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1. 发明申请

US20110136702A1 Wellbore Fluid Additives and Methods of Producing the Same 有权
标题翻译：井筒流体添加剂及其生产方法
公开(公告)号：US20110136702A1
公开(公告)日：2011-06-09
申请号：US12791965
申请日：2010-06-02
申请人： Jeffery R. Harris , Marshall D. Bishop , Jeffery C. Gee , Carleton E. Stouffer
发明人： Jeffery R. Harris , Marshall D. Bishop , Jeffery C. Gee , Carleton E. Stouffer
IPC分类号： C09K8/24 , C08G63/08
CPC分类号： C09K8/508 , C09K8/035
摘要： Disclosed herein is a polymer useful in a method of forming a wellbore fluid additive. This polymer comprises a polyethylene backbone comprising pendant aminoalkylsulfonic acid amides which comprise a carbonyl directly attached to a backbone carbon, and an amide formed via the amine group from the aminoalkylsulfonic acid. Methods of preparing these polymers by addition of the aminoalkylsulfonic acid to a polymeric anhydride are disclosed. Methods related to oil extraction using the wellbore fluid with the additive are also disclosed.
摘要翻译：本文公开了可用于形成井筒流体添加剂的方法中的聚合物。该聚合物包括聚乙烯主链，其包含氨基烷基磺酸酰胺，其包含直接连接到主链碳上的羰基，以及通过氨基烷基磺酸的胺基形成的酰胺。公开了通过将氨基烷基磺酸加入聚合物酸酐制备这些聚合物的方法。还公开了使用具有添加剂的井筒流体进行提油的方法。

2. 发明授权

US07939584B2 Bi-or multi-modal particle size distribution to improve drag reduction polymer dissolution 有权
标题翻译：双模或多模态粒度分布，以提高阻聚剂聚合物溶解度
公开(公告)号：US07939584B2
公开(公告)日：2011-05-10
申请号：US11451741
申请日：2006-06-13
申请人： Jeffery R. Harris , Lu Chien Chou , George G. Ramsay , John F. Motier , Nagesh S. Kommareddi , Thomas Mathew
发明人： Jeffery R. Harris , Lu Chien Chou , George G. Ramsay , John F. Motier , Nagesh S. Kommareddi , Thomas Mathew
IPC分类号： B05D5/08 , C08J5/16 , C09K3/00 , C08F10/00
CPC分类号： C10M171/06 , C09K8/035 , C10L1/10 , C10L1/1616 , C10L1/1641 , C10L1/165 , C10L1/1824 , C10L1/1826 , C10L1/1852 , C10L1/1857 , C10L1/19 , C10L1/1963 , C10L1/1973 , C10L1/207 , C10L10/08 , C10L10/14 , C10L2300/20 , C10M143/00 , C10N2230/00 , F17D1/16 , F17D1/17
摘要： Drag reduction of hydrocarbon fluids flowing through pipelines of various lengths is improved by polyolefin drag reducer dispersions or dispersions using bi- or multi-modal particle size distributions. Drag reducers having larger particle sizes dissolve more slowly than drag reducers having smaller particle sizes. By using at least bi-modal particle size distributions drag reduction can be distributed more uniformly over the length of the pipeline where smaller sized particles dissolve sooner or earlier in the pipeline and larger sized particles dissolve later or further along the pipeline.
摘要翻译：通过使用双模式或多模态粒度分布的聚烯烃阻滞剂分散体或分散体，改善流过各种长度管道的烃流体的减阻。具有较大颗粒尺寸的减阻剂比具有较小粒径的减阻剂溶解得更慢。通过使用至少双模式粒度分布，可以在管道的长度上更均匀地分布阻力减小，其中较小尺寸的颗粒在管道中较早或早期溶解，并且较大尺寸的颗粒在管道之后或之后溶解。

