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1. 发明申请

US20100105792A1 RADIATION-CURING BINDERS AND A PROCESS FOR THEIR PREPARATION 有权
标题翻译：辐射固化粘合剂及其制备方法
公开(公告)号：US20100105792A1
公开(公告)日：2010-04-29
申请号：US12651576
申请日：2010-01-04
申请人： Jan Weikard , Christoph Gürtler , Wolfgang Fischer , Jörg Schmitt , Holger Mundstock
发明人： Jan Weikard , Christoph Gürtler , Wolfgang Fischer , Jörg Schmitt , Holger Mundstock
IPC分类号： C08G59/68
CPC分类号： C08G18/8175 , B33Y70/00 , C09D175/14 , Y10T428/31551
摘要： The invention relates to a process for preparing binders which contain 1) allophanate groups, 2) groups that react with ethylenically unsaturated compounds with polymerization on exposure to actinic radiation (radiation-curing groups) and 3) optionally NCO-reactive groups, by reacting at temperatures ≦130° C. A) one or more NCO-functional compounds containing uretdione groups with B) one or more compounds that contain isocyanate-reactive groups and groups that react with ethylenically unsaturated compounds with polymerization on exposure to actinic radiation (radiation-curing groups), and then C) with one or more saturated, hydroxyl-containing compounds other than B), at least one of these compounds having an OH functionality of ≧2, in the presence of D) a catalyst containing one or more ammonium salts or phosphonium salts of aliphatic or cycloaliphatic carboxylic acids, the reaction with compounds C) taking place at least proportionally with the formation of allophanate groups. The present invention also relates to the binders obtained by the process of the invention.
摘要翻译：本发明涉及一种制备粘合剂的方法，其包含1）脲基甲酸酯基团，2）与烯键式不饱和化合物反应的基团与暴露于光化辐射（辐射固化基团）和3）任选的NCO-反应性基团反应的基团， A）一种或多种含有脲二酮基团的NCO-官能化合物，B）一种或多种含有异氰酸酯反应性基团的化合物和与烯键式不饱和化合物反应而与光化辐射（辐射 - 固化基团），然后C）与除了B）之外的一种或多种饱和的含羟基化合物，在D的存在下，在具有OH官能度≥2的这些化合物中的至少一种的化合物中含有一种或多种铵脂肪族或脂环族羧酸的盐或鏻盐，与化合物C）的反应至少与脲基甲酸酯基团的形成成比例地发生。本发明还涉及通过本发明的方法获得的粘合剂。

2. 发明授权

US07659425B2 Process for preparing hydroxyalkyl(meth) acrylates using Lewis acid catalysts 有权
标题翻译：使用路易斯酸催化剂制备（甲基）丙烯酸羟烷基酯的方法
公开(公告)号：US07659425B2
公开(公告)日：2010-02-09
申请号：US11356334
申请日：2006-02-16
申请人： Jan Weikard , Christoph Gürtler
发明人： Jan Weikard , Christoph Gürtler
IPC分类号： C07C67/26 , C07C69/52
CPC分类号： C07C67/26 , C07C69/54
摘要： The present invention relates to a process for preparing hydroxyalkyl (meth)acrylates by reacting at least one compound A which contains at least one epoxide group with at least one compound B which contains at least one carboxylic acid group, wherein A and/or B also contains at least one (meth)acrylate group, in the presence of Lewis acid catalysts, each of which contains at least one directly bonded di(cyclo)alkylamino group.
摘要翻译：本发明涉及通过使至少一种含有至少一个环氧基的化合物A与至少一种含有至少一个羧酸基团的化合物B反应来制备（甲基）丙烯酸羟烷基酯的方法，其中A和/或B也是在路易斯酸催化剂存在下含有至少一种（甲基）丙烯酸酯基团，其各自含有至少一个直接键合的二（环）烷基氨基。

