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1. 发明授权

US6090745A Process for preparing water-treatment catalysts 失效
标题翻译：制备水处理催化剂的方法
公开(公告)号：US6090745A
公开(公告)日：2000-07-18
申请号：US202171
申请日：1999-03-22
申请人： Jean-Luc DuBois , Edmond Payen , Michel Fournier , Pascal Blanchard , Anne Griboval
发明人： Jean-Luc DuBois , Edmond Payen , Michel Fournier , Pascal Blanchard , Anne Griboval
IPC分类号： B01J23/28 , B01J23/30 , B01J23/85 , B01J27/188 , B01J27/19 , C10G45/08 , B01J23/00 , B01J21/02 , B01J21/08 , B01J27/185
CPC分类号： B01J23/85 , B01J27/188 , C10G45/08
摘要： The invention provides a method for preparing catalysts, containing metals of groups VI and VIII on a carrier. The metals of groups VI and VIII metals are introduced in the form of a compound of formula M.sub.x A B.sub.12 O.sub.40 in which M is cobalt and/or nickel, A is phosphorus, silicon and/or boron, B is molybdenum and/or tungsten and x is 2 or more, 2.5 or more, or 3 or more depending on whether A is respectively phosphorus, silicon or boron. The catalysts thus obtained are useful for hydro-treating hydrocarbon feedstocks.
摘要翻译： PCT No.PCT / FR97 / 01029 Sec。 371日期1999年3月22日 102（e）1999年3月22日PCT 1997年6月10日PCT公布。出版物WO97 / 47385 日期：1997年12月18日本发明提供了一种在载体上制备含有VI和VIII族金属的催化剂的方法。 VI族和Ⅷ族金属的金属以式Mx A B12 O40化合物的形式引入，其中M为钴和/或镍，A为磷，硅和/或硼，B为钼和/或钨，取决于A是分别是磷，硅还是硼，x是2以上，2.5以上，3以上。因此得到的催化剂可用于烃类原料的加氢处理。

2. 发明授权

US08562940B2 Process for preparing an alumina with controlled mesoporosity 有权
标题翻译：制备具有受控中孔隙度的氧化铝的方法
公开(公告)号：US08562940B2
公开(公告)日：2013-10-22
申请号：US12978774
申请日：2010-12-27
申请人： Loic Rouleau , Sébastien Royer , Christine Lancelot , Franck Dumeignil , Edmond Payen , Pascal Blanchard
发明人： Loic Rouleau , Sébastien Royer , Christine Lancelot , Franck Dumeignil , Edmond Payen , Pascal Blanchard
IPC分类号： C01F7/00
CPC分类号： C01F7/36 , B01J29/0308 , B01J29/0333 , B01J35/1019 , B01J35/1042 , C01F7/441 , C01P2004/10 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C04B35/111 , C04B38/00 , C04B38/0054 , C04B2111/0081 , C04B2235/3218
摘要： A process for preparing a mesoporous alumina is described, comprising the following steps: a) mixing, in aqueous solution, at least one source of aluminum constituted by an aluminum alkoxide, at least one cationic surfactant and at least one organic solvent selected from methanol and ethanol; b) hydrothermally treating the mixture formed in said step a); c) drying the solid formed in said step b); d) calcining the solid formed in said step c).
摘要翻译：描述了一种制备介孔氧化铝的方法，包括以下步骤：a）在水溶液中混合至少一种由烷氧基铝构成的铝源，至少一种阳离子表面活性剂和至少一种选自甲醇和乙醇; b）水热处理在所述步骤a）中形成的混合物; c）干燥所述步骤b）中形成的固体; d）煅烧在步骤c）中形成的固体。

