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1. 发明授权

US08558049B2 Process and apparatus for para-xylene production using multiple adsorptive separation units and multiple adsorptive bed feed points 有权
公开(公告)号：US08558049B2
公开(公告)日：2013-10-15
申请号：US13326961
申请日：2011-12-15
申请人： Jason T. Corradi , Sara A. Williams , Stanley J. Frey
发明人： Jason T. Corradi , Sara A. Williams , Stanley J. Frey
IPC分类号： C07C7/12
CPC分类号： C07C5/2729 , B01D15/1828 , C07C7/04 , C07C7/12 , C07C7/13 , C10G25/00 , C10G25/12 , C10G2300/4056 , C10G2400/30 , C07C15/08
摘要： A process for separating para-xylene from aromatic compounds is presented. The process introduces throughout a first step-time interval a first mixed xylene stream into a first feed input on a first adsorptive separation unit comprising multiple bed lines. The process further introduces throughout the first step-time interval a second mixed xylene stream into a second feed input on the first adsorptive separation unit. During a first portion of the first step-time interval, the process introduces material from a feed stream used during the first step-time interval into a bed line not used to deliver a stream into, or withdraw a stream from, the first adsorptive separation unit during the first step time interval. During a second portion of the first step-time interval, the process introduces material from a purification zone into the feed stream used during the first step-time interval.

2. 发明申请

US20130158331A1 Process and Apparatus for para-Xylene Production using Multiple Adsorptive Separation Units and Multiple Adsorptive Bed Feed Points 有权
标题翻译：使用多个吸附分离单元和多个吸附床进料点的对二甲苯生产的方法和装置
公开(公告)号：US20130158331A1
公开(公告)日：2013-06-20
申请号：US13326961
申请日：2011-12-15
申请人： Jason T. Corradi , Sara A. Williams , Stanley J. Frey
发明人： Jason T. Corradi , Sara A. Williams , Stanley J. Frey
IPC分类号： C07C7/12 , B01J19/00 , B01D15/00
CPC分类号： C07C5/2729 , B01D15/1828 , C07C7/04 , C07C7/12 , C07C7/13 , C10G25/00 , C10G25/12 , C10G2300/4056 , C10G2400/30 , C07C15/08
摘要： A process for separating para-xylene from aromatic compounds is presented. The process introduces throughout a first step-time interval a first mixed xylem stream into a first feed input on a first adsorptive separation unit comprising multiple bed lines. The process further introduces throughout the first step-time interval a second mixed xylene stream into a second feed input on the first adsorptive separation unit. During a first portion of the first step-time interval, the process introduces material from a feed stream used during the first step-time interval into a bed line not used to deliver a stream into, or withdraw a stream from, the first adsorptive separation unit during the first step time interval. During a second portion of the first step-time interval, the process introduces material from a purification zone into the feed stream used during the first step-time interval.
摘要翻译：提出了一种从芳族化合物中分离对二甲苯的方法。该过程在第一步骤间隔期间将第一混合木质部流引入包含多个床线的第一吸附分离单元上的第一进料输入。该方法在第一步骤间隔期间将第二混合二甲苯流引入第一吸附分离单元上的第二进料输入。在第一步骤间隔的第一部分期间，该过程将来自在第一步骤间隔期间使用的进料流的材料引入不用于将流输送到或从第一吸附分离物流中取出流的床线单位在第一步时间间隔。在第一步骤间隔的第二部分期间，该过程将来自纯化区域的材料引入在第一步骤间隔期间使用的进料流中。

3. 发明申请

US20100305380A1 Process for Improved Meta-Xylene Yield from C8 Aromatics 有权
标题翻译： C8芳烃改进二甲苯产率的方法
公开(公告)号：US20100305380A1
公开(公告)日：2010-12-02
申请号：US12622824
申请日：2009-11-20
申请人： Stanley J. Frey , Jason T. Corradi , Richard S. Kempf , David W. Liu
发明人： Stanley J. Frey , Jason T. Corradi , Richard S. Kempf , David W. Liu
IPC分类号： C07C5/00 , C07C15/08
CPC分类号： C07C7/04 , C07C5/2737 , C07C7/13 , C07C15/08
摘要： Meta-xylene is recovered from admixture with other C8 aromatic hydrocarbons including ortho-xylene by liquid phase adsorptive separation. Performance is improved by reducing the concentration of ortho-xylene through adding a sidecut to a prefractionator preparing the feedstock to adsorptive separation.
摘要翻译：通过液相吸附分离从与其它C8芳族烃（包括邻二甲苯）混合中回收元二甲苯。通过向准备原料进行吸附分离的初步分选机中添加一次侧馏分，可以降低邻二甲苯的浓度来提高性能。