3. 发明授权

US07553906B2 Dual cure systems 有权
标题翻译：双重治疗系统
公开(公告)号：US07553906B2
公开(公告)日：2009-06-30
申请号：US10738879
申请日：2003-12-17
申请人： Jan Weikard , Christoph Gürtler , Wolfgang Fischer , Diethelm Rappen , Michael Schelhaas
发明人： Jan Weikard , Christoph Gürtler , Wolfgang Fischer , Diethelm Rappen , Michael Schelhaas
IPC分类号： C08G18/80 , C08G18/81 , C08L75/14 , C07C233/57 , C07C263/00
CPC分类号： C08G18/672 , C08G18/8048 , C08G18/8093 , C08G18/8096 , C08G18/8175 , C08L75/16 , C09D175/16 , Y10T428/31551 , C08G18/62 , C08L2666/20
摘要： An organic polyisocyanate with at least one unsaturated functional group is capable of copolymerizing when exposed to actinic radiation. The polyisocyanate comprises structural units with the formula (1): wherein: X is an electron-attracting group; R1, and R2 are hydrogen atoms, a saturated or unsaturated aliphatic or cycloaliphatic radical, or an aromatic or araliphatic radical; and n is an integer from 0 to 5. A process for producing this polyisocyanate is also disclosed.
摘要翻译：具有至少一个不饱和官能团的有机多异氰酸酯在暴露于光化辐射时能够共聚。多异氰酸酯包括具有式（1）的结构单元：其中：X是吸电子基团; R1和R2是氢原子，饱和或不饱和的脂族或脂环族基团，或芳族或芳脂族基团; 并且n为0至5的整数。还公开了制备该多异氰酸酯的方法。

4. 发明授权

US09085656B2 Low viscosity allophanates containing actinically curable groups 有权
标题翻译：含有光化学可固化基团的低粘度脲基甲酸酯
公开(公告)号：US09085656B2
公开(公告)日：2015-07-21
申请号：US11217727
申请日：2005-09-01
申请人： Jan Weikard , Frank Richter , Christoph Gürtler , Wolfgang Fischer , Jörg Schmitz , Holger Mundstock
发明人： Jan Weikard , Frank Richter , Christoph Gürtler , Wolfgang Fischer , Jörg Schmitz , Holger Mundstock
IPC分类号： C08G18/79 , C08G18/67 , C08G18/18 , C09D175/00 , C09D175/14 , C09D175/16 , C07C275/60 , C08G73/00 , C08L75/00 , C08L75/16 , C08L75/14 , C08G18/78 , C08G18/81
CPC分类号： C08G18/798 , C07C275/60 , C08G18/1825 , C08G18/1875 , C08G18/671 , C08G18/672 , C08G18/7837 , C08G18/8166 , C08G73/00 , C08L75/00 , C08L75/14 , C08L75/16 , C09D175/00 , C09D175/14 , C09D175/16
摘要： The present invention relates to a process for preparing radiation-curing binders containing allophanate groups by reacting at temperatures of ≦130° C. A) one or more compounds containing uretdione groups with B) one or more OH-functional compounds which contain groups which react, with polymerization, with ethylenically unsaturated compounds on exposure to actinic radiation, (radiation-curing groups), C) optionally NCO-reactive compounds other than B), in the presence of D) a catalyst containing at least one tetrasubstituted ammonium or phosphonium salt of an aliphatic or cycloaliphatic carboxylic acid, to form allophanate groups by opening the uretdione ring. The present invention also relates to the binders obtained by the process of the invention.
摘要翻译：本发明涉及通过在温度为130℃的温度下反应制备含有脲基甲酸酯基的辐射固化粘合剂的方法。A）一种或多种含有脲二酮基团的化合物与B）一种或多种含OH官能化合物，在曝光于光化辐射下与烯属不饱和化合物反应（辐射固化基团），C）任选除B）之外的NCO-反应性化合物，在D）存在下，含有至少一种四取代的铵或鏻的催化剂脂肪族或脂环族羧酸的盐，通过打开脲二酮环形成脲基甲酸酯基。本发明还涉及通过本发明的方法获得的粘合剂。