3. 发明申请

US20120237439A1 PROCESS FOR PREPARING AN ALUMINA WITH CONTROLLED MESOPOROSITY 有权
标题翻译：用于制备具有受控的MESOPOROSITY的铝的方法
公开(公告)号：US20120237439A1
公开(公告)日：2012-09-20
申请号：US12978774
申请日：2010-12-27
申请人： Loic ROULEAU , Sébastien Royer , Christine Lancelot , Franck Dumeignil , Edmond Payen , Pascal Blanchard
发明人： Loic ROULEAU , Sébastien Royer , Christine Lancelot , Franck Dumeignil , Edmond Payen , Pascal Blanchard
IPC分类号： C01F7/30
CPC分类号： C01F7/36 , B01J29/0308 , B01J29/0333 , B01J35/1019 , B01J35/1042 , C01F7/441 , C01P2004/10 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C04B35/111 , C04B38/00 , C04B38/0054 , C04B2111/0081 , C04B2235/3218
摘要： A process for preparing a mesoporous alumina is described, comprising the following steps: a) mixing, in aqueous solution, at least one source of aluminium constituted by an aluminium alkoxide, at least one cationic surfactant and at least one organic solvent selected from methanol and ethanol; b) hydrothermally treating the mixture formed in said step a); c) drying the solid formed in said step b); d) calcining the solid formed in said step c).
摘要翻译：描述了一种制备介孔氧化铝的方法，包括以下步骤：a）在水溶液中混合至少一种由烷氧基铝构成的铝源，至少一种阳离子表面活性剂和至少一种选自甲醇和乙醇; b）水热处理在所述步骤a）中形成的混合物; c）干燥所述步骤b）中形成的固体; d）煅烧在步骤c）中形成的固体。

4. 发明授权

US07179366B2 Catalyst based on a group VI metal and a group VIII metal at least partially present in the form of heteropolyanions in the oxide precursor 有权
标题翻译：至少部分以氧化物前体中杂多阴离子形式存在的基于VI族金属和VIII族金属的催化剂
公开(公告)号：US07179366B2
公开(公告)日：2007-02-20
申请号：US10631966
申请日：2003-08-01
申请人： Virginie Harle , Catherine Martin , Edmond Payen , Carole Lamonier , Pascal Blanchard
发明人： Virginie Harle , Catherine Martin , Edmond Payen , Carole Lamonier , Pascal Blanchard
IPC分类号： C10G11/02 , C10G11/04 , B01J21/00 , B01J23/00 , C01G47/00
CPC分类号： B01J37/03 , B01J23/85 , B01J23/882 , B01J23/883 , B01J37/20 , C10G45/08 , C10G45/12 , C10G45/62 , C10G45/64 , C10G47/14 , C10G47/16 , C10G47/18 , C10G49/04 , C10G49/08
摘要： A catalyst contains at least one group VIII element and at least molybdenum and/or tungsten, said elements being present at least in part in the catalyst in the dry state in the form of at least one heteropolyanion with formula MxAB6O24H6C(3-2x), tH2O; MxAB6O24H6C(4-2x), tH2O; MxA2B10O38H4C(6-2x), tH2O; MxA2B10O38H4C(8-2x), tH2O; or MxA2B10O38H4C(7-2x), tH2O, in which M is cobalt and/or nickel and/or iron and/or copper and/or zinc, A is one or two elements from group VIII of the periodic table, B is molybdenum and/or tungsten and C is an H+ ion and/or a (NR1R2R3R4)+ type ammonium ion, in which R1, R2, R3 and R4, which may be identical or different, correspond either to a hydrogen atom or to an alkyl group and/or caesium and/or potassium and/or sodium, t is a number between 0 and 15 and x takes a value in the range 0 to 4 depending on the formula.
摘要翻译：催化剂含有至少一种VIII族元素和至少钼和/或钨，所述元素至少部分地以至少一种具有式M x x的杂多阴离子的形式存在于干燥状态的催化剂中，（3-2x），tH 2，...，...，...，...，...，...，... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ... ...“ SUB> O; （4-2x），其中，C 1，C 2，C 4， t H 2 O; （A）（A）（A）（B） 6-2x），tH 2 O; （A）（A）（A）（B） 8-2x），tH 2 O; 或者M 1 A 2 B 2 O 3 C 3 H 4 C 3 H 3 （7-2x），其中M是钴和/或镍和/或铁和/或铜和/或锌，A是一个或两个元素，元素周期表第Ⅷ族，B为钼和/或钨，C为H +离子和/或（NR 1 R 2 R 2）其中R 1，R 2，R 2，R 3，R 3，R 3，R 3， R 3，R 3和R 4可以相同或不同，对应于氢原子或烷基和/或铯和/或钾和/或钠，t为0至15之间的数字，x取值范围为0至4，具体取决于公式。