4. 发明申请

US20120067774A1 PROCESSES FOR INCREASING THE OVERALL AROMATICS AND XYLENES YIELD IN AN AROMATICS COMPLEX 有权
标题翻译：增加复合物中整体的芳族化合物和二甲苯的制备方法
公开(公告)号：US20120067774A1
公开(公告)日：2012-03-22
申请号：US12883977
申请日：2010-09-16
申请人： Stanley J. Frey , Jason T. Corradi , Gregory Werba
发明人： Stanley J. Frey , Jason T. Corradi , Gregory Werba
IPC分类号： C10G35/04 , C10G35/00
CPC分类号： C10G69/123 , C10G35/04 , C10G2300/1044 , C10G2300/1096 , C10G2300/4081 , C10G2400/30
摘要： Processes for increasing overall aromatics and xylenes yield in an aromatics complex are provided. A C8+ aromatics stream from an aromatics-rich reformate is separated into a C8 aromatics fraction and a C9+ aromatics fraction comprising higher alkyl group-substituted C9 and C10 aromatics. The C9+ aromatics fraction is separated into a lighter boiling, higher alkyl group-substituted C9 or C9/C10 aromatics fraction and a heavier boiling, C10+ or C11+ aromatics fraction. The lighter boiling, higher alkyl group-substituted C9 or C9/C10 aromatics fraction is isomerized to convert a portion of the higher alkyl group-substituted C9 or C9/C10 aromatics therein into methyl-enriched C9 aromatics or methyl-enriched C9/C10 aromatics. The methyl-enriched C9+ aromatics stream comprising the methyl-enriched C9+ aromatics stream or the methyl-enriched C9/C10 aromatics is transalkylated with a toluene-containing stream.
摘要翻译：提供了用于增加芳族化合物中总体芳族化合物和二甲苯产率的方法。将来自富含芳香族化合物的重整产物的C8 +芳族化合物流分离成C8芳族化合物馏分和包含较高级烷基取代的C9和C10芳族化合物的C9 +芳烃馏分。将C9 +芳族化合物馏分分离成较轻沸点的较高级烷基取代的C9或C9 / C10芳烃馏分和较重沸腾的C10 +或C11 +芳烃馏分。较轻的沸点较高的烷基取代的C9或C9 / C10芳族化合物部分被异构化，以将其中一部分高级烷基取代的C9或C9 / C10芳族化合物转化成甲基富集的C9芳族化合物或甲基富集的C9 / C10芳族化合物。包含甲基富集的C9 +芳族化合物流或甲基富集的C9 / C10芳族化合物的甲基富集的C9 +芳族化合物物流与含甲苯的物流转烷基化。

5. 发明授权

US07960600B2 Process for improved meta-xylene yield from C8 aromatics 有权
标题翻译：改进C8芳族化合物的间二甲苯产率的方法
公开(公告)号：US07960600B2
公开(公告)日：2011-06-14
申请号：US12622824
申请日：2009-11-20
申请人： Stanley J. Frey , Jason T. Corradi , Richard S. Kempf , David W. Liu
发明人： Stanley J. Frey , Jason T. Corradi , Richard S. Kempf , David W. Liu
IPC分类号： C07C7/12 , C07C7/04
CPC分类号： C07C7/04 , C07C5/2737 , C07C7/13 , C07C15/08
摘要： Meta-xylene is recovered from admixture with other C8 aromatic hydrocarbons including ortho-xylene by liquid phase adsorptive separation. Performance is improved by reducing the concentration of ortho-xylene through adding a sidecut to a prefractionator preparing the feedstock to adsorptive separation.
摘要翻译：通过液相吸附分离从与其它C8芳族烃（包括邻二甲苯）混合中回收元二甲苯。通过向准备原料进行吸附分离的初步分选机中添加一次侧馏分来降低邻二甲苯的浓度来提高性能。

