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    • 9. 发明授权
    • Method for manufacturing magnesium borohydride
    • 镁硼氢化物的制造方法
    • US07381390B2
    • 2008-06-03
    • US11305914
    • 2005-12-19
    • Grigorii Lev SoloveichikJi-Cheng Zhao
    • Grigorii Lev SoloveichikJi-Cheng Zhao
    • C01B6/21
    • C01B6/21
    • Disclosed herein is a method comprising reacting a metal borohydride with a metal chloride composition that comprises magnesium chloride in a solvent to form a reaction mixture; wherein either the metal borohydride, the metal chloride composition or both the metal borohydride and the metal chloride composition are soluble in the solvent and a formed metal chloride is insoluble in the solvent; removing the solvent from the reaction mixture to produce a borohydride complex; treating the borohydride complex to obtain magnesium borohydride; extracting magnesium borohydride solvate; and desolvating the magnesium borohydride solvate to form magnesium borohydride.
    • 本文公开了一种方法,其包括使金属硼氢化物与金属氯化物组合物反应,所述金属氯化物组合物在溶剂中包含氯化镁以形成反应混合物; 其中金属硼氢化物,金属氯化物组合物或金属硼氢化物和金属氯化物组合物都溶于溶剂中,形成的金属氯化物不溶于溶剂; 从反应混合物中除去溶剂以产生硼氢化物络合物; 处理硼氢化物复合物得到硼氢化镁; 提取硼氢化镁溶剂合物; 并将硼氢化镁溶剂化物脱醇形成硼氢化镁。
    • 10. 发明申请
    • COMPOSITION AND ENERGY STORAGE DEVICE
    • 组合物和能源储存装置
    • US20120077070A1
    • 2012-03-29
    • US12893661
    • 2010-09-29
    • Grigorii Lev SoloveichikRichard Louis HartJohn Patrick Lemmon
    • Grigorii Lev SoloveichikRichard Louis HartJohn Patrick Lemmon
    • H01M10/02H01M2/18H01M10/26
    • H01M10/26H01M2300/0054H01M2300/0057Y10T29/49108Y10T29/49115
    • A cathode composition is provided. The cathode composition includes at least one electroactive metal, wherein the electroactive metal is at least one selected from the group consisting of titanium, vanadium, niobium, molybdenum, nickel, iron, cobalt, chromium, manganese, silver, antimony, cadmium, tin, lead and zinc; a first alkali metal halide; an electrolyte salt comprising a reaction product of a second alkali metal halide and a metal halide, wherein the electrolyte salt has a melting point of less than about 300 degrees Centigrade; and a metal chlorosulfide compound having a formula (I) M1M2p+1SnCl4+3p-2n wherein “M1” is a metal selected from group IA of the periodic table, “M2” is a metal selected from group IIIA of the periodic table, “p” is 0 or 1, and “n” is equal to or greater than 0.5. An article and an energy storage device comprising the cathode composition is provided. A method of forming the energy storage device is provided.
    • 提供阴极组合物。 阴极组合物包括至少一种电活性金属,其中电活性金属是选自钛,钒,铌,钼,镍,铁,钴,铬,锰,银,锑,镉,锡, 铅锌 第一碱金属卤化物; 电解质盐,其包含第二碱金属卤化物和金属卤化物的反应产物,其中所述电解质盐的熔点小于约300摄氏度; 和具有式(I)M1M2p + 1SnCl4 + 3p-2n的金属氯化硫化物,其中“M1”是选自元素周期表的IA族的金属,“M2”是选自元素周期表IIIA族的金属, p“为0或1,”n“等于或大于0.5。 提供了一种包含阴极组合物的制品和储能装置。 提供一种形成能量存储装置的方法。