚合聚氧亚烷基 - 胺和连接体而制备。接头可以是酐，羧酸，环氧，异氰酸酯或聚（苯乙烯 - 共 - 马来酸酐）共聚物（SMA）。本发明还公开了一种用聚合多胺稳定Ag纳米颗粒的方法。用作稳定剂或分散剂的聚合多胺与银盐水溶液混合，然后提供还原剂以还原银离子并形成Ag纳米颗粒的有机或水溶液。该溶液的水或溶剂可以通过加热，冷冻或减压方法进一步除去，从而可以提高溶液的固体含量。浓缩溶液也可以稀释以获得稳定的分散体而不凝聚。

5. 发明申请

US20120279352A1 METHOD FOR PREPARING SILVER NANOPARTICLES BY EMPLOYING ETHANOLAMINE AND POLY(STYRENE-CO-MALEIC ANHYDRIDE) COPOLYMERS 有权
标题翻译：通过使用乙醇胺和聚（苯乙烯 - 马来酸酐）共聚物制备银纳米粒子的方法
公开(公告)号：US20120279352A1
公开(公告)日：2012-11-08
申请号：US13549417
申请日：2012-07-14
申请人： Jiang-Jen Lin , Wei-Cheng Tsai , Chao-Po Hsu , Wei-Li Lin , Yueh-Hsien Wu
发明人： Jiang-Jen Lin , Wei-Cheng Tsai , Chao-Po Hsu , Wei-Li Lin , Yueh-Hsien Wu
IPC分类号： B22F9/16 , B82Y40/00
CPC分类号： B22F9/24 , B22F1/0018 , B82Y30/00 , Y10S977/896
摘要： The present invention provides a method for producing silver nanoparticles by employing ethanolamine. The method of this invention can be easily operated and no organic solvent is required. Ethanolamine first reacts with copolymers of poly(styrene-co-maleic anhydride) (abbreviated as SMA) to generate polymeric polymers. The polymeric polymers then reduce silver ions to silver atoms which are dispersed in the form of silver nanoparticles. Functional groups of the polymeric polymers can chelate with silver ions and be stably compatible with water or organic solvents, whereby the silver nanoparticles can be stably dispersed without aggregation and the produced silver nanoparticles.
摘要翻译：本发明提供使用乙醇胺制造银纳米粒子的方法。本发明的方法可以容易地操作，不需要有机溶剂。乙醇胺首先与聚（苯乙烯 - 共 - 马来酸酐）（缩写为SMA）的共聚物反应生成聚合物聚合物。聚合物聚合物然后将银离子还原成以银纳米颗粒形式分散的银原子。聚合物聚合物的官能团可以与银离子螯合并与水或有机溶剂稳定地相容，由此可以稳定地分散银纳米颗粒而不会聚集，并且所制备的银纳米颗粒。

6. 发明授权

US08951330B2 Method for preparing silver nanoparticles by employing ethanolamine and poly(styrene-co-maleic anhydride) copolymers 有权
标题翻译：通过使用乙醇胺和聚（苯乙烯 - 共 - 马来酸酐）共聚物制备银纳米颗粒的方法
公开(公告)号：US08951330B2
公开(公告)日：2015-02-10
申请号：US13549417
申请日：2012-07-14
申请人： Jiang-Jen Lin , Wei-Cheng Tsai , Chao-Po Hsu , Wei-Li Lin , Yueh-Hsien Wu
发明人： Jiang-Jen Lin , Wei-Cheng Tsai , Chao-Po Hsu , Wei-Li Lin , Yueh-Hsien Wu
IPC分类号： B22F9/24 , B22F1/00 , B82Y30/00
CPC分类号： B22F9/24 , B22F1/0018 , B82Y30/00 , Y10S977/896
摘要： The present invention provides a method for producing silver nanoparticles by employing ethanolamine. The method of this invention can be easily operated and no organic solvent is required. Ethanolamine first reacts with copolymers of poly(styrene-co-maleic anhydride) (abbreviated as SMA) to generate polymeric polymers. The polymeric polymers then reduce silver ions to silver atoms which are dispersed in the form of silver nanoparticles. Functional groups of the polymeric polymers can chelate with silver ions and be stably compatible with water or organic solvents, whereby the silver nanoparticles can be stably dispersed without aggregation and the produced silver nanoparticles.
摘要翻译：本发明提供使用乙醇胺制造银纳米粒子的方法。本发明的方法可以容易地操作，不需要有机溶剂。乙醇胺首先与聚（苯乙烯 - 共 - 马来酸酐）（缩写为SMA）的共聚物反应生成聚合物聚合物。聚合物聚合物然后将银离子还原成以银纳米颗粒形式分散的银原子。聚合物聚合物的官能团可以与银离子螯合并与水或有机溶剂稳定地相容，由此可以稳定地分散银纳米颗粒而不会聚集，并且所制备的银纳米颗粒。