6. 发明授权

US08431758B2 Processes for increasing the overall aromatics and xylenes yield in an aromatics complex 有权
标题翻译：用于增加芳族化合物中总芳烃和二甲苯产率的方法
公开(公告)号：US08431758B2
公开(公告)日：2013-04-30
申请号：US12883977
申请日：2010-09-16
申请人： Stanley J. Frey , Jason T. Corradi , Gregory Werba
发明人： Stanley J. Frey , Jason T. Corradi , Gregory Werba
IPC分类号： C07C2/66 , C07C5/27
CPC分类号： C10G69/123 , C10G35/04 , C10G2300/1044 , C10G2300/1096 , C10G2300/4081 , C10G2400/30
摘要： Processes for increasing overall aromatics and xylenes yield in an aromatics complex are provided. A C8+ aromatics stream from an aromatics-rich reformate is separated into a C8 aromatics fraction and a C9+ aromatics fraction comprising higher alkyl group-substituted C9 and C10 aromatics. The C9+ aromatics fraction is separated into a lighter boiling, higher alkyl group-substituted C9 or C9/C10 aromatics fraction and a heavier boiling, C10+ or C11+ aromatics fraction. The lighter boiling, higher alkyl group-substituted C9 or C9/C10 aromatics fraction is isomerized to convert a portion of the higher alkyl group-substituted C9 or C9/C10 aromatics therein into methyl-enriched C9 aromatics or methyl-enriched C9/C10 aromatics. The methyl-enriched C9+ aromatics stream comprising the methyl-enriched C9+ aromatics stream or the methyl-enriched C9/C10 aromatics is transalkylated with a toluene-containing stream.
摘要翻译：提供了用于增加芳族化合物中总体芳族化合物和二甲苯产率的方法。将来自富含芳香族化合物的重整产物的C8 +芳族化合物流分离成C8芳族化合物馏分和包含较高级烷基取代的C9和C10芳族化合物的C9 +芳烃馏分。将C9 +芳族化合物馏分分离成较轻沸点的较高级烷基取代的C9或C9 / C10芳烃馏分和较重沸腾的C10 +或C11 +芳烃馏分。较轻的沸点较高的烷基取代的C9或C9 / C10芳族化合物部分被异构化，以将其中一部分高级烷基取代的C9或C9 / C10芳族化合物转化成甲基富集的C9芳族化合物或甲基富集的C9 / C10芳族化合物。包含甲基富集的C9 +芳族化合物流或甲基富集的C9 / C10芳族化合物的甲基富集的C9 +芳族化合物物流与含甲苯的物流转烷基化。

7. 发明授权

US08841503B2 Product recovery from adsorption-separation purge fluids 有权
标题翻译：从吸附分离清洗液中回收产品
公开(公告)号：US08841503B2
公开(公告)日：2014-09-23
申请号：US13116616
申请日：2011-05-26
申请人： Jason T. Corradi , James W. Harris , Lewis H. Pettengill
发明人： Jason T. Corradi , James W. Harris , Lewis H. Pettengill
IPC分类号： C07C7/12 , B01D15/18
CPC分类号： C07C7/12 , B01D15/1835 , C07C15/08
摘要： Purge fluid from a vessel head in an adsorption process is distributed to recovery processes according to the purity of product contained in the fluid. Extract-rich fluid thus is routed directly to recovery of the extract product. Distribution preferably is determined by internal positioning of feed, desorbent and product streams in the adsorption vessel.
摘要翻译：根据流体中含有的产品的纯度将吸附过程中的容器头部清洗液分配到回收过程中。因此，提取物富含的流体直接路由到萃取产物的回收。分布优选通过进料，解吸剂和产物流在吸附容器中的内部定位来确定。

8. 发明申请

US20130158333A1 Process and Apparatus for para-Xylene Production using Multiple Adsorptive Separation Units with Shared Raffinate Processing 有权
标题翻译：使用具有共享残液加工的多个吸附分离单元的对二甲苯生产的方法和装置
公开(公告)号：US20130158333A1
公开(公告)日：2013-06-20
申请号：US13326824
申请日：2011-12-15
申请人： Jason T. Corradi
发明人： Jason T. Corradi
IPC分类号： C07C7/12 , C10C3/08
CPC分类号： C07C7/12 , B01D53/0423 , B01D2256/24 , B01D2257/7027 , C07C7/005 , C07C7/04 , C07C15/08
摘要： A process for separating para-xylene from a plurality of aromatic compounds, wherein the process introduces a first mixed xylene stream comprising a plurality of xylene isomers into a first adsorptive separation unit to produce a first para-xylene enriched stream and a first raffinate stream. The process further introduces a second mixed xylene stream comprising a plurality of xylene isomers into a second adsorptive separation unit to produce a second para-xylene enriched stream and a second raffinate stream. The process further feeds both the first raffinate stream and the second raffinate stream into a shared raffinate column.
摘要翻译：一种用于从多种芳族化合物中分离对二甲苯的方法，其中该方法将包含多个二甲苯异构体的第一混合二甲苯流引入第一吸附分离单元以产生富含第一对二甲苯的流和第一萃余液流。该方法进一步将包含多个二甲苯异构体的第二混合二甲苯料流引入第二吸附分离单元以产生第二对二甲苯富集料流和第二萃余物料流。该方法进一步将第一萃余液流和第二萃余液流进料到共用萃余塔中。

