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1. 发明申请

US20170107787A1 MICROWAVE INDUCED CURING OF NANOMATERIALS FOR GEOLOGICAL FORMATION REINFORCEMENT 审中-公开
公开(公告)号：US20170107787A1
公开(公告)日：2017-04-20
申请号：US15295509
申请日：2016-10-17
申请人： James M. Tour , Nam Dong Kim , Andrew Metzger , Anton Kovalchuk , Brandi Katherine Price-Hoelscher , James E. Friedheim
发明人： James M. Tour , Nam Dong Kim , Andrew Metzger , Anton Kovalchuk , Brandi Katherine Price-Hoelscher , James E. Friedheim
IPC分类号： E21B33/138 , C08J3/28 , C09K8/035 , C08K3/04 , C08F279/02 , C08K9/08 , C08J5/00 , C08J3/24
CPC分类号： E21B33/138 , C08F279/02 , C08J3/247 , C08J3/28 , C08J5/005 , C08J2309/00 , C08K3/042 , C08K9/08 , C09K8/03 , C09K8/516 , C09K8/56 , C09K2208/08 , C09K2208/10 , C08F222/1006 , C08L71/00
摘要： Embodiments of the present disclosure pertain to methods of forming a polymer composite by exposing a solution that includes nanomaterials (e.g., functionalized graphene nanoribbons) and cross-linkable polymer components (e.g., thermoset polymers and monomers) to a microwave source, where the exposing results in the curing of the cross-linkable polymer component in the presence of the nanomaterial to form the polymer composite. The solution may be exposed to a microwave source in a geological formation such that the formed polymer composite becomes embedded with the geological formation and thereby enhances the stability of the geological formation. Additional embodiments of the present disclosure pertain to the aforementioned polymer composites.

2. 发明申请

US20140120024A1 METHODS FOR PREPARATION OF GRAPHENE NANORIBBONS FROM CARBON NANOTUBES AND COMPOSITIONS, THIN FILMS AND DEVICES DERIVED THEREFROM 审中-公开
标题翻译：从碳纳米管和组合物制备石墨纳米颗粒的方法，薄膜和其衍生的器件
公开(公告)号：US20140120024A1
公开(公告)日：2014-05-01
申请号：US14148159
申请日：2014-01-06
申请人： James M. Tour , Dmitry V. Kosynkin , Amanda Dugue , Brandi Katherine Price-Hoelscher
发明人： James M. Tour , Dmitry V. Kosynkin , Amanda Dugue , Brandi Katherine Price-Hoelscher
IPC分类号： C01B31/04
CPC分类号： C01B32/184 , B82Y30/00 , B82Y40/00 , C01B32/194 , C01B32/23 , C01B2204/06 , C04B14/024 , H01J9/025 , Y10S977/734 , Y10S977/842
摘要： Methods for producing macroscopic quantities of oxidized graphene nanoribbons are disclosed herein. The methods include providing a plurality of carbon nanotubes and reacting the plurality of carbon nanotubes with at least one oxidant to form oxidized graphene nanoribbons. The at least one oxidant is operable to longitudinally open the carbon nanotubes. In some embodiments, the reacting step takes place in the presence of at least one acid. In some embodiments, the reacting step takes place in the presence of at least one protective agent. Various embodiments of the present disclosure also include methods for producing reduced graphene nanoribbons by reacting oxidized graphene nanoribbons with at least one reducing agent. Oxidized graphene nanoribbons, reduced graphene nanoribbons and compositions and articles derived therefrom are also disclosed herein.
摘要翻译：本文公开了生产宏观量的氧化石墨烯纳米带的方法。所述方法包括提供多个碳纳米管并使多个碳纳米管与至少一种氧化剂反应以形成氧化石墨烯纳米带。至少一种氧化剂可操作以纵向打开碳纳米管。在一些实施方案中，反应步骤在至少一种酸的存在下进行。在一些实施方案中，反应步骤在至少一种保护剂的存在下进行。本公开的各种实施方案还包括通过使氧化石墨烯纳米带与至少一种还原剂反应来生产还原的石墨烯纳米带的方法。氧化石墨烯纳米带，还原石墨烯纳米带以及由其衍生的组合物和制品也在本文中公开。

