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1. 发明授权

US5506007A Polymerization of systems using a deoxygenated medium 失效
标题翻译：使用脱氧培养基进行系统聚合
公开(公告)号：US5506007A
公开(公告)日：1996-04-09
申请号：US510475
申请日：1995-08-02
申请人： Jerry W. Williams , George V. D. Tiers , Jeanne M. Goetzke , Gerald L. Uhl
发明人： Jerry W. Williams , George V. D. Tiers , Jeanne M. Goetzke , Gerald L. Uhl
IPC分类号： B05D1/36 , B05D3/00 , B05D3/06 , B05D3/10 , C08F2/00 , C08L33/04 , C08L33/10 , C08L33/18 , C08L33/20 , C08L33/24 , C08L33/26 , C09D4/00 , C09D133/02 , C09D133/04 , C09D133/18 , C09D133/24 , C09D201/00 , C08J7/04
CPC分类号： B05D3/107 , B05D3/068 , C09D4/00
摘要： A process for polymerizing a free-radically polymerizable composition comprising the steps:(a) coating a coatable free-radically polymerizable mixture onto at least one major surface of a web;(b) deoxygenating a liquid inerting medium;(c) immersing the coated web into the deoxygenated liquid inerting medium; and(d) irradiating the immersed coated web with actinic radiation sufficient to effect polymerization of the free-radically polymerizable mixture, while maintaining the liquid inerting medium in an essentially oxygen-free state.
摘要翻译：一种使可自由基聚合的组合物聚合的方法，包括以下步骤：（a）将可涂布的可自由基聚合的混合物涂布在幅材的至少一个主表面上; （b）使液体惰性介质脱氧; （c）将涂覆的纤维网浸入脱氧液体惰性介质中; 和（d）用足够的自由基聚合混合物进行聚合的光化辐射照射浸渍的涂布网，同时保持液体使介质处于基本上不含氧的状态。

2. 发明授权

US5962546A Cationically polymerizable compositions capable of being coated by electrostatic assistance 失效
公开(公告)号：US5962546A
公开(公告)日：1999-10-05
申请号：US847206
申请日：1997-05-01
申请人： Albert I. Everaerts , William M. Lamanna , Albert E. Seaver , George V. D. Tiers
发明人： Albert I. Everaerts , William M. Lamanna , Albert E. Seaver , George V. D. Tiers
IPC分类号： B05D1/04 , C07C311/48 , C07C311/51 , C07C317/14 , C07D303/34 , C08G59/68 , C08G77/14 , C09D125/18 , C09D163/00 , H01B1/20
CPC分类号： C07D303/34 , C07C311/48 , C07C311/51
摘要： Compositions containing conductivity enhancers, which are capable of being coated onto a substrate by means of electrostatic assistance. The compositions comprise one or more cationically polymerizable monomer(s), one or more cationic initiator(s), and one or more non-volatile conductivity enhancer(s) having anionic and cationic portions which are soluble in the monomer(s) and which do not interfere with cationic polymerization wherein the anionic portion is a non-coordinating carbon-containing anion. The compositions may further comprise one or more dissociation enhancing agent(s), oligomer(s) or polymer(s), preferably co-reactive, free-radically curable monomer(s), free-radical generating initiator(s), leveling agents, and other additives or adjuvants to impart specific properties to the polymerized composition.

3. 发明授权

US5047444A Fluorescent degree of cure monitors 失效
标题翻译：荧光度治愈显示器
公开(公告)号：US5047444A
公开(公告)日：1991-09-10
申请号：US359108
申请日：1989-05-31
申请人： Robert J. DeVoe , Katherine A. Brown-Wensley , George V. D. Tiers
发明人： Robert J. DeVoe , Katherine A. Brown-Wensley , George V. D. Tiers
IPC分类号： C08F2/38 , C08F2/40 , C08F283/12 , C08G85/00 , C08J3/20 , C08K5/00 , C08L83/04 , C09K11/06 , G01N21/64 , G03F7/105
CPC分类号： G01N21/643 , C08G85/00 , C08J3/20 , C08L83/04 , C09K11/06 , G03F7/105 , C08G77/12 , C08G77/20 , Y10S430/148
摘要： A curable composition, the cure of which can be monitored optically, comprises at least one of a hydride curable silicone, an ethylenically unsaturated compound, and a cationically polymerizable monomer, and as cure monitor dibenzofulvene or derivatives thereof. The cure monitor is a latent fluorophore which reacts under the cure conditions to form a UV-detectable fluorophore.The invention also provides a method for measuring degree of cure of a polymeric material which can be a coating or an article.

