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1. 发明授权

US4929646A Polyurethane foam prepared using high functionality cell openers 失效
标题翻译：使用高功能性开孔剂制备聚氨酯泡沫
公开(公告)号：US4929646A
公开(公告)日：1990-05-29
申请号：US270178
申请日：1988-11-14
申请人： Jerram B. Nichols , Douglas L. Hunter , Ronald M. Herrington , John F. Serratelli , David G. Carey
发明人： Jerram B. Nichols , Douglas L. Hunter , Ronald M. Herrington , John F. Serratelli , David G. Carey
IPC分类号： C08J9/02 , C08G18/40 , C08G18/48 , C08G18/50 , C08G65/28 , C08J9/12
CPC分类号： C08G18/4804 , C08G18/4018 , C08G18/4072 , C08G18/4837 , C08G2101/0008 , C08G2101/0041 , Y10S521/914
摘要： Flexible polyurethane foams are prepared using certain high molecular weight, high functionality poly(oxyethylene) compounds as cell openers and softeners. These high functionality polyether polyols have been found to be very effective in opening the cells of the foam, even when used in making foams based on PIPA polyols, which are notoriously closed-celled. They are also quite effective in softening foams made using MDI-based polyisocyanates.

2. 发明授权

US4863976A Polyurethane foam prepared using high functionalilty cell openers 失效
标题翻译：使用高功能性开孔剂制备聚氨酯泡沫
公开(公告)号：US4863976A
公开(公告)日：1989-09-05
申请号：US186418
申请日：1988-04-26
申请人： Jerram B. Nichols , Ronald M. Herrington , Douglas L. Hunter , John F. Serratelli , David G. Carey
发明人： Jerram B. Nichols , Ronald M. Herrington , Douglas L. Hunter , John F. Serratelli , David G. Carey
IPC分类号： C08G18/40 , C08G18/48
CPC分类号： C08G18/4072 , C08G18/4018 , C08G18/4804 , C08G18/4837 , C08G18/632 , C08G2101/0008 , C08G2101/0041 , Y10S521/914
摘要： Flexible polyurethane foams are prepared using certain high molecular weight, high functionality poly(oxyethylene) compounds as cell openers and softeners. These high functionality polyether polyols have been found to be very effective in opening the cells of the foam, even when used in making foams based on PIPA polyols, which are notoriously closed-celled. They are also quite effective in softening foams made using MDI-based polyisocyanates.
摘要翻译：使用某些高分子量，高官能度的聚（氧乙烯）化合物作为细胞开放剂和软化剂制备柔性聚氨酯泡沫。已经发现，这些高官能度聚醚多元醇在打开泡沫细胞方面非常有效，即使在制造基于众所周知的封闭细胞的PIPA多元醇制造泡沫体时也是如此。它们在使用基于MDI的多异氰酸酯制成的泡沫体也是非常有效的。

3. 发明授权

US4632943A Polyurethane foams prepared from alkyl dialkanol amine-containing polyols 失效
标题翻译：由烷基二链烷醇胺多元醇制备的聚氨酯泡沫
公开(公告)号：US4632943A
公开(公告)日：1986-12-30
申请号：US725608
申请日：1985-04-22
申请人： Jerram B. Nichols
发明人： Jerram B. Nichols
IPC分类号： C08G18/32 , C08G18/65 , C08G18/14
CPC分类号： C08G18/6535 , C08G18/3275 , C08G18/3287 , C08G18/329
摘要： Polyurethane foams are prepared by reacting a polyisocyanate and a polyahl in the presence of water and a dialkanol tertiary amine. The foams are rigid, useful for thermal insulation in roofs, walls, refrigerators, etc., and are capable of filling mold space completely on foaming (good flowability) without shrinking excessively.
摘要翻译：聚氨酯泡沫体是通过在水和二烷醇叔胺的存在下使多异氰酸酯和聚芳醚反应来制备的。泡沫是刚性的，可用于屋顶，墙壁，冰箱等中的隔热，并且能够在发泡（良好的流动性）下完全填充模具空间而不会过度收缩。