5. 发明授权

US07666970B2 Radiation-curing binders and a process for their preparation 有权
标题翻译：辐射固化粘合剂及其制备方法
公开(公告)号：US07666970B2
公开(公告)日：2010-02-23
申请号：US11217728
申请日：2005-09-01
申请人： Jan Weikard , Christoph Gürtler , Wolfgang Fischer , Jörg Schmitz , Holger Mundstock
发明人： Jan Weikard , Christoph Gürtler , Wolfgang Fischer , Jörg Schmitz , Holger Mundstock
IPC分类号： C08G18/04 , C08G18/08 , C08G18/00 , C08G18/78
CPC分类号： C08G18/8175 , B33Y70/00 , C09D175/14 , Y10T428/31551
摘要： The invention relates to a process for preparing binders which contain 1) allophanate groups, 2) groups that react with ethylenically unsaturated compounds with polymerization on exposure to actinic radiation (radiation-curing groups) and 3) optionally NCO-reactive groups, by reacting at temperatures ≦130° C. A) one or more NCO-functional compounds containing uretdione groups with B) one or more compounds that contain isocyanate-reactive groups and groups that react with ethylenically unsaturated compounds with polymerization on exposure to actinic radiation (radiation-curing groups), and then C) with one or more saturated, hydroxyl-containing compounds other than B), at least one of these compounds having an OH functionality of ≧2, in the presence of D) a catalyst containing one or more ammonium salts or phosphonium salts of aliphatic or cycloaliphatic carboxylic acids, the reaction with compounds C) taking place at least proportionally with the formation of allophanate groups. The present invention also relates to the binders obtained by the process of the invention.
摘要翻译：本发明涉及一种制备粘合剂的方法，其包含1）脲基甲酸酯基团，2）与烯键式不饱和化合物反应的基团与暴露于光化辐射（辐射固化基团）和3）任选的NCO-反应性基团反应的基团， A）一种或多种含有脲二酮基团的NCO-官能化合物，B）一种或多种含有异氰酸酯反应性基团的化合物和与烯键式不饱和化合物反应而与光化辐射（辐射 - 固化基团），然后C）与除了B）之外的一种或多种饱和的含羟基化合物，在D的存在下，在具有OH官能度≥2的这些化合物中的至少一种的化合物中含有一种或多种铵脂肪族或脂环族羧酸的盐或鏻盐，与化合物C）的反应至少与脲基甲酸酯基团的形成成比例地发生。本发明还涉及通过本发明的方法获得的粘合剂。

6. 发明授权

US09080010B2 Process for preparing polyether carbonate polyols with double metal cyanide catalysts and in the presence of metal salts 有权
标题翻译：用双金属氰化物催化剂和金属盐存在下制备聚醚碳酸酯多元醇的方法
公开(公告)号：US09080010B2
公开(公告)日：2015-07-14
申请号：US13579222
申请日：2011-02-17
申请人： Aurel Wolf , Stefan Grasser , Christoph Gürtler , Jörg Hofmann
发明人： Aurel Wolf , Stefan Grasser , Christoph Gürtler , Jörg Hofmann
IPC分类号： C08G65/04 , C08G64/34 , C08G18/44 , C08G65/26 , C08G64/20 , C08G18/32
CPC分类号： C08G64/34 , C08G18/32 , C08G18/44 , C08G64/205 , C08G65/2603 , C08G65/2663 , C08G65/2696
摘要： The present invention relates to a process for the preparation of polyether carbonate polyols by catalytic copolymerization of carbon dioxide (CO2) with alkylene oxides in the presence of one or more H-functional starter substances with the aid of double metal cyanide (DMC) catalysts and in the presence of metal salts.
摘要翻译：本发明涉及一种通过在双金属氰化物（DMC）催化剂的帮助下，在一种或多种H官能起始物质存在下，通过二氧化碳（CO 2）与环氧烷的催化共聚制备聚醚碳酸酯多元醇的方法，在金属盐的存在下。