7. 发明授权

US08491699B2 Method for preparing silver nanoparticles by employing ethanolamine 有权
标题翻译：采用乙醇胺制备银纳米颗粒的方法
公开(公告)号：US08491699B2
公开(公告)日：2013-07-23
申请号：US12836762
申请日：2010-07-15
申请人： Jiang-Jen Lin , Wei-Cheng Tsai , Chao-Po Hsu , Wei-Li Lin , Yueh-Hsien Wu
发明人： Jiang-Jen Lin , Wei-Cheng Tsai , Chao-Po Hsu , Wei-Li Lin , Yueh-Hsien Wu
IPC分类号： B22F9/24 , B82Y40/00
CPC分类号： B22F9/24 , B22F1/0018 , B82Y30/00 , Y10S977/896
摘要： The present invention provides a method for producing silver nanoparticles by employing ethanolamine. The method of this invention can be easily operated and no organic solvent is required. Ethanolamine first reacts with a mixture of poly(oxyalkylene)-amine/epoxy or copolymers of poly(styrene-co-maleic anhydride) (abbreviated as SMA) to generate polymeric polymers. The polymeric polymers then reduce silver ions to silver atoms which are dispersed in the form of silver nanoparticles. Functional groups of the polymeric polymers can chelate with silver ions and be stably compatible with water or organic solvents, whereby the silver nanoparticles can be stably dispersed without aggregation and the produced silver nanoparticles.
摘要翻译：本发明提供使用乙醇胺制造银纳米粒子的方法。本发明的方法可以容易地操作，不需要有机溶剂。乙醇胺首先与聚（氧化烯） - 胺/环氧树脂或聚（苯乙烯 - 共 - 马来酸酐）（缩写为SMA）的共聚物的混合物反应生成聚合物聚合物。聚合物聚合物然后将银离子还原成以银纳米颗粒形式分散的银原子。聚合物聚合物的官能团可以与银离子螯合并与水或有机溶剂稳定地相容，由此可以稳定地分散银纳米颗粒而不会聚集，并且所制备的银纳米颗粒。

8. 发明申请

US20130035445A1 METHOD OF MAKING POLYMERIC POLYMER CONTAINING POLY(OXYETHYLENE)-AMINE 审中-公开
标题翻译：制备聚（聚氧乙烯）胺聚合物聚合物的方法
公开(公告)号：US20130035445A1
公开(公告)日：2013-02-07
申请号：US13621149
申请日：2012-09-15
申请人： Jiang-Jen Lin , Wei-Cheng Tsai , Rui-Xuan Dong , Wei-Li Lin , Chao-Po Hsu
发明人： Jiang-Jen Lin , Wei-Cheng Tsai , Rui-Xuan Dong , Wei-Li Lin , Chao-Po Hsu
IPC分类号： C08F265/02
CPC分类号： C08F222/08 , B22F9/24 , B22F2998/00 , C08F222/1006 , C08F222/38 , C30B7/14 , C30B29/02 , H01B1/22 , B22F1/0018
摘要： A polymeric polymer is prepared from poly(oxyethylene)-amine and a linker, for example, poly(styrene-co-maleic anhydride) (SMA) or dianhydride. The polymeric polymer can chelate silver ions and reduce them to silver atoms which are dispersed as nanoparticles. No additional reducing agent is needed and more than 30% of solid content of the nanoparticles solution can be achieved without aggregation. The prepared silver nanoparticles are both hydrophilic and hydrophobic and therefore are compatible with polymers.
摘要翻译：由聚（氧乙烯） - 胺和接头例如聚（苯乙烯 - 共 - 马来酸酐）（SMA）或二酐制备聚合物聚合物。聚合物聚合物可以螯合银离子并将其还原成分散为纳米颗粒的银原子。不需要额外的还原剂，并且可以在没有聚集的情况下实现超过30％的纳米颗粒溶液的固体含量。所制备的银纳米颗粒是亲水和疏水的，因此与聚合物相容。