4. 发明授权

US4258644A Depositing latent fingerprints and development thereof 失效
标题翻译：沉积潜伏指纹及其发展
公开(公告)号：US4258644A
公开(公告)日：1981-03-31
申请号：US59608
申请日：1979-07-23
申请人： Edward J. Goettert , George V. D. Tiers
发明人： Edward J. Goettert , George V. D. Tiers
IPC分类号： A61B5/117 , B05B7/06
CPC分类号： A61B5/1172
摘要： Latent fingerprints having a latency of several weeks are applied to paper substrates using compositions comprising trimeric aliphatic acids of at least 30 carbon atoms which are substantive to paper fibers are substantially non-volatile, and are non-hardening, non-toxic and non-hygroscopic. The latent fingerprints are developed as desired by dusting in the conventional manner with toner particles, suitably, comprising magnetic particles in oleophilic matrix.
摘要翻译：具有几周潜伏期的潜在指纹应用于纸基质，其中使用包含至少30个碳原子的三聚脂肪酸的组合物，其对纸纤维是实质上基本上是非挥发性的，并且是非硬化的，无毒的和非吸湿性的。根据需要，通过以常规方式通过用调色剂颗粒进行粉化来适当地包含亲油基质中的磁性颗粒来显影潜在指纹。

5. 发明授权

US4152165A One-part hydrophilic treatment compositions 失效
标题翻译：一部分亲水处理组合物
公开(公告)号：US4152165A
公开(公告)日：1979-05-01
申请号：US895527
申请日：1978-04-11
申请人： Bruce A. Langager , Boyd R. Beck , Frank T. Sher , George V. D. Tiers
发明人： Bruce A. Langager , Boyd R. Beck , Frank T. Sher , George V. D. Tiers
IPC分类号： C03C17/30 , C04B41/49 , C09K3/18
CPC分类号： C04B41/4944 , C03C17/30 , C04B41/4927 , C04B41/4938 , C04B41/4966 , C04B2111/00112
摘要： One-part hydrophilic treatment compositions are provided which comprise (i) an aqueous solution of a sulfonato-organosilanol compound which has at least one sulfonato-organic substituent therein, and (ii) an abrasive material. These compositions are particularly useful in imparting hydrophilicity to siliceous surfaces.
摘要翻译：提供了一部分亲水处理组合物，其包括（i）其中具有至少一个磺酸基 - 有机取代基的磺化 - 有机硅烷化合物的水溶液和（ii）研磨材料。这些组合物特别可用于赋予硅质表面亲水性。

6. 发明授权

US5583178A Cure-indicating molding and coating composition 失效
标题翻译：固化指示成型和涂料组合物
公开(公告)号：US5583178A
公开(公告)日：1996-12-10
申请号：US496499
申请日：1995-06-29
申请人： Joel D. Oxman , Mark S. Konings , George V. D. Tiers , Kim M. Vogel , Dennis E. Vogel
发明人： Joel D. Oxman , Mark S. Konings , George V. D. Tiers , Kim M. Vogel , Dennis E. Vogel
IPC分类号： A61K6/093 , A61K6/10 , A61L27/18 , B05D3/00 , B05D5/06 , B05D7/24 , C08J3/24 , C08K5/00 , C08L83/04 , C09B23/00 , C09B53/00 , C09D183/05 , C09D183/07 , C08L83/05
CPC分类号： C08L83/04 , A61K6/0017 , A61K6/0023 , A61K6/0061 , A61K6/10 , A61L27/18 , C08J3/248 , C08K5/0041 , C09B19/00 , C09B23/06 , C09B23/083 , C09B23/086 , C09B23/102 , C09B23/107 , C09B23/145 , C09B55/002 , C08G77/045 , C08G77/12 , C08G77/20
摘要： The present invention provides novel hydrosilation-curable compositions, the cure of which can be monitored visually, comprising: (1) an ethylenic compound; (2) a compound containing silicon-bonded-hydrogen groups; (3) a hydrosilation catalyst; and (4) one or more cure-indicating dyes with light absorption in the visible spectrum that exhibit a color change in the presence of a silicon-bonded-hydrogen compound and a precious metal hydrosilation catalyst. The cure-indicating dye provides the composition with an initial pre-cure color and a different post-cure color. As a result of this change in color, the state of cure of the composition can be visually monitored.
摘要翻译：本发明提供了新的可氢化硅烷化固化的组合物，其固化可以目视监测，包括：（1）烯属化合物; （2）含有硅键合氢基团的化合物; （3）硅氢化催化剂; 和（4）一种或多种在可见光谱中具有光吸收的固化指示染料，其在硅键合氢化合物和贵金属硅氢化催化剂存在下表现出颜色变化。固化指示染料为组合物提供初始预固化颜色和不同的后固化颜色。作为颜色变化的结果，可以目视监视组合物的固化状态。