5. 发明授权

US08633128B2 Lacunary Keggin type heteropolyanion based on tungsten for hydrocracking 有权
标题翻译：基于钨用于加氢裂化的Lacunary Keggin型杂多阴离子
公开(公告)号：US08633128B2
公开(公告)日：2014-01-21
申请号：US13059254
申请日：2009-07-29
申请人： Audrey Bonduelle , Fabrice Bertoncini , Karima Ben Tayeb , Carole Lamonier , Michel Fournier , Edmond Payen
发明人： Audrey Bonduelle , Fabrice Bertoncini , Karima Ben Tayeb , Carole Lamonier , Michel Fournier , Edmond Payen
IPC分类号： B01J21/02 , B01J27/00 , B01J27/19 , B01J27/185 , B01J27/182 , B01J29/70 , C10G47/00 , C10G47/02 , C10G47/24 , C10G11/00 , C10G11/02 , C10G45/00
CPC分类号： C01G41/006 , B01J23/002 , B01J23/888 , B01J27/188 , B01J37/0213 , B01J37/20 , B01J37/30 , B01J2523/00 , C01G53/006 , C01P2002/82 , C01P2002/86 , C10G45/08 , C10G47/12 , C10G49/04 , B01J2523/51 , B01J2523/69 , B01J2523/847 , B01J2523/41
摘要： The invention describes a heteropolycompound constituted by a nickel salt of a lacunary Keggin type heteropolyanion comprising tungsten in its structure, with formula: Nix+y/2AW11-yO39-5/2y, zH2O wherein Ni is nickel, A is selected from phosphorus, silicon and boron, W is tungsten, O is oxygen, y=0 or 2, x=3.5 if A is phosphorus, x=4 if A is silicon, x=4.5 if A is boron, and x=m/2+2 for the rest, and z is a number in the range 0 to 36, in which said heteropolycompound has no nickel atom in substitution for a tungsten atom in its structure, said nickel atoms being placed in the counter-ion position in the structure of said compound.
摘要翻译：本发明描述了由其结构中包含钨的缺口Keggin型杂多阴离子的镍盐构成的杂多化合物，其结构为：Nix + y / 2AW11-yO39-5 / 2y，zH2O，其中Ni是镍，A选自磷，硅和硼，W是钨，O是氧，y = 0或2，如果A是磷，x = 3.5，如果A是硅，x = 4，如果A是硅则x = 4.5，如果A是硼则x = 4.5，并且x = m / 2 + 2 其余，z为0〜36的数，其中所述杂多化合物在其结构中不具有取代钨原子的镍原子，所述镍原子位于所述化合物的结构中的反离子位置。