4. 发明授权

US5240635A Composition of flexible polyurethane foams blown using reduced amounts of chlorofluorocarbon blowing agents and method for preparation 失效
标题翻译：使用减少量的氯氟烃发泡剂吹制的柔性聚氨酯泡沫的组成及其制备方法
公开(公告)号：US5240635A
公开(公告)日：1993-08-31
申请号：US929741
申请日：1992-08-13
申请人： Ricardo DeGenova , Jerram B. Nichols
发明人： Ricardo DeGenova , Jerram B. Nichols
IPC分类号： C08G18/10 , C08G18/40 , C08G18/48 , C08G18/80
CPC分类号： C08G18/8019 , C08G18/10 , C08G18/4072 , C08G18/4812 , C08G18/4841 , C08G2101/0008 , C08G2101/0083
摘要： Flexible polyurethane foams prepared from formulations requiring reduced amounts of chlorofluorocarbon blowing agents are disclosed. The foams can be prepared without undesirable loss of physical properties with formulations comprising an "A" component which is a blend of a polymethylene polydiphenyldiisccyanate and a methylene diphenyldiisocyanate prepolymer wherein the methylene diphenyldiisocyanate prepolymer is prepared from a prepolymer formulation containing an active hydrogen containing compound which has an equivalent weight of about 30 to about 600; a "B" component which includes an active hydrogen containing compound; and a carbon dioxide generating blowing agent. Also disclosed are polyisocyanate blends consisting of polymethylene polydiphenyldiisocyanate and methylene diphenyldiisocyanate prepolymers useful for preparing flexible polyurethane foams. Methods of preparing both the foams and the polyisocyanate blends are also disclosed. The foams of the present invention can be prepared to have improved tensile and tear values. Formulations of the present invention also display advantageously improved processing characteristics such as flowability.
摘要翻译：公开了由需要减少量的氯氟烃发泡剂的制剂制备的柔性聚氨酯泡沫体。可以制备不含有物理性质损失的泡沫，其中包含“A”组分的制剂是由聚亚甲基多二苯基二氰基氰化物和亚甲基二苯基二异氰酸酯预聚物的共混物组成的，其中亚甲基二苯基二异氰酸酯预聚物由含有活性氢化合物的预聚物制剂制备，具有约30至约600的当量; 包含含活性氢的化合物的“B”成分; 和发生二氧化碳的发泡剂。还公开了由聚亚甲基聚二苯基二异氰酸酯和用于制备柔性聚氨酯泡沫的亚甲基二苯基二异氰酸酯预聚物组成的多异氰酸酯共混物。还公开了制备泡沫和多异氰酸酯共混物的方法。本发明的泡沫可以被制备成具有改善的拉伸和撕裂值。本发明的制剂还显示出有利地改进的加工特性，例如流动性。

