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1. 发明申请

US20050258578A1 Method for producing high purity low dielectric constant ceramic and hybrid ceramic films field of the invention 失效
标题翻译：本发明制备高纯度低介电常数陶瓷和复合陶瓷薄膜领域的方法
公开(公告)号：US20050258578A1
公开(公告)日：2005-11-24
申请号：US10489924
申请日：2001-09-14
申请人： Jerome Birnbaum , Glen Fryxell , Shari Xiaohong , Christopher Coyle , Glen Dunham , Suresh Baskaran , Ralph Williford
发明人： Jerome Birnbaum , Glen Fryxell , Shari Xiaohong , Christopher Coyle , Glen Dunham , Suresh Baskaran , Ralph Williford
IPC分类号： C04B38/06 , B28B1/30 , B28B11/00 , C01B33/12 , C04B20/00 , C04B33/32 , C04B35/14 , C04B35/16 , C04B35/624 , C04B38/00 , C04B38/10 , C04B41/80 , H01L21/316
CPC分类号： C04B35/62655 , B01D67/0048 , B01D67/0058 , B01D67/0088 , B01D67/0093 , B01D71/024 , B01D2323/18 , B01D2323/30 , C04B20/0056 , C04B35/14 , C04B35/16 , C04B35/624 , C04B38/0022 , C04B2111/00482 , C04B2111/1025 , C04B2235/72 , H01L21/31695 , C04B38/0051 , C04B38/009 , C04B38/02 , C04B38/10 , C04B14/4631
摘要： Porous ceramic and hybrid ceramic films are useful as low dielectric constant interlayers in semiconductor interconnects. (Hybrid ceramic films are defined as films that contain organic and ceramic molecular components in the structure, as, for example, organosilicates). This invention describes the usefulness of humidity treatments (using specific temperature/humidity treatments as illustrative examples) in increasing mechanical integrity of porous dielectric films with minimal detrimental effect on film porosity or dielectric constant and with no adverse impact on film quality. The efficacy of such treatments is illustrated using surfactant-templated mesoporous silicate films as an example. This invention also describes a specific family of additives to be used with highly pure alkali-metal-free ceramic and hybrid precursors for such dielectric films that will enable better control of the film porosity and quality and lower dielectric constants with the required mechanical integrity. The efficacy of such additives is illustrated using surfactant-templated mesoporous silicate films as a model example. The invention should be broadly applicable to any cross-linked ceramic or hybrid ceramic films (including silicate and organosilicate films, and especially highly porous forms of the films for low-dielectric constant applications). The invention has been found to be particularly effective with surfactant-templated silicate films with nanometer-scale porosity. The invention in either embodiment should also be applicable to evaporation-induced formation of other cross-linked shapes such as fibers and powders.
摘要翻译：多孔陶瓷和混合陶瓷膜可用作半导体互连中的低介电常数中间层。（混合陶瓷膜被定义为在结构中含有有机和陶瓷分子组分的膜，例如有机硅酸盐）。本发明描述了在增加多孔电介质膜的机械完整性的情况下，湿度处理（使用特定温度/湿度处理作为说明性实例）的有用性，对膜孔隙率或介电常数具有最小的有害影响，并且对膜质量没有不利影响。以表面活性剂模板的介孔硅酸盐膜为例说明了这种处理的效果。本发明还描述了与用于这种介电膜的高纯度无碱金属的陶瓷和混合前体一起使用的特定的添加剂族，其将能够以所需的机械完整性更好地控制膜孔隙率和质量以及更低的介电常数。作为示例，使用表面活性剂模板的中孔硅酸盐膜来说明这些添加剂的功效。本发明应广泛适用于任何交联的陶瓷或混合陶瓷膜（包括硅酸盐和有机硅酸盐膜，特别是用于低介电常数应用的膜的高度多孔形式）。已经发现本发明对于具有纳米级孔隙率的表面活性剂模板化硅酸盐膜是特别有效的。在任一实施方案中的本发明也应适用于其它交联形状如纤维和粉末的蒸发诱导形成。