7. 发明授权

US5258274A Thermal dye bleach construction sensitive to ultraviolet radiation 失效
标题翻译：热染料漂白剂施工对紫外线辐射敏感
公开(公告)号：US5258274A
公开(公告)日：1993-11-02
申请号：US887778
申请日：1992-05-22
申请人： Randall H. Helland , George V. D. Tiers , Dian E. Stevenson
发明人： Randall H. Helland , George V. D. Tiers , Dian E. Stevenson
IPC分类号： B41M5/28 , G03C1/498 , G03C1/825
CPC分类号： G03C1/49845 , B41M5/286 , G03C1/49854 , Y10S430/156 , Y10S430/165
摘要： A thermal-dye-bleach construction comprising a thermal nucleophile-generating agent in association with a styryl dye having a nucleus of general formula (I): ##STR1## representing the nucleus of a styryl dye in which R=methyl or ethyl groupY=alkoxy of 1 to 20 carbon atomsm=1 or 2,n=1, 2, or 3, andx.sup..crclbar. =an anionThe aromatic fused benzene portion of the indolenine ring may be further substituted with commonly acceptable dye substituents such as alkyl and substituted alkyl (of 1 to 10 carbon atoms) groups, alkoxy groups (preferably of 1 to 10 carbon atoms), fused aromatic rings (as to make the benzene ring a fused naphthalene ring), halogen (including fluoro), cyano, nitro, carboxamido, amido, etc. One or two substituents chosen variously from said group may also be present on the phenyl ring to which the alkoxy group is attached. These substituents and their combinations should not be chosen so as to alter the absorption characteristics of the dye greatly enough to remove the maximum absorption from between 300 and 490 nm. X.sup..crclbar. may be any anion, but certain classes of anions and certain particular anions are preferred. Aromatic and perfluorinated anions and, in particular dodecylbenzenesulfonate and especially perfluoro(ethylcyclohexane sulfonate) are preferred on account of their solubilizing power, but simpler anions such as iodide, chloride, bromide, methylsulfate, perchlorate and the like may also be used.

8. 发明授权

US5240780A Colored salts of polymeric sulfonate polyanions and dye cations, and light-absorbing coatings made therewith 失效
标题翻译：聚合磺酸盐聚阴离子和染料阳离子的有色盐和由其制成的光吸收涂层
公开(公告)号：US5240780A
公开(公告)日：1993-08-31
申请号：US771514
申请日：1991-10-02
申请人： George V. D. Tiers , Percy C. Hughes, III
发明人： George V. D. Tiers , Percy C. Hughes, III
IPC分类号： C09B69/06 , C09B69/10 , G03F1/68
CPC分类号： G03F1/68 , C09B69/06 , C09B69/10 , Y10T428/28 , Y10T428/2848 , Y10T428/31797 , Y10T428/31855
摘要： Light-stable film-forming salts of a sulfonated polymer, especially a sulfonated polyester, and a cationic dye. When these dye-polysalts are coated onto shaped polymeric structures, especially transparent self-supporting films, the resultant products have important optical uses. A polyester film coated with certain red or amber blends of dye-polysalts and provided with a pressure-sensitive adhesive coating is useful as a lithographers' tape.
摘要翻译：磺化聚合物，特别是磺化聚酯和阳离子染料的光稳定成膜盐。当这些染料多聚物涂覆在成型的聚合物结构，特别是透明的自支撑膜上时，所得产品具有重要的光学用途。涂有一些红色或琥珀色的染料 - 多聚物混合物并提供压敏粘合剂涂层的聚酯薄膜可用作平版印刷胶带。