5. 发明授权

US5200435A Composition of flexible polyurethane foams blown using reduced amouns of chlorofluorocarbon blowing agents and method for preparation 失效
标题翻译：使用减少氟氯烃发泡剂吹制的柔性聚氨酯泡沫的组成及其制备方法
公开(公告)号：US5200435A
公开(公告)日：1993-04-06
申请号：US757862
申请日：1991-09-11
申请人： Ricardo DeGenova , Jerram B. Nichols
发明人： Ricardo DeGenova , Jerram B. Nichols
IPC分类号： C08G18/10 , C08G18/40 , C08G18/48 , C08G18/80
CPC分类号： C08G18/8019 , C08G18/10 , C08G18/4072 , C08G18/4812 , C08G18/4841 , C08G2101/0008 , C08G2101/0083
摘要： Flexible polyurethane foams prepared from formulations requiring reduced amounts of chlorofluorocarbon blowing agents are disclosed. The foams can be prepared without undesirable loss of physical properties with formulations comprising an "A" component which is a blend of a polymethylene polydiphenyldiisocyanate and a methylene diphenyldiisocyanate prepolymer wherein the methylene diphenyldiisocyanate prepolymer is prepared from a prepolymer formulation containing an active hydrogen containing compound which has an equivalent weight of about 30 to about 600; a "B" component which includes an active hydrogen containing compound; and a carbon dioxide generating blowing agent. Also disclosed are polyisocyanate blends consisting of polymethylene polydiphenyldiisocyanate and methylene diphenyldiisocyanate prepolymers useful for preparing flexible polyurethane foams. Methods of preparing both the foams and the polyisocyanate blends are also disclosed. The foams of the present invention can be prepared to have improved tensile and tear values. Formulations of the present invention also display advantageously improved processing characteristics such as flowability.
摘要翻译：公开了由需要减少量的氯氟烃发泡剂的制剂制备的柔性聚氨酯泡沫体。可以用不含有物理性质的物质损失制备泡沫体，其中包含“A”组分的制剂是一种多亚甲基聚二苯基二异氰酸酯和亚甲基二苯基二异氰酸酯预聚物的混合物，其中亚甲基二苯基二异氰酸酯预聚物由含有活性氢化合物的预聚物制剂制备，具有约30至约600的当量; 包含含活性氢的化合物的“B”成分; 和发生二氧化碳的发泡剂。还公开了由聚亚甲基聚二苯基二异氰酸酯和用于制备柔性聚氨酯泡沫的亚甲基二苯基二异氰酸酯预聚物组成的多异氰酸酯共混物。还公开了制备泡沫体和多异氰酸酯共混物的方法。本发明的泡沫可以被制备成具有改善的拉伸和撕裂值。本发明的制剂还显示出有利地改进的加工特性，例如流动性。

6. 发明授权

US5164423A Composition of flexible polyurethane foams below using reduced amounts of chlorofluorocarbone blowing agents and method for preparation 失效
标题翻译：下面使用减少量的氯氟代烃发泡剂的柔性聚氨酯泡沫的组成及其制备方法
公开(公告)号：US5164423A
公开(公告)日：1992-11-17
申请号：US834172
申请日：1992-02-06
申请人： Ricardo De Genova , Jerram B. Nichols
发明人： Ricardo De Genova , Jerram B. Nichols
IPC分类号： C08G18/10 , C08G18/40 , C08G18/48 , C08G18/80
CPC分类号： C08G18/8019 , C08G18/10 , C08G18/4072 , C08G18/4812 , C08G18/4841 , C08G2101/0008 , C08G2101/0083
摘要： Flexible polyurethane foams prepared from formulations requiring reduced amounts of chlorofluoro-carbon blowing agents are disclosed. The foams can be prepared without undesirable loss of physical properties with formulations comprising an "A" component which is a blend of a polymethylene polydiphenyldiisocyanate and a methylene diphenyldiisocyanate prepolymer wherein the methylene diphenyldiisocyanate prepolymer is prepared from a prepolymer formulation containing an active hydrogen containing compound which has an equivalent weight of about 30 to about 600; a "B" component which includes an active hydrogen containing compound; and a carbon dioxide generating blowing agent. Also disclosed are polyisocyanate blends consisting of polymethylene polydiphenyldiisocyanate and methylene diphenyldiisocyanate prepolymers useful for preparing flexible polyurethane foams. Methods of preparing both the foams and the polyisocyanate blends are also disclosed. The foams of the present invention can be prepared to have improved tensile and tear values. Formulations of the present invention also display advantageously improved processing characteristics such as flowability.
摘要翻译：公开了由需要减少量的氯氟碳发泡剂的制剂制备的柔性聚氨酯泡沫。可以用不含有物理性质的物质损失来制备泡沫，其中包含“A”组分的制剂是一种聚亚甲基聚二苯基二异氰酸酯和亚甲基二苯基二异氰酸酯预聚物的混合物，其中亚甲基二苯基二异氰酸酯预聚物由含有活性氢化合物的预聚物制剂制备，具有约30至约600的当量; 包含含活性氢的化合物的“B”成分; 和发生二氧化碳的发泡剂。还公开了由聚亚甲基聚二苯基二异氰酸酯和用于制备柔性聚氨酯泡沫的亚甲基二苯基二异氰酸酯预聚物组成的多异氰酸酯共混物。还公开了制备泡沫和多异氰酸酯共混物的方法。本发明的泡沫可以被制备成具有改善的拉伸和撕裂值。本发明的制剂还显示出有利地改进的加工特性，例如流动性。