6. 发明申请

US20110230691A1 LACUNARY KEGGIN TYPE HETEROPOLYANION BASED ON TUNGSTEN FOR HYDROCRACKING 有权
标题翻译：基于TUNGSTEN用于水力裂化的LACUNICAL KEGGIN类型异构体
公开(公告)号：US20110230691A1
公开(公告)日：2011-09-22
申请号：US13059254
申请日：2009-07-29
申请人： Audrey Bonduelle , Fabrice Bertoncini , Karima Ben Tayeb , Carole Lamonier , Michel Fournier , Edmond Payen
发明人： Audrey Bonduelle , Fabrice Bertoncini , Karima Ben Tayeb , Carole Lamonier , Michel Fournier , Edmond Payen
IPC分类号： C07C5/10 , B01J27/188 , B01J21/06 , B01J21/02 , C01B33/20 , B01J37/30 , C10G11/04
CPC分类号： C01G41/006 , B01J23/002 , B01J23/888 , B01J27/188 , B01J37/0213 , B01J37/20 , B01J37/30 , B01J2523/00 , C01G53/006 , C01P2002/82 , C01P2002/86 , C10G45/08 , C10G47/12 , C10G49/04 , B01J2523/51 , B01J2523/69 , B01J2523/847 , B01J2523/41
摘要： The invention describes a heteropolycompound constituted by a nickel salt of a lacunary Keggin type heteropolyanion comprising tungsten in its structure, with formula: Nix+y/2AW11-yO39-5/2y,zH2O wherein Ni is nickel, A is selected from phosphorus, silicon and boron, W is tungsten, O is oxygen, y=0 or 2, x=3.5 if A is phosphorus, x=4 if A is silicon, x=4.5 if A is boron, and x=m/2+2 for the rest, and z is a number in the range 0 to 36, in which said heteropolycompound has no nickel atom in substitution for a tungsten atom in its structure, said nickel atoms being placed in the counter-ion position in the structure of said compound.
摘要翻译：本发明描述了由其结构中包含钨的缺口Keggin型杂多阴离子的镍盐构成的杂多化合物，其结构为：Nix + y / 2AW11-yO39-5 / 2y，zH2O，其中Ni是镍，A选自磷，硅和硼，W是钨，O是氧，y = 0或2，如果A是磷，x = 3.5，如果A是硅，x = 4，如果A是硅则x = 4.5，如果A是硼则x = 4.5，并且x = m / 2 + 2 其余，z为0〜36的数，其中所述杂多化合物在其结构中不具有取代钨原子的镍原子，所述镍原子位于所述化合物的结构中的反离子位置。

7. 发明申请

US20060180501A1 Process and device for desulphurizing hydrocarbons containing thiophene derivatives 审中-公开
标题翻译：用于脱硫含噻吩衍生物的烃的方法和装置
公开(公告)号：US20060180501A1
公开(公告)日：2006-08-17
申请号：US10250431
申请日：2001-12-20
申请人： Pedro Da Silva , Edmond Payen , Jean-Yves Carriat , Marc Bisson
发明人： Pedro Da Silva , Edmond Payen , Jean-Yves Carriat , Marc Bisson
IPC分类号： C10G45/00
CPC分类号： C10G27/12
摘要： The invention relates to a selective desulphurisation method for thiophene derivatives contained in the hydrocarbons emitted from the distillation of crude oil, refined or not, consisting in oxidising the atoms of thiophene sulphur in sulphone in the presence of an oxidising agent and separating the sulphonated compounds from said hydrocarbons. This inventive method comprises at least one first stage involving the oxidation/absorption by heterogeneous catalysis of the sulphurous compounds in an organic environment, at a temperature of at least 40?C, at atmospheric pressure in the presence of an organic oxidiser from the family of peroxides and peracids, in the presence of a catalyst having a specific surface area greater than 100 m2/g and a porosity varying from 0.2 to 4 ml/g, and a second stage wherein the used catalyst is regenerated.
摘要翻译：本发明涉及一种选择性脱硫方法，其用于从蒸馏原油中排出的烃中含有的噻吩衍生物，其被精炼或不精炼，其包括在氧化剂存在下氧化砜中噻吩硫的原子并将磺化化合物从说碳氢化合物。本发明的方法包括至少一个第一阶段，其涉及在有机环境中，在至少40℃的温度下，在大气压下，在存在有机氧化剂的情况下，通过非极性催化亚硫化合物的氧化/吸收，过氧化物和过酸，在比表面积大于100m 2 / g，孔隙率为0.2-4ml / g的催化剂存在下，再次使用所用的催化剂。