3. 发明授权

US09449743B2 Synthesis of magnetic carbon nanoribbons and magnetic functionalized carbon nanoribbons 有权
标题翻译：磁性碳纳米带和磁性官能化碳纳米带的合成
公开(公告)号：US09449743B2
公开(公告)日：2016-09-20
申请号：US14374591
申请日：2013-01-28
申请人： James M. Tour , Bostjan Genorio , Wei Lu , Brandi Katherine Price-Hoelscher
发明人： James M. Tour , Bostjan Genorio , Wei Lu , Brandi Katherine Price-Hoelscher
IPC分类号： H01F1/34 , C01B31/02 , H01F1/01 , C09K8/03 , C09K8/32 , C09K8/36 , E21B21/00 , C01B31/04 , B82Y30/00 , B82Y40/00 , E21B47/12
CPC分类号： H01F1/01 , B82Y30/00 , B82Y40/00 , C01B32/168 , C01B32/194 , C09K8/032 , C09K8/32 , C09K8/36 , C09K2208/10 , E21B21/00 , E21B47/12
摘要： Various embodiments of the present disclosure pertain to methods of making magnetic carbon nanoribbons. Such methods generally include: (1) forming carbon nanoribbons by splitting carbon nanomaterials; and (2) associating graphene nanoribbons with magnetic materials, precursors of magnetic materials, or combinations thereof. Further embodiments of the present disclosure also include a step of reducing the precursors of magnetic materials to magnetic materials. In various embodiments, the associating occurs before, during or after the splitting of the carbon nanomaterials. In some embodiments, the methods of the present disclosure further comprise a step of (3) functionalizing the carbon nanoribbons with functionalizing agents. In more specific embodiments, the functionalizing occurs in situ during the splitting of carbon nanomaterials. In further embodiments, the carbon nanoribbons are edge-functionalized. Additional embodiments of the present disclosure pertain to magnetic carbon nanoribbon compositions that were formed in accordance with the methods of the present disclosure.
摘要翻译：本公开的各种实施方案涉及制备磁性碳纳米带的方法。这些方法通常包括：（1）通过分解碳纳米材料形成碳纳米带; 和（2）将石墨烯纳米带与磁性材料，磁性材料的前体或其组合相关联。本公开的另外的实施方案还包括将磁性材料的前体还原成磁性材料的步骤。在各种实施方案中，缔合发生在碳纳米材料分裂之前，期间或之后。在一些实施方案中，本公开的方法还包括（3）用官能化试剂官能化碳纳米带的步骤。在更具体的实施方案中，官能化在碳纳米材料分裂过程中就地发生。在另外的实施方案中，碳纳米带是边缘官能化的。本公开的另外的实施方案涉及根据本公开的方法形成的磁性碳纳米纤维组合物。

4. 发明申请

US20150108391A1 SYNTHESIS OF MAGNETIC CARBON NANORIBBONS AND MAGNETIC FUNCTIONALIZED CARBON NANORIBBONS 有权
标题翻译：磁性纳米颗粒和磁性功能碳纳米管的合成
公开(公告)号：US20150108391A1
公开(公告)日：2015-04-23
申请号：US14374591
申请日：2013-01-28
申请人： James M. Tour , Bostjan Genorio , Wei Lu , Brandi Katherine Price-Hoelscher
发明人： James M. Tour , Bostjan Genorio , Wei Lu , Brandi Katherine Price-Hoelscher
IPC分类号： H01F1/01
CPC分类号： H01F1/01 , B82Y30/00 , B82Y40/00 , C01B32/168 , C01B32/194 , C09K8/032 , C09K8/32 , C09K8/36 , C09K2208/10 , E21B21/00 , E21B47/12
摘要： Various embodiments of the present disclosure pertain to methods of making magnetic carbon nanoribbons. Such methods generally include: (1) forming carbon nanoribbons by splitting carbon nanomaterials; and (2) associating graphene nanoribbons with magnetic materials, precursors of magnetic materials, or combinations thereof. Further embodiments of the present disclosure also include a step of reducing the precursors of magnetic materials to magnetic materials. In various embodiments, the associating occurs before, during or after the splitting of the carbon nanomaterials. In some embodiments, the methods of the present disclosure further comprise a step of (3) functionalizing the carbon nanoribbons with functionalizing agents. In more specific embodiments, the functionalizing occurs in situ during the splitting of carbon nanomaterials. In further embodiments, the carbon nanoribbons are edge-functionalized. Additional embodiments of the present disclosure pertain to magnetic carbon nanoribbon compositions that were formed in accordance with the methods of the present disclosure.
摘要翻译：本公开的各种实施方案涉及制备磁性碳纳米带的方法。这些方法通常包括：（1）通过分解碳纳米材料形成碳纳米带; 和（2）将石墨烯纳米带与磁性材料，磁性材料的前体或其组合相关联。本公开的另外的实施方案还包括将磁性材料的前体还原成磁性材料的步骤。在各种实施方案中，缔合发生在碳纳米材料分裂之前，期间或之后。在一些实施方案中，本公开的方法还包括（3）用官能化试剂官能化碳纳米带的步骤。在更具体的实施方案中，官能化在碳纳米材料分裂过程中就地发生。在另外的实施方案中，碳纳米带是边缘官能化的。本公开的另外的实施方案涉及根据本公开的方法形成的磁性碳纳米纤维组合物。