7. 发明授权

US5600019A Polyisocyanate based polymers perpared from formulations including non-silicone surfactants and method for the preparation thereof 失效
标题翻译：从含有非硅氧烷表面活性剂的制剂制备的聚异氰酸酯基聚合物及其制备方法
公开(公告)号：US5600019A
公开(公告)日：1997-02-04
申请号：US342299
申请日：1994-11-23
申请人： Debkumar Bhattacharjee , Jerram B. Nichols , Warren A. Kaplan , Vaughn M. Nace
发明人： Debkumar Bhattacharjee , Jerram B. Nichols , Warren A. Kaplan , Vaughn M. Nace
IPC分类号： C08L71/00 , C08G18/00 , C08G18/08 , C08G18/28 , C08G18/40 , C08G18/48 , C08G101/00 , C08J9/00 , C08L75/00 , C08L75/04 , C09K3/00 , C07C43/11
CPC分类号： C08J9/0061 , C08G18/283 , C08G18/4018 , C08G18/4812 , C08G18/4854 , C08G2101/0025 , C08G2101/005 , C08J2375/04 , C08J2471/00 , Y10S516/01
摘要： Polyurethane, polyisocyanurate and polyurea polymers, particularly foamed polymers can be prepared from formulations including non-silicone polyether surfactants. The non-silicone polyether surfactants can be polyethers having from about 10 to about 90 weight percent oxyethylene units and from about 10 to about 90 weight percent oxyalkylene units having at least 4 carbons. The non-silicone polyether surfactants can be used to prepare foams having properties substantially similar to foams prepared with conventional silicone based surfactants.
摘要翻译：聚氨酯，聚异氰脲酸酯和聚脲聚合物，特别是泡沫聚合物可以由包括非硅氧烷聚醚表面活性剂的制剂制备。非硅氧烷聚醚表面活性剂可以是具有约10至约90重量％氧化乙烯单元和约10至约90重量％具有至少4个碳的氧化烯单元的聚醚。非硅氧烷聚醚表面活性剂可用于制备具有基本上类似于用常规硅氧烷基表面活性剂制备的泡沫的性质的泡沫体。

8. 发明授权

US5674918A Polyisocyanate based polymers prepare from formulations including non-silicone surfactants and method for the preparation thereof 失效
标题翻译：基于多异氰酸酯的聚合物由包括非硅氧烷表面活性剂的制剂和由其制备的方法制备
公开(公告)号：US5674918A
公开(公告)日：1997-10-07
申请号：US701369
申请日：1996-08-22
申请人： Debkumar Bhattacharjee , Jerram B. Nichols , Warren A. Kaplan , Vaughn M. Nace
发明人： Debkumar Bhattacharjee , Jerram B. Nichols , Warren A. Kaplan , Vaughn M. Nace
IPC分类号： C08L71/00 , C08G18/00 , C08G18/08 , C08G18/28 , C08G18/40 , C08G18/48 , C08G101/00 , C08J9/00 , C08L75/00 , C08L75/04 , C08J9/04 , C08G18/30
CPC分类号： C08J9/0061 , C08G18/283 , C08G18/4018 , C08G18/4812 , C08G18/4854 , C08G2101/0025 , C08G2101/005 , C08J2375/04 , C08J2471/00 , Y10S516/01
摘要： Polyurethane, polyisocyanurate and polyurea polymers, particularly foamed polymers can be prepared from formulations including non-silicone polyether surfactants. The non-silicone polyether surfactants can be polyethers having from about 10 to about 90 weight percent oxyethylene units and from about 10 to about 90 weight percent oxyalkylene units having at least 4 carbons. The non-silicone polyether surfactants can be used to prepare foams having properties substantially similar to foams prepared with conventional silicone based surfactants.
摘要翻译：聚氨酯，聚异氰脲酸酯和聚脲聚合物，特别是泡沫聚合物可以由包括非硅氧烷聚醚表面活性剂的制剂制备。非硅氧烷聚醚表面活性剂可以是具有约10至约90重量％氧化乙烯单元和约10至约90重量％具有至少4个碳的氧化烯单元的聚醚。非硅氧烷聚醚表面活性剂可用于制备具有基本上类似于用常规硅氧烷基表面活性剂制备的泡沫的性质的泡沫体。