9. 发明授权

US4978731A Process for fluorimetric monitoring of functional coatings and compositions and fluorescent agents therefor 失效
标题翻译：功能性涂料及其组合物和荧光剂的荧光测定方法
公开(公告)号：US4978731A
公开(公告)日：1990-12-18
申请号：US474461
申请日：1990-02-02
申请人： Kurt C. Melancon , George V. D. Tiers
发明人： Kurt C. Melancon , George V. D. Tiers
IPC分类号： C09K11/06 , G01N21/64 , G01N21/84 , G01N21/95
CPC分类号： G01N21/64 , C09K11/06 , G01N2021/6439 , G01N2021/8427
摘要： A method for monitoring the coating weight, uniformity, defects or markings present in a coating of a composition applied to a substrate comprises the steps:(a) providing a substrate with a functional coating of a composition comprising an effective amount of uvescer that absorbs radiant energy, i.e., has excitation energy, of wavelength .lambda..sub.1 and emits radiant energy of wavelength .lambda..sub.2 ;(b) scanning the coating with radiant energy having a wavelength within wavelength .lambda..sub.1 ;(c) detecting the radiant energy of wavelength .lambda..sub.2 emitted by the coating; and(d) optionally, correlating the emitted radiant energy to independently measured standard coating weights or thicknesses, of the coating so as to measure coating weight, thickness, uniformity, defects, or markings.The invention also provides novel siloxane polymers containing fluorene uvaphores which are useful in the coating comopsition of the invention.
摘要翻译：用于监测施用于基材的组合物的涂层中存在的涂层重量，均匀性，缺陷或标记的方法包括以下步骤：（a）向基底提供包含有效量的吸收辐射的清洁剂的组合物的功能性涂层能量，即具有波长λ1的激发能，并发射波长λ2的辐射能; （b）用波长λ1的辐射能扫描涂层; （c）检测由涂层发射的波长λ2的辐射能; 和（d）任选地，将所发射的辐射能量与涂层的独立测量的标准涂层重量或厚度相关联，以便测量涂层重量，厚度，均匀性，缺陷或标记。本发明还提供了可用于本发明的涂料组合的含有芴uvap的新的硅氧烷聚合物。

10. 发明授权

US4267213A Sulfonato-organosilanol compounds and aqueous solutions thereof 失效
标题翻译：磺酸 - 有机硅烷醇化合物及其水溶液
公开(公告)号：US4267213A
公开(公告)日：1981-05-12
申请号：US83465
申请日：1979-10-10
申请人： Boyd R. Beck , Frank T. Sher , George V. D. Tiers
发明人： Boyd R. Beck , Frank T. Sher , George V. D. Tiers
IPC分类号： C03C17/30 , C04B41/49 , C07F7/08 , C09C1/30 , C07F7/02
CPC分类号： C07F7/0836 , C03C17/30 , C04B41/4927 , C04B41/4938 , C04B41/4944 , C04B41/4966 , C09C1/3081 , C01P2004/80 , C01P2006/90 , C04B2111/00439
摘要： Sulfonato-organosilanol compounds and aqueous solutions and compositions thereof are provided which have at least one sulfonato-organic substituent therein. The weight percentage of oxygen in the compounds is at least about 30% and the weight percentage of silicon in the compounds is not greater than about 15%, these percentages being taken with reference to the water-free acid form of the compounds. Hydrophilic siliceous surfaces and processes for imparting hydrophilicity to such surfaces are also provided.
摘要翻译：提供了磺酸 - 有机硅烷醇化合物及其水溶液及其组合物，其中具有至少一个磺酸 - 有机取代基。化合物中氧的重量百分数至少为约30％，化合物中硅的重量百分数不大于约15％，这些百分比参考化合物的无水酸形式。还提供亲水性硅质表面和赋予这些表面亲水性的方法。

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