5. 发明申请

US20170096600A1 GRAPHENE QUANTUM DOT-POLYMER COMPOSITES AND METHODS OF MAKING THE SAME 审中-公开
公开(公告)号：US20170096600A1
公开(公告)日：2017-04-06
申请号：US15314224
申请日：2015-05-22
申请人： James M. Tour , Anton Kovalchuk , Xiang Changsheng
发明人： James M. Tour , Anton Kovalchuk , Xiang Changsheng
IPC分类号： C09K11/02 , C08J5/18 , C08K3/04 , C08K9/04 , C09K11/65 , C09K11/06
CPC分类号： C09K11/025 , B82Y20/00 , B82Y30/00 , B82Y40/00 , C08J5/18 , C08J2329/04 , C08K3/04 , C08K3/042 , C08K9/04 , C08K2201/011 , C09K11/06 , C09K11/65 , C09K2211/10 , Y10S977/734 , Y10S977/842 , Y10S977/847 , Y10S977/95 , C08L101/00 , C08L29/04 , C08L25/06
摘要： Various embodiments of the present disclosure pertain to methods of forming polymer composites that include polymers and graphene quantum dots. The methods occur by mixing a polymer component (e.g., polymers, polymer precursors and combinations thereof) with graphene quantum dots. In some embodiments, the polymers are in the form of a polymer matrix, and the graphene quantum dots are homogenously dispersed within the polymer matrix. In some embodiments, the graphene quantum dots include, without limitation, coal-derived graphene quantum dots, coke-derived graphene quantum dots, unfunctionalized graphene quantum dots, functionalized graphene quantum dots, pristine graphene quantum dots, and combinations thereof. Additional embodiments of the present disclosure pertain to polymer composites that are formed by the methods of the present disclosure. In some embodiments, the polymer composites of the present disclosure are fluorescent and optically transparent. In some embodiments, the polymer composites of the present disclosure are in the form of a film.

6. 发明授权

US09493355B2 Solvent-based methods for production of graphene nanoribbons 有权
标题翻译：用于生产石墨烯纳米带的基于溶剂的方法
公开(公告)号：US09493355B2
公开(公告)日：2016-11-15
申请号：US14345016
申请日：2012-09-14
申请人： James M. Tour , Wei Lu , Bostjan Genorio
发明人： James M. Tour , Wei Lu , Bostjan Genorio
IPC分类号： C01B31/02 , C07C29/32 , C08F112/08 , C01B31/04
CPC分类号： C08F112/08 , B82Y30/00 , B82Y40/00 , C01B32/174 , C01B32/178 , C01B32/18 , C01B32/184 , C01B32/194 , C01B2202/06 , C01B2204/06 , C07C2/76 , C07C15/56 , C07C29/32 , C07C67/035 , C07C69/76 , D01F9/12 , Y10S977/734 , Y10S977/846 , Y10S977/961
摘要： The present invention provides methods of preparing functionalized graphene nanoribbons. Such methods include: (1) exposing a plurality of carbon nanotubes (CNTs) to an alkali metal source in the presence of an aprotic solvent to open them; and (2) exposing the opened CNTs to an electrophile to form functionalized graphene nanoribbons (GNRs). The methods may also include a step of exposing the opened CNTs to a protic solvent to quench any reactive species on them. Additional methods include preparing unfunctionalized GNRs by: (1) exposing a plurality of CNTs to an alkali metal source in the presence of an aprotic solvent to open them; and (2) exposing the opened CNTs to a protic solvent to form unfunctionalized GNRs.
摘要翻译：本发明提供了制备官能化石墨烯纳米带的方法。这些方法包括：（1）在非质子溶剂的存在下将多个碳纳米管（CNT）暴露于碱金属源以将其打开; 和（2）将开放的CNT暴露于亲电子试剂以形成官能化的石墨烯纳米带（GNR）。所述方法还可以包括将开放的CNT暴露于质子溶剂以淬灭其上的任何反应性物质的步骤。另外的方法包括：通过以下步骤制备未官能化的GNR：（1）在非质子溶剂存在下将多个CNT暴露于碱金属源以打开它们; 和（2）将开放的CNT暴露于质子溶剂以形成未官能化的GNR。