7. 发明授权

US09045592B2 Process for the preparation of polyether carbonate polyols 有权
标题翻译：制备聚醚碳酸酯多元醇的方法
公开(公告)号：US09045592B2
公开(公告)日：2015-06-02
申请号：US13821254
申请日：2011-09-06
申请人： Christoph Gürtler , Jörg Hofmann , Aurel Wolf , Stefan Grasser
发明人： Christoph Gürtler , Jörg Hofmann , Aurel Wolf , Stefan Grasser
IPC分类号： C08G64/32 , C08G64/34 , C08G64/18 , C08G65/26 , C08G59/20
CPC分类号： C08G64/34 , C08G64/183 , C08G65/2603 , C08G65/2663
摘要： The present invention relates to a process for the preparation of polyether carbonate polyols from one or more alkylene oxides, carbon dioxide and optionally from one or more H-functional starter substances in the presence of at least one double metal cyanide catalyst, wherein the double metal cyanide catalyst comprises an unsaturated alcohol as a complexing ligand.
摘要翻译：本发明涉及一种在至少一种双金属氰化物催化剂存在下由一种或多种烯化氧，二氧化碳和任选地由一种或多种H官能起始物质制备聚醚碳酸酯多元醇的方法，其中双金属氰化物催化剂包含不饱和醇作为络合配体。

8. 发明申请

US20140221602A1 METHOD FOR ACTIVATING DOUBLE METAL CYANIDE CATALYSTS FOR THE PRODUCTION OF POLYETHER CARBONATE POLYOLS 有权
标题翻译：用于生产聚碳酸酯多元醇的双金属氰化物催化剂的活化方法
公开(公告)号：US20140221602A1
公开(公告)日：2014-08-07
申请号：US14232633
申请日：2012-07-16
申请人： Thomas Ernst Müller , Christoph Gürtler , Yvonne Dienes , Julien Barruet , Burkhard Köhler , Walter Leitner
发明人： Thomas Ernst Müller , Christoph Gürtler , Yvonne Dienes , Julien Barruet , Burkhard Köhler , Walter Leitner
IPC分类号： C08G64/32
CPC分类号： C08G64/323 , C08G64/34 , C08G65/2603 , C08G65/2663
摘要： The present invention relates to a process for the activation of double metal cyanide (DMC) catalysts with heterocumulenes for the preparation of polyether carbonate polyols by catalytic copolymerization of carbon dioxide (CO2) with alkylene oxides in the presence of one or more H-functional starter substances, and to a process for the preparation of polyether carbonate polyols from one or more H-functional starter substances, one or more alkylene oxides and carbon dioxide in the presence of a double metal cyanide catalyst, characterized in that (α) under an inert gas atmosphere, under an atmosphere of an inert gas/carbon dioxide mixture or under a pure carbon dioxide atmosphere, at temperatures of from 90 to 150° C., the DMC catalyst is mixed with a heterocumulene and H-functional starter substance, (β) alkylene oxide is added at temperatures of from 100 to 150° C. to the mixture from step (α) under an inert gas atmosphere, under an atmosphere of an inert gas/carbon dioxide mixture or under a pure carbon dioxide atmosphere, and (γ) one or more alkylene oxides and carbon dioxide are metered continuously into the mixture resulting from step (β).
摘要翻译：本发明涉及一种用于通过在一种或多种H功能性起始剂存在下通过二氧化碳（CO 2）与氧化烯的催化共聚来制备聚醚碳酸酯多元醇的异氰脲酸双金属氰化物（DMC）催化剂的活化方法以及在双金属氰化物催化剂存在下从一种或多种H官能起始物质，一种或多种环氧烷和二氧化碳制备聚醚碳酸酯多元醇的方法，其特征在于（α）在惰性气体气氛中，在惰性气体/二氧化碳混合气氛下或在纯二氧化碳气氛下，在90〜150℃的温度下，将DMC催化剂与杂多烯和H官能起始物质（＆bgr ;）在惰性气体气氛下，在惰性气体/二氧化碳气氛下，将氧化烯在100至150℃的温度下加入步骤（α）的混合物中或者在纯二氧化碳气氛下，将（γ）一种或多种烯化氧和二氧化碳连续计量到由步骤（bgr）得到的混合物中。