3. 发明授权

US06946500B2 Non-cryogenic process for grinding polyolefin drag reducing agents 有权
标题翻译：用于研磨聚烯烃减阻剂的非低温工艺
公开(公告)号：US06946500B2
公开(公告)日：2005-09-20
申请号：US10322050
申请日：2002-12-17
申请人： Jeffery R. Harris , John F. Motier
发明人： Jeffery R. Harris , John F. Motier
IPC分类号： B29B13/10 , C08J3/12 , C08J3/11
CPC分类号： C08J3/124 , B29B13/10
摘要： A process for producing fine particulate polymer drag reducing agent (DRA) without cryogenic temperatures, is described. The grinding or pulverizing of polymer, such as poly(alpha-olefin) may be achieved by the use of at least one solid organic grinding aid and at least one liquid grinding aid. In one non-limiting embodiment of the invention, the grinding is conducted at ambient temperature. Examples of a solid organic grinding aid include ethene/butene copolymer particles, paraffin waxes and solid alcohols. An example of a suitable liquid grinding aid includes a blend of glycol, water and isopropyl alcohol. Particulate DRA may be produced at a size of about 500 microns or less. Use of an attrition mill is preferred.
摘要翻译：描述了一种在没有低温的情况下生产细颗粒聚合物减阻剂（DRA）的方法。聚合物如聚（α-烯烃）的研磨或粉碎可以通过使用至少一种固体有机研磨助剂和至少一种液体研磨助剂来实现。在本发明的一个非限制性实施方案中，研磨在环境温度下进行。固体有机研磨助剂的实例包括乙烯/丁烯共聚物颗粒，石蜡和固体醇。合适的液体研磨助剂的实例包括二醇，水和异丙醇的共混物。颗粒状DRA可以以约500微米或更小的尺寸生产。优选使用研磨机。

4. 发明授权

US09034800B2 Fluid loss additives and methods of making and using same 有权
标题翻译：流体损失添加剂及其制造和使用方法
公开(公告)号：US09034800B2
公开(公告)日：2015-05-19
申请号：US13250882
申请日：2011-09-30
申请人： Jeffery R. Harris , Frank E. Evans
发明人： Jeffery R. Harris , Frank E. Evans
IPC分类号： C09K8/502 , C09K8/32 , C09K8/64
CPC分类号： C09K8/32 , C08G61/02 , C08G2261/12 , C08G2261/3222 , C08G2261/3327 , C08G2261/72 , C09K8/36 , C09K8/502 , C09K8/64 , E21B21/003 , E21B33/138
摘要： A non-aqueous wellbore servicing fluid comprising a fluid loss additive wherein the fluid loss additive comprises the reaction product of (i) a functional polymer and (ii) an oligomerized fatty acid. A method of conducting an oil-field operation comprising placing a non-aqueous wellbore servicing fluid downhole wherein the non-aqueous wellbore servicing fluid comprises a fluid loss additive comprising the reaction product of (i) a functional polymer and (ii) an oligomerized fatty acid.
摘要翻译：包含流体损失添加剂的非水性井筒维修流体，其中所述流体损失添加剂包含（i）官能聚合物和（ii）低聚脂肪酸的反应产物。一种进行油田操作的方法，包括在井下放置非水井筒维修流体，其中非水井筒维修流体包括流体损失添加剂，其包含（i）官能聚合物和（ii）低聚脂肪酸。

5. 发明授权

US08575072B2 Fluid loss additives and methods of making and using same 有权
公开(公告)号：US08575072B2
公开(公告)日：2013-11-05
申请号：US13248715
申请日：2011-09-29
申请人： Jeffery R. Harris , Frank E. Evans
发明人： Jeffery R. Harris , Frank E. Evans
IPC分类号： C09K8/588
CPC分类号： C09K8/36 , C09K8/502 , C09K8/588 , C09K8/64
摘要： A non-aqueous wellbore servicing fluid comprising a fluid loss additive wherein the fluid loss additive comprises the reaction product of (i) a functional polymer and (ii) an oligomerized fatty acid. A method of conducting an oil-field operation comprising placing a non-aqueous wellbore servicing fluid downhole wherein the non-aqueous wellbore servicing fluid comprises a fluid loss additive comprising the reaction product of (i) a functional polymer and (ii) an oligomerized fatty acid.

6. 发明申请

US20130288933A1 Rheology Modifiers 审中-公开
公开(公告)号：US20130288933A1
公开(公告)日：2013-10-31
申请号：US13459677
申请日：2012-04-30
申请人： Jeffery R. Harris , Jim D. Byers
发明人： Jeffery R. Harris , Jim D. Byers
IPC分类号： C09K8/32
CPC分类号： C09K8/36 , C09K8/34
摘要： A non-aqueous wellbore servicing fluid comprising a rheology modifier wherein the rheology modifier comprises a reaction product of a polysulfide, a dimer acid and a polyfunctional amine. A method of conducting an oilfield operation comprising placing an oil-based mud comprising a rheology modifier into a wellbore wherein the rheology modifier comprises a reaction product of a polysulfide, a dimer acid and a polyfunctional amine.