7. 发明授权

US09356151B2 Fabrication of graphene nanoribbons and nanowires using a meniscus as an etch mask 有权
标题翻译：使用弯月面作为蚀刻掩模制造石墨烯纳米带和纳米线
公开(公告)号：US09356151B2
公开(公告)日：2016-05-31
申请号：US14171642
申请日：2014-02-03
申请人： James M. Tour , Vera Abramova , Alexander Slesarev
发明人： James M. Tour , Vera Abramova , Alexander Slesarev
IPC分类号： H01L21/44 , H01L29/786 , C01B31/04 , H01L21/3065 , H01L21/311 , H01L21/3213 , H01L29/66 , B82Y40/00
CPC分类号： H01L29/78684 , B82Y40/00 , C01B32/182 , C01B32/194 , H01L21/3065 , H01L21/31116 , H01L21/32131 , H01L29/66742 , H01L29/78606 , H01L29/78696
摘要： In some embodiments, the present disclosure pertains to methods of preparing graphene nanoribbons from a graphene film associated with a meniscus, where the method comprises patterning the graphene film while the meniscus acts as a mask above a region of the graphene film, and where the patterning results in formation of graphene nanoribbons from the meniscus-masked region of the graphene film. Additional embodiments of the present disclosure pertain to methods of preparing wires from a film associated with a meniscus, where the method comprises patterning the film while the meniscus acts as a mask above a region of the film, and where the patterning results in formation of a wire from the meniscus-masked region of the film. Additional embodiments of the present disclosure pertain to chemical methods of preparing wires from water-reactive materials.
摘要翻译：在一些实施方案中，本公开涉及从与弯液面相关联的石墨烯膜制备石墨烯纳米带的方法，其中所述方法包括图案化所述石墨烯膜，同时所述弯液面用作所述石墨烯膜的区域上方的掩模，并且其中所述图案化导致从石墨烯膜的弯液面掩蔽区域形成石墨烯纳米带。本公开的另外的实施例涉及从与弯液面相关联的膜制备线的方法，其中所述方法包括图案化所述膜，同时所述弯月面用作所述膜的区域上方的掩模，并且其中所述图案化导致形成电线从弯月面掩盖的区域。本公开的另外的实施方案涉及从水反应性材料制备电线的化学方法。

8. 发明申请

US20150162381A1 ADDRESSABLE SIOX MEMORY ARRAY WITH INCORPORATED DIODES 有权
标题翻译：可寻址的存储器阵列与入射二极管
公开(公告)号：US20150162381A1
公开(公告)日：2015-06-11
申请号：US14240973
申请日：2012-08-27
申请人： James M. Tour , Jun Yao , Jian Lin , Gunuk Wang , Krishna Palem
发明人： James M. Tour , Jun Yao , Jian Lin , Gunuk Wang , Krishna Palem
IPC分类号： H01L27/24 , H01L29/66 , H01L45/00
CPC分类号： H01L27/2463 , H01L27/2409 , H01L29/66136 , H01L29/66143 , H01L29/8611 , H01L29/8613 , H01L29/872 , H01L45/04 , H01L45/1233 , H01L45/1253 , H01L45/145 , H01L45/1608 , H01L45/1616 , H01L45/1625 , H01L45/1675
摘要： Various embodiments of the resistive memory cells and arrays discussed herein comprise: (1) a first electrode; (2) a second electrode; (3) resistive memory material; and (4) a diode. The resistive memory material is selected from the group consisting of SiOx, SiOxH, SiOxNy, SiOxNyH, SiOxCz, SiOxCzH, and combinations thereof, wherein each of x, y and z are equal or greater than 1 or equal or less than 2. The diode may be any suitable diode, such as n-p diodes, p-n diodes, and Schottky diodes.
摘要翻译：本文讨论的电阻式存储器单元和阵列的各种实施例包括：（1）第一电极; （2）第二电极; （3）电阻记忆材料; 和（4）二极管。电阻性存储材料选自SiOx，SiOxH，SiOxNy，SiOxNyH，SiOxCz，SiOxCzH及其组合，其中x，y和z各自等于或大于1或等于或小于2.二极管可以是任何合适的二极管，例如np二极管，pn二极管和肖特基二极管。