9. 发明申请

US20130296450A1 METHOD FOR PRODUCING POLYETHER CARBONATE POLYOLS HAVING PRIMARY HYDROXYL END GROUPS AND POLYURETHANE POLYMERS PRODUCED THEREFROM 审中-公开
标题翻译：生产具有主要羟基末端基团的聚碳酸酯多元醇的方法和由其生产的聚氨酯聚合物
公开(公告)号：US20130296450A1
公开(公告)日：2013-11-07
申请号：US13994449
申请日：2011-12-12
申请人： Jörg Hofmann , Christoph Gürtler , Hartmut Nefzger , Norbert Hahn , Klaus Lorenz , Thomas Ernst Müller
发明人： Jörg Hofmann , Christoph Gürtler , Hartmut Nefzger , Norbert Hahn , Klaus Lorenz , Thomas Ernst Müller
IPC分类号： C08G64/34 , C08G18/48 , C08G64/02
CPC分类号： C08G64/34 , C08G18/4018 , C08G18/4261 , C08G18/44 , C08G18/4887 , C08G64/0208 , C08G64/183 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要： The present invention relates to a process for the preparation of polyether carbonate polyols with primary hydroxyl end groups, comprising the steps of reaction of a starter compound containing active hydrogen atoms with an epoxide and carbon dioxide under double metal cyanide catalysis, reaction of the product obtained with a cyclic carboxylic acid anhydride and reaction of this product obtained with ethylene oxide in the presence of a catalyst which contains at least one nitrogen atom per molecule, excluding non-cyclic tertiary amines with identical substituents. The invention furthermore relates to polyether carbonate polyols obtainable by this process, compositions comprising these polyether carbonate polyols and polyurethane polymers based on these polyether carbonate polyols.
摘要翻译：本发明涉及一种制备具有伯羟基端基的聚醚碳酸酯多元醇的方法，包括在双金属氰化物催化下使含有活性氢原子的起始化合物与环氧化物和二氧化碳反应的步骤，所得产物的反应与环状羧酸酐反应，并在每分子含有至少一个氮原子的催化剂存在下，与环氧乙烷反应，除去具有相同取代基的非环状叔胺。本发明还涉及通过该方法获得的聚醚碳酸酯多元醇，包含这些聚醚碳酸酯多元醇和基于这些聚醚碳酸酯多元醇的聚氨酯聚合物的组合物。

10. 发明申请

US20120148478A1 PROCESS FOR THE PREPARATION OF CHLORINE BY GAS PHASE OXIDATION ON NANOSTRUCTURED SUPPORTED RUTHENIUM CATALYSTS 审中-公开
标题翻译：通过气相氧化在纳米结构支持的钌催化剂上制备氯的方法
公开(公告)号：US20120148478A1
公开(公告)日：2012-06-14
申请号：US13384792
申请日：2010-07-14
申请人： Timm Schmidt , Christoph Gürtler , Jürgen Kintrup , Thomas Ernst Müller , Tim Loddenkemper , Frank Gerhartz , Walther Müller
发明人： Timm Schmidt , Christoph Gürtler , Jürgen Kintrup , Thomas Ernst Müller , Tim Loddenkemper , Frank Gerhartz , Walther Müller
IPC分类号： C01B7/04 , B01J35/10 , B01J21/02 , B01J21/06 , B01J23/62 , B01J23/14 , B01J27/13 , B01J23/89 , B01J23/755 , B01J23/18 , B01J23/644 , B01J37/08 , B01J23/46 , B82Y30/00 , B82Y40/00
CPC分类号： C01B7/04 , B01J21/12 , B01J23/462 , B01J23/626 , B01J23/63 , B01J23/6445 , B01J23/6447 , B01J23/892 , B01J35/0013 , B01J35/006 , B01J35/023 , B01J35/04 , B01J35/1014 , B01J35/1042 , B01J35/108 , B01J37/0203 , B01J37/0211 , B01J37/349
摘要： The present invention relates to a process for the preparation of chlorine by gas phase oxidation using a supported catalyst based on ruthenium, characterised in that the catalyst support has a plurality of pores having a pore diameter>50 nm and carries nanoparticles containing ruthenium and/or ruthenium compounds as catalytically active components.
摘要翻译：本发明涉及一种使用基于钌的负载型催化剂通过气相氧化制备氯的方法，其特征在于催化剂载体具有多个孔径> 50nm的孔，并载有含钌和/或钌化合物作为催化活性组分。

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