9. 发明授权

US4722942A Flexible polyurethane foams which exhibit excellent flame resistance 失效
标题翻译：具有优异阻燃性的柔性聚氨酯泡沫
公开(公告)号：US4722942A
公开(公告)日：1988-02-02
申请号：US19904
申请日：1987-02-27
申请人： Jerram B. Nichols , Hans R. Friedli , Stephen R. Burks
发明人： Jerram B. Nichols , Hans R. Friedli , Stephen R. Burks
IPC分类号： C08G18/38 , C08G18/65 , C08G18/32
CPC分类号： C08G18/3823 , C08G18/6523
摘要： This invention is an active hydrogen-containing composition suitable for the production of flexible polyurethane foam when reacted with a polyisocyanate, said composition comprising,(a) a polyol having an average functionality of about 2.0 to about 4.0, having at least about 50% of its active hydroxyl groups in the form of primary hydroxyl groups, and an equivalent weight from about 500 to about 5000;(b) from about 0.5 to about 5 parts, per 100 parts by weight of component (a) of a crosslinker selected from the group consisting of monoethanolamine, diethanolamine, triethanolamine, monoisopropanolamine, diisopropanolamine, methylene bis(o-chloroaniline) and mixtures thereof; and(c) at least about 0.15 equivalent per equivalent of (a) and (b), of a polyfunctional flame retarding additive having an equivalent weight of less than about 300, which flame retarding additive is selected from the group consisting of (i) hydroxyl-terminated alkanes having a plurality of primary hydroxyl groups, (ii) alkylene ethers and polyethers having a plurality of primary hydroxyl groups, (iii) polyurea compounds having at least 2 hydroxyalkyl groups which are attached to a urea nitrogen atom, (iv) polycarbamates having a plurality of primary hydroxyl groups or a plurality of primary hydroxyalkyl groups attached to a tertiary nitrogen atoms.Foams prepared from this active hydrogen-containing composition have excellent burn properties, as determined by tests described herein, as well as good physical properties.
摘要翻译：本发明是一种适用于在与多异氰酸酯反应时生产柔性聚氨酯泡沫的活性含氢组合物，所述组合物包含（a）平均官能度为约2.0至约4.0的多元醇，其具有至少约50％其活性羟基为伯羟基，当量为约500至约5000; （a）交联剂的组分（a）为约0.5至约5份，选自单乙醇胺，二乙醇胺，三乙醇胺，单异丙醇胺，二异丙醇胺，亚甲基双（邻氯苯胺）及其混合物 ; 和（c）当量重量小于约300的多官能阻燃添加剂中每当量（a）和（b））至少约0.15当量，该阻燃添加剂选自（i）具有多个伯羟基的羟基封端的烷烃，（ii）具有多个伯羟基的亚烷基醚和聚醚，（iii）与脲氮原子连接的具有至少2个羟烷基的聚脲化合物，（iv）具有多个伯羟基的多氨基甲酸盐或与叔氮原子连接的多个伯羟基烷基。由该活性含氢组合物制备的泡沫体具有优异的燃烧性能，如通过本文所述的测试确定的，以及良好的物理性能。

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