7. 发明授权

US4871371A Tint compositions useful for providing coloration to aqueous and non-aqueous liquids 失效
标题翻译：用于提供水性和非水性液体着色的着色组合物
公开(公告)号：US4871371A
公开(公告)日：1989-10-03
申请号：US261205
申请日：1988-10-24
申请人： Jeffery R. Harris
发明人： Jeffery R. Harris
IPC分类号： C09B57/00 , C09B67/42 , C09B67/44 , C09B69/00
CPC分类号： C09B67/0083 , C09B69/00
摘要： A two component tint composition is provided which comprises as a first component, a colorant of the formula: ##STR1## wherein X is a polar group selected from sulfonic acids, sulfonic acid salts, sulfonamides, sulfonates, carboxylic acids, carboxylic acid salts, carboxylic acid amides, carboxylic aldehydes, carboxylic acid esters, ureas, thioureas, nitro groups, hydroxy groups, polyethers, and hydroxyalkylethers;R.sub.1 is selected from nitrogen, oxygen, sulfur, or a sulfur, or a sulfur-containing divalent linking group;R.sub.2 is hydrogen or a lower alkyl group;a is an integer of from 2-10;b is an integer of from 2-10;c and d are each independently selected from one or two;A is a chromophore selected from nitro, nitroso, monazo, diazo, diarylmethane, triarylmethane, acridine, methine, thiazole, indamine, oxazine, or anthraquinone; andB is --H, -alkyl, or -alkyl carboxylate; andas a second component a diluent selected from alkoxylated fatty acids and long chain alcohols, the weight ratio of diluent to colorant being from about 2.5 to about 5 parts diluent to 1 part colorant.

8. 发明授权

US07119132B2 Continuous neat polymerization and ambient grinding methods of polyolefin drag reducing agents 有权
公开(公告)号：US07119132B2
公开(公告)日：2006-10-10
申请号：US10694585
申请日：2003-10-27
申请人： Jeffery R. Harris , John F. Motier , Lu-Chien Chou , Thomas J. Martin
发明人： Jeffery R. Harris , John F. Motier , Lu-Chien Chou , Thomas J. Martin
IPC分类号： B05D5/08
CPC分类号： C08F2/002 , C08K5/0025 , Y10T137/0391 , C08L23/08
摘要： A process for continuously producing a polymer drag reducing agent (DRA) is described. The process concerns mixing a monomer and a catalyst in at least one continuously stirred tank reactor (CSTR) to form a mixture. The mixture is continuously injected into a volume continuously formed by a thermoplastic material, such as polyethylene. The thermoplastic material is periodically sealed off to form a temporary container or bag. The monomer is permitted to polymerize in the temporary container to form polymer. In one non-limiting embodiment, the polymerization in the bag takes place within an inert, circulating fluid that accelerates heat transfer. The polymer and the temporary container are then ground together, preferably at non-cryogenic temperatures, to produce a particulate polymer drag reducing agent. In one preferred, non-limiting embodiment, the grinding or pulverizing occurs in the presence of at least one solid organic grinding aid. Finally, the particulate polymer drag reducing agent may be combined with a dispersing fluid.