9. 发明授权

US08333822B2 Polymeric polymer containing poly(oxyethylene)-amine and application thereof to preparing silver nanoparticle 有权
标题翻译：含聚（氧乙烯） - 胺的聚合物聚合物及其在制备银纳米颗粒中的应用
公开(公告)号：US08333822B2
公开(公告)日：2012-12-18
申请号：US12843050
申请日：2010-07-26
申请人： Jiang-Jen Lin , Wei-Cheng Tsai , Rui-Xuan Dong , Wei-Li Lin , Chao-Po Hsu
发明人： Jiang-Jen Lin , Wei-Cheng Tsai , Rui-Xuan Dong , Wei-Li Lin , Chao-Po Hsu
IPC分类号： B22F9/24
CPC分类号： C08F222/08 , B22F9/24 , B22F2998/00 , C08F222/1006 , C08F222/38 , C30B7/14 , C30B29/02 , H01B1/22 , B22F1/0018
摘要： A polymeric polymer containing poly(oxyethylene)-amine and its application to preparation of silver nanoparticles. The polymeric polymer is prepared from poly(oxyethylene)-amine and a linker, for example, poly(styrene-co-maleic anhydride) (SMA) or dianhydride. The polymeric polymer can chelate silver ions and reduce them to silver atoms which are dispersed as nanoparticles. No additional reducing agent is needed and more than 30% of solid content of the nanoparticles solution can be achieved without aggregation. The prepared silver nanoparticles are both hydrophilic and hydrophobic and therefore are compatible with polymers.
摘要翻译：含聚（氧乙烯） - 胺的聚合物聚合物及其在制备银纳米颗粒中的应用。聚合物聚合物由聚（氧乙烯） - 胺和接头例如聚（苯乙烯 - 共 - 马来酸酐）（SMA）或二酐制备。聚合物聚合物可以螯合银离子并将其还原成分散为纳米颗粒的银原子。不需要额外的还原剂，并且可以在没有聚集的情况下实现超过30％的纳米颗粒溶液的固体含量。所制备的银纳米颗粒是亲水和疏水的，因此与聚合物相容。

10. 发明授权

US08318844B2 Oil-dispersible composite of metallic nanoparticle and method for synthesizing same 有权
标题翻译：金属纳米颗粒的油分散复合材料及其合成方法
公开(公告)号：US08318844B2
公开(公告)日：2012-11-27
申请号：US13109919
申请日：2011-05-17
申请人： Jiang-Jen Lin , Wei-Cheng Tsai , Rui-Xuan Dong , Hui-Fen Lin , Yueh-Hsien Wu
发明人： Jiang-Jen Lin , Wei-Cheng Tsai , Rui-Xuan Dong , Hui-Fen Lin , Yueh-Hsien Wu
IPC分类号： C08K3/08
CPC分类号： C08G18/6674 , C08G18/4833 , C08G59/50 , C08K3/18 , C08K9/08 , C08K2201/011
摘要： The present invention provides an oil-dispersible composite of metallic nanoparticles and a method for synthesizing the same. The composite primarily includes metallic nanoparticles and an oily polymeric polymer such as polyurethane (PU). The oily polymeric polymer serves as a carrier of the metallic nanoparticles by chelating therewith so that the metallic nanoparticles are dispersed uniformly. In the method of the present invention, the metallic ions are first chelated by the oily polymeric polymer and then reduced into nanoparticles. The composite of the present invention is about 5 to 100 nm in particle size.
摘要翻译：本发明提供一种金属纳米粒子的油分散性复合体及其合成方法。复合材料主要包括金属纳米颗粒和油性聚合物聚合物如聚氨酯（PU）。油性聚合物聚合物通过与其螯合而用作金属纳米颗粒的载体，使得金属纳米颗粒均匀分散。在本发明的方法中，金属离子首先被油性聚合物聚合物螯合，然后还原成纳米颗粒。本发明的复合体的粒径为约5〜100nm。

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