2. 发明申请

US20060063057A1 High strength insulating metal-to-metal joints for solid oxide fuel cells and other high temperature applications and method of making 审中-公开
标题翻译：用于固体氧化物燃料电池的高强度绝缘金属 - 金属接头和其他高温应用和制造方法
公开(公告)号：US20060063057A1
公开(公告)日：2006-03-23
申请号：US10948359
申请日：2004-09-22
申请人： K. Weil , Lawrence Chick , Christopher Coyle , John Hardy , Guanguang Xia , Kerry Meinhardt , Vincent Sprenkle , Dean Paxton
发明人： K. Weil , Lawrence Chick , Christopher Coyle , John Hardy , Guanguang Xia , Kerry Meinhardt , Vincent Sprenkle , Dean Paxton
IPC分类号： H01M2/02
CPC分类号： H01M8/0282 , C03C8/24 , C03C29/00 , H01M8/0286 , H01M8/1246 , Y02E60/525 , Y02P70/56
摘要： A seal formed between a metal part and a second part that will remain gas tight in high temperature operating environments which experience frequent thermal cycling, which is particularly useful as an insulating joint in solid oxide fuel cells. A first metal part is attached to a reinforcing material. A glass forming material in the positioned in between the first metal part and the second part, and a seal is formed between the first metal part and the second part by heating the glass to a temperature suitable to melt the glass forming materials. The glass encapsulates and bonds at least a portion of the reinforcing material, thereby adding tremendous strength to the overall seal. A ceramic material may be added to the glass forming materials, to assist in forming an insulating barrier between the first metal part and the second part and to regulating the viscosity of the glass during the heating step.
摘要翻译：形成在金属部件和第二部件之间的密封件，其将在经受频繁热循环的高温操作环境中保持气密，这在固体氧化物燃料电池中作为绝缘接头特别有用。第一金属部件附接到增强材料。定位在第一金属部分和第二部分之间的玻璃形成材料，并且通过将玻璃加热到适于熔化玻璃形成材料的温度，在第一金属部分和第二部分之间形成密封。玻璃封装并粘合至少一部分增强材料，从而为整个密封件增加了巨大的强度。陶瓷材料可以添加到玻璃形成材料中，以有助于在第一金属部分和第二部分之间形成绝缘屏障，并且在加热步骤期间调节玻璃的粘度。

3. 发明申请

US20060060633A1 High strength insulating metal-to-ceramic joints for solid oxide fuel cells and other high temperature applications and method of making 审中-公开
标题翻译：用于固体氧化物燃料电池的高强度绝缘金属 - 陶瓷接头和其他高温应用和制造方法
公开(公告)号：US20060060633A1
公开(公告)日：2006-03-23
申请号：US10948346
申请日：2004-09-22
申请人： K. Weil , Lawrence Chick , Christopher Coyle , John Hardy , Guanguang Xia , Kerry Meinhardt , Vincent Sprenkle , Dean Paxton
发明人： K. Weil , Lawrence Chick , Christopher Coyle , John Hardy , Guanguang Xia , Kerry Meinhardt , Vincent Sprenkle , Dean Paxton
IPC分类号： H01M2/02
CPC分类号： C04B37/023 , B32B2311/22 , B32B2311/30 , C04B35/01 , C04B35/013 , C04B37/025 , C04B2235/3246 , C04B2235/3279 , C04B2235/424 , C04B2235/6025 , C04B2237/10 , C04B2237/34 , C04B2237/405 , C04B2237/406 , H01J49/025 , H01M8/0271 , H01M8/0282 , H01M8/0286 , Y02P70/56
摘要： A seal formed between a metal part and a second part that will remain gas tight in high temperature operating environments which experience frequent thermal cycling, which is particularly useful as an insulating joint in solid oxide fuel cells. A first metal part is attached to an reinforcing material. A glass forming material in the positioned in between the first metal part and the second part, and a seal is formed between the first metal part and the second part by heating the glass to a temperature suitable to melt the glass forming materials. The glass encapsulates and bonds at least a portion of the reinforcing material, thereby adding tremendous strength to the overall seal. A ceramic material may be added to the glass forming materials, to assist in forming an insulating barrier between the first metal part and the second part and to regulating the viscosity of the glass during the heating step.
摘要翻译：形成在金属部件和第二部件之间的密封件，其将在经受频繁热循环的高温操作环境中保持气密，这在固体氧化物燃料电池中作为绝缘接头特别有用。第一金属部件附接到增强材料。定位在第一金属部分和第二部分之间的玻璃形成材料，并且通过将玻璃加热到适于熔化玻璃形成材料的温度，在第一金属部分和第二部分之间形成密封。玻璃封装并粘合至少一部分增强材料，从而为整个密封件增加了巨大的强度。陶瓷材料可以添加到玻璃形成材料中，以有助于在第一金属部分和第二部分之间形成绝缘屏障，并且在加热步骤期间调节玻璃的粘度。