8. 发明申请

US20080020926A1 Process for preparing at least one cobalt and/or nickel salt of at least one Anderson heterpolyanion combining molybdenum and cobalt or nickel in its structure 有权
标题翻译：用于制备至少一种在其结构中结合钼和钴或镍的安德森杂多阴离子的至少一种钴和/或镍盐的方法
公开(公告)号：US20080020926A1
公开(公告)日：2008-01-24
申请号：US11878308
申请日：2007-07-23
申请人： Denis Guillaume , Edmond Payen , Carole Lamonier , Karin Marchand
发明人： Denis Guillaume , Edmond Payen , Carole Lamonier , Karin Marchand
IPC分类号： B01J23/28
CPC分类号： B01J23/882 , B01J21/04 , B01J23/002 , B01J23/883 , B01J37/0009 , B01J37/0201 , B01J37/0213 , B01J37/08 , B01J37/12 , B01J37/20 , B01J2523/00 , C10G45/08 , C10G45/12 , B01J2523/68 , B01J2523/845 , B01J2523/847
摘要： A process is described for preparing a solution formed by at least one cobalt and/or nickel salt of at least one heteropolyanion combining molybdenum and cobalt or molybdenum and nickel in its structure, said process comprising: a) mixing at least one source of molybdenum and at least one oxidizing compound in aqueous solution to synthesize peroxomolybdate ions at an acidic pH, the (oxidizing compound/molybdenum source) mole ratio being in the range 0.1 to 20; b) introducing at least one cobalt precursor and/or at least one nickel precursor into the solution from step a) to form a solution comprising at least said salt in which the (Co+Ni)/Mo mole ratio is in the range 0.25 to 0.85.
摘要翻译：描述了一种制备由至少一种结合钼和钴或钼和镍的杂多阴离子的至少一种钴和/或镍盐形成的溶液的方法，所述方法包括：a）将至少一种钼源和至少一种氧化性化合物在水溶液中，在酸性pH下合成过氧钼酸根离子，（氧化化合物/钼源）的摩尔比在0.1至20的范围内; b）将至少一种钴前体和/或至少一种镍前体引入到步骤a）的溶液中以形成至少包含所述盐的溶液，其中（Co + Ni）/ Mo摩尔比在0.25至 0.85。

9. 发明授权

US07687430B2 Process for preparing at least one cobalt and/or nickel salt of at least one Anderson heterpolyanion combining molybdenum and cobalt or nickel in its structure 有权
标题翻译：用于制备至少一种在其结构中结合钼和钴或镍的安德森杂多阴离子的至少一种钴和/或镍盐的方法
公开(公告)号：US07687430B2
公开(公告)日：2010-03-30
申请号：US11878308
申请日：2007-07-23
申请人： Denis Guillaume , Edmond Payen , Carole Lamonier , Karin Marchand
发明人： Denis Guillaume , Edmond Payen , Carole Lamonier , Karin Marchand
IPC分类号： B01J23/00
CPC分类号： B01J23/882 , B01J21/04 , B01J23/002 , B01J23/883 , B01J37/0009 , B01J37/0201 , B01J37/0213 , B01J37/08 , B01J37/12 , B01J37/20 , B01J2523/00 , C10G45/08 , C10G45/12 , B01J2523/68 , B01J2523/845 , B01J2523/847
摘要： A process is described for preparing a solution formed by at least one cobalt and/or nickel salt of at least one heteropolyanion combining molybdenum and cobalt or molybdenum and nickel in its structure, said process comprising: a) mixing at least one source of molybdenum and at least one oxidizing compound in aqueous solution to synthesize peroxomolybdate ions at an acidic pH, the (oxidizing compound/molybdenum source) mole ratio being in the range 0.1 to 20; b) introducing at least one cobalt precursor and/or at least one nickel precursor into the solution from step a) to form a solution comprising at least said salt in which the (Co+Ni)/Mo mole ratio is in the range 0.25 to 0.85.
摘要翻译：描述了一种制备由至少一种结合钼和钴或钼和镍的杂多阴离子的至少一种钴和/或镍盐形成的溶液的方法，所述方法包括：a）将至少一种钼源和至少一种氧化性化合物在水溶液中，在酸性pH下合成过氧钼酸根离子，（氧化化合物/钼源）的摩尔比在0.1至20的范围内; b）将至少一种钴前体和/或至少一种镍前体引入到步骤a）的溶液中以形成至少包含所述盐的溶液，其中（Co + Ni）/ Mo摩尔比在0.25至 0.85。

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