9. 发明授权

US06649670B1 Continuous neat polymerization and ambient grinding methods of polyolefin drag reducing agents 有权
标题翻译：聚烯烃减阻剂的连续纯聚合和环境研磨方法
公开(公告)号：US06649670B1
公开(公告)日：2003-11-18
申请号：US10321762
申请日：2002-12-17
申请人： Jeffery R. Harris , John F. Motier , Mike Callaway , George G. Ramsay
发明人： Jeffery R. Harris , John F. Motier , Mike Callaway , George G. Ramsay
IPC分类号： C08K501
CPC分类号： C08F2/002 , C08K5/0025 , Y10T137/0391 , C08L23/08
摘要： A process for continuously producing a polymer drag reducing agent (DRA) is described. The process concerns mixing a monomer and a catalyst in at least one continuously stirred tank reactor (CSTR) to form a mixture. The mixture is continuously injected into a volume continuously formed by a thermoplastic material, such as polyethylene. The thermoplastic material is periodically sealed off to form a temporary container or bag. The monomer is permitted to polymerize in the temporary container to form polymer. In one non-limiting embodiment, the polymerization in the bag takes place within an inert, circulating fluid that accelerates heat transfer. The polymer and the temporary container are then ground together, preferably at non-cryogenic temperatures, to produce a particulate polymer drag reducing agent. In one preferred, non-limiting embodiment, the grinding or pulverizing occurs in the presence of at least one solid organic grinding aid. Finally, the particulate polymer drag reducing agent may be combined with a dispersing fluid.
摘要翻译：描述了连续生产聚合物减阻剂（DRA）的方法。该方法涉及在至少一个连续搅拌釜式反应器（CSTR）中混合单体和催化剂以形成混合物。将混合物连续地注入由热塑性材料如聚乙烯连续形成的体积中。周期性地密封热塑性材料以形成临时容器或袋子。允许单体在临时容器中聚合以形成聚合物。在一个非限制性实施方案中，袋中的聚合在加速热传递的惰性循环流体中进行。然后将聚合物和临时容器一起研磨，优选在非低温温度下，以产生颗粒状聚合物减阻剂。在一个优选的非限制性实施方案中，研磨或粉碎发生在至少一种固体有机研磨助剂的存在下。最后，颗粒状聚合物减阻剂可与分散液组合。

10. 发明授权

US5240464A Organic materials having sulfonamido linked poly(oxyalkylene) moieties and their preparation 失效
标题翻译：具有亚磺酰氨基连接的聚（氧化烯）部分的有机材料及其制备
公开(公告)号：US5240464A
公开(公告)日：1993-08-31
申请号：US896508
申请日：1992-06-02
申请人： Edward W. Kluger , Max A. Weaver , Jeffery R. Harris , David J. Moody
发明人： Edward W. Kluger , Max A. Weaver , Jeffery R. Harris , David J. Moody
IPC分类号： C07C311/29 , C07C311/37 , C07C311/40 , C07C311/46 , C07C311/48 , C07D209/14 , C07D209/40 , C07D209/48 , C07D213/85 , C07D213/90 , C07D215/38 , C07D221/18 , C07D233/70 , C07D233/88 , C07D233/90 , C07D277/50 , C07D277/64 , C07D277/82 , C07D285/12 , C07D285/135 , C07D307/34 , C07D317/28 , C07D333/34 , C07D333/36 , C07D333/38 , C07D333/60 , C08G65/329 , C08G65/334 , C09B69/00
CPC分类号： C07D209/48 , C07C311/29 , C07C311/37 , C07C311/40 , C07C311/46 , C07C311/48 , C07D209/14 , C07D209/40 , C07D213/85 , C07D213/90 , C07D215/38 , C07D221/18 , C07D233/70 , C07D233/88 , C07D233/90 , C07D277/50 , C07D277/64 , C07D277/82 , C07D285/135 , C07D307/34 , C07D317/28 , C07D333/34 , C07D333/36 , C07D333/38 , C07D333/60 , C08G65/329 , C08G65/3348 , C09B69/00
摘要： The process for chemically modifying metal-free, organic material for improving one or more properties thereof such as water dispersibility, compatibility with other organics, or increased chemical reactivity, wherein the process includes providing material with from 1-6 sulfonylhalide groups or sulfonate ester groups or mixtures thereof, and contacting the material under sulfonamido forming conditions with one or more reactants containing one or more poly(oxyalkylene) moieties, each of the reactants having from 1 to 4 functional amine groups, and each of the poly(oxyalkylene) moieties being comprised of from about 4 to about 200 epoxide reactant residues at least about 50 mole percent of which residues contain 2-4 carbons.
摘要翻译：化学改性无机有机材料以改进其一种或多种性质如水分散性，与其它有机物的相容性或增加的化学反应性的方法，其中该方法包括提供具有1-6个磺酰卤基团或磺酸酯基团的材料或其混合物，并且在亚磺酰氨基形成条件下使材料与一种或多种含有一个或多个聚（氧化烯）部分的反应物接触，每个反应物具有1至4个官能胺基，并且每个聚（氧化烯）部分为由约4至约200个环氧化物反应物残余物组成，其残留物的至少约50摩尔％含有2-4个碳。

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