4. 发明申请

US20070010146A1 Integrated flow systems 审中-公开
标题翻译：集成流量系统
公开(公告)号：US20070010146A1
公开(公告)日：2007-01-11
申请号：US11175532
申请日：2005-07-05
申请人： Randal Richenberg , Christopher Coyle
发明人： Randal Richenberg , Christopher Coyle
IPC分类号： B63B1/00
CPC分类号： B63B1/18 , B63B2001/186
摘要： A device for improving speed, control, and performance of water sports craft achieved by capturing lateral water flow and redirecting water flow longitudinally thereby increasing speed and control. The apparatus is designed to be attached to the underside of a water sports craft in the aft area by means of P.S.A. The invention consists of triangular shaped ridges or elevated ridges extending downward from the bottom surface of craft with a tapered leading entry point and exit point (FIGS. 1, 2, 3) consisting of a smooth flexible plastic. The invention can be applied in various configurations and locations on the underside of a water vehicle to achieve desired effect. Invention requires installer to first clean surface that invention is to be applied to. A desirable configuration must first be obtained before removing the protective adhesive backing and then applying with firm pressure for proper bond.
摘要翻译：一种用于提高水上运动工具的速度，控制和性能的装置，通过捕获横向水流和纵向重新定向水流，从而提高速度和控制。该设备被设计成通过P.S.A在后方附接到水上运动工具的下侧。本发明由三角形脊或从工艺底面向下延伸的升高的脊组成，其具有由柔性柔性塑料组成的锥形前进入口点和出口点（图1，图2，图3）。本发明可以应用在水车辆的下侧上的各种构造和位置中以实现期望的效果。本发明要求安装者首先清洁要应用的发明的表面。必须首先在去除保护性粘合剂背衬之前获得理想的配置，然后以稳定的压力施加适当的粘合。

5. 发明授权

US5604582A Methods and apparatus for taking spectroscopic measurements of sediment layers beneath a body of water 失效
标题翻译：用于对水体下面的沉积层进行光谱测量的方法和装置
公开(公告)号：US5604582A
公开(公告)日：1997-02-18
申请号：US395515
申请日：1995-02-27
申请人： Donald C. Rhoads , Christopher Coyle , Roger Ward , Gregory Mooradian , Richard Anderson
发明人： Donald C. Rhoads , Christopher Coyle , Roger Ward , Gregory Mooradian , Richard Anderson
IPC分类号： E21B47/00 , G01N21/31 , G01N21/64 , G01V8/02 , G01N21/27
CPC分类号： G01N21/6456 , G01J3/2823 , G01N21/31 , G01N2021/6419 , G01N2021/6423
摘要： A spectrometer system includes a processing center, an underwater remote sensor and a communication link coupled therebetween. The sensor is deployed to at least partially penetrate a sediment layer disposed beneath a body of water. The sensor includes a window defining a sediment window plane through which a profile of the sediment layer is observable and a camera, an image plane of which is a conjugate of the window, the camera imaging light from objects in the sediment window plane to generate imagewise data, the imagewise data being transmitted over the communications link to the processing center. The sensor also includes at least one removable cell disposed in the sediment window plane, each removable cell being comprised of a transparent solid material having a void therein, the void in each removable cell for holding a standard material corresponding to the respective removable cell. The sensor further includes a camera filter device having at least one camera filter. Each camera filter is characterized as passing radiant energy within a corresponding emission band of camera wavelengths, the camera filter device being controllable to select a current camera filter. The sensor further includes an illumination source to produce radiant energy and an illumination filter device having at least one illumination filter. Each illumination filter is characterized as passing radiant energy within a corresponding illumination band of wavelengths. The sensor further includes a blocking filter device having at least one blocking filter, each blocking filter being synchronously coordinated with a corresponding illumination filter to block light in the illumination band from reaching the camera.
摘要翻译：光谱仪系统包括处理中心，水下远程传感器和耦合在其间的通信链路。传感器被部署以至少部分地穿透设置在水体下方的沉积物层。该传感器包括一个窗口，其界定了可观察到沉积物层的轮廓的沉积物窗平面，以及一个摄像机，其图像平面是窗口的共轭，来自沉积物窗平面中的物体的照相机成像光，以产生成像数据，图像数据通过通信链路发送到处理中心。该传感器还包括设置在沉积物窗平面中的至少一个可拆卸电池，每个可拆卸电池由其中具有空隙的透明固体材料构成，每个可移除电池中的空隙用于保持对应于可移除电池的标准材料。传感器还包括具有至少一个相机滤光器的相机滤光器装置。每个相机滤镜的特征在于在照相机波长的相应发射频带内通过辐射能，照相机滤波器装置可控制以选择当前的相机滤镜。传感器还包括产生辐射能的照明源和具有至少一个照明滤光器的照明滤光装置。每个照明滤光器的特征在于在相应的波长的照明带内通过辐射能。传感器还包括具有至少一个阻塞滤波器的阻塞滤波器装置，每个阻塞滤波器与相应的照明滤波器同步协调，以阻挡照明带中的光线到达照相机。

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