9. 发明申请

US20110116991A1 Propylene Recovery During Regeneration of an Oxygenate Removal Unit 有权
标题翻译：氧化剂去除单元再生过程中的丙烯回收
公开(公告)号：US20110116991A1
公开(公告)日：2011-05-19
申请号：US13011182
申请日：2011-01-21
申请人： Jason T. Corradi
发明人： Jason T. Corradi
IPC分类号： B01D15/00
CPC分类号： C07C1/20 , B01D53/77 , B01D2257/504 , B01D2257/70 , B01D2257/80 , C07C7/12 , F25J3/0219 , F25J3/0233 , F25J3/0238 , F25J3/0242 , F25J2210/12 , F25J2215/62 , Y02P20/152 , Y02P20/51 , C07C11/06
摘要： Processes and systems are disclosed that relate to the removal of impurities and separation the light olefins from an MTO product vapor stream. Specifically, the processes and systems relate to recovery of light olefins during regeneration of an adsorber in an oxygenate removal unit. Processes and systems for recovering light olefins during regeneration of an adsorber in an oxygenate removal unit can include recycling residual effluent stream to an upstream operation unit upstream of the oxygenate removal unit. Processes and systems for recovering light olefins during regeneration of an adsorber in an oxygenate removal unit can also include recycling residual effluent gas produced by depressurizing residual effluent in the first adsorber, as well as preferably venting an effluent gas from the first adsorber to a compressor upstream of the oxygenate removal unit.
摘要翻译：公开了涉及去除杂质并将轻质烯烃与MTO产物蒸气流分离的方法和系统。具体地，该方法和系统涉及在含氧化合物去除单元中的吸附剂再生期间回收轻质烯烃。在含氧物去除单元中的吸附剂再生期间回收轻质烯烃的方法和系统可以包括将残留流出物流再循环到含氧化合物去除单元上游的上游操作单元。在含氧化合物去除单元中的吸附器再生期间回收轻质烯烃的方法和系统还可以包括将在第一吸附器中的残留流出物减压产生的残余流出气体循环，以及优选将排出气体从第一吸附器排出到压缩机上游的含氧化合物去除单元。

10. 发明授权

US08754281B2 Energy conservation in heavy-hydrocarbon distillation 有权
标题翻译：重烃蒸馏节能
公开(公告)号：US08754281B2
公开(公告)日：2014-06-17
申请号：US12868309
申请日：2010-08-25
申请人： Gregory R. Werba , Jason T. Corradi , Zin X. Zhu , David W. Ablin , Saadet Ulas Acikgoz
发明人： Gregory R. Werba , Jason T. Corradi , Zin X. Zhu , David W. Ablin , Saadet Ulas Acikgoz
IPC分类号： C07C7/04 , C07C7/12 , C07C15/08 , B01D3/14
CPC分类号： B01D3/143 , C07C7/005 , C07C7/04 , C07C7/08 , C07C7/12 , C10G7/00 , C10G2300/1096 , C10G2400/30 , Y02P20/124 , Y02P20/57 , C07C15/08
摘要： An aromatics complex producing one or more xylene isomers offers a large number of opportunities to conserve energy by heat exchange within the complex. One previously unrecognized opportunity is through providing two parallel distillation columns operating at different pressures to separate C8 aromatics from C9+ aromatics. The parallel columns offer additional opportunities to conserve energy within the complex through heat exchange in associated xylene recovery facilities.
摘要翻译：产生一种或多种二甲苯异构体的芳族化合物通过复合物内的热交换提供了大量的节能能量的机会。一个以前未被认识的机会是通过提供在不同压力下操作的两个平行蒸馏塔来分离C8芳族化合物与C9 +芳族化合物。平行柱提供了额外的机会，通过相关的二甲苯回收设备中的热交换来节省复合物内的能量。

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