9. 发明申请

US20150023858A1 REBAR HYBRID MATERIALS AND METHODS OF MAKING THE SAME 有权
标题翻译： REBAR混合材料及其制备方法
公开(公告)号：US20150023858A1
公开(公告)日：2015-01-22
申请号：US14335566
申请日：2014-07-18
申请人： James M. Tour , Zheng Yan , Zhiwei Peng , Robert H. Hauge , Yilun Li
发明人： James M. Tour , Zheng Yan , Zhiwei Peng , Robert H. Hauge , Yilun Li
IPC分类号： C01B31/36 , B29C39/00 , H01B1/04 , C01B31/04 , C01B31/02
CPC分类号： C01B32/956 , B29C39/003 , B29K2105/124 , B29K2995/0005 , B29L2007/00 , C01B21/064 , C01B32/178 , C01B32/18 , C01B32/184 , C01B32/186 , C01P2004/13
摘要： In some embodiments, the present disclosure pertains to methods of forming a reinforcing material by: (1) depositing a first material onto a catalyst surface; and (2) forming a second material on the catalyst surface, where the second material is derived from and associated with the first material. In some embodiments, the first material includes, without limitation, carbon nanotubes, graphene nanoribbons, boron nitride nanotubes, chalcogenide nanotubes, carbon onions, and combinations thereof. In some embodiments, the formed second material includes, without limitation, graphene, hexagonal boron nitride, chalcogenides, and combinations thereof. In additional embodiments, the methods of the present disclosure also include a step of separating the formed reinforcing material from the catalyst surface, and transferring the separated reinforcing material onto a substrate without the use of polymers. Additional embodiments of the present disclosure pertain to reinforcing materials formed by the aforementioned methods.
摘要翻译：在一些实施方案中，本公开涉及通过以下步骤形成增强材料的方法：（1）将第一材料沉积到催化剂表面上; 和（2）在所述催化剂表面上形成第二材料，其中所述第二材料衍生并与所述第一材料相关联。在一些实施方案中，第一材料包括但不限于碳纳米管，石墨烯纳米带，氮化硼纳米管，硫族化物纳米管，碳鎓和它们的组合。在一些实施例中，所形成的第二材料包括但不限于石墨烯，六方氮化硼，硫族化合物及其组合。在另外的实施方案中，本公开的方法还包括将形成的增强材料从催化剂表面分离并将分离的增强材料转移到基材上而不使用聚合物的步骤。本公开的另外的实施方案涉及通过上述方法形成的增强材料。

10. 发明授权

US08703090B2 Methods for preparation of graphene nanoribbons from carbon nanotubes and compositions, thin films and devices derived therefrom 有权
标题翻译：从碳纳米管和组合物制备石墨烯纳米带的方法，由其衍生的薄膜和器件
公开(公告)号：US08703090B2
公开(公告)日：2014-04-22
申请号：US12544017
申请日：2009-08-19
申请人： James M. Tour , Dmitry V. Kosynkin , Amanda Higginbotham , Brandi Katherine Price
发明人： James M. Tour , Dmitry V. Kosynkin , Amanda Higginbotham , Brandi Katherine Price
IPC分类号： D01F9/12 , C01B31/00 , C08F290/14
CPC分类号： C01B31/0446 , B82Y30/00 , B82Y40/00 , C01B32/184 , C01B32/194 , C01B32/23 , C01B2204/06 , H01J9/025 , Y10S977/734 , Y10S977/842
摘要： Methods for producing macroscopic quantities of oxidized graphene nanoribbons are disclosed herein. The methods include providing a plurality of carbon nanotubes and reacting the plurality of carbon nanotubes with at least one oxidant to form oxidized graphene nanoribbons. The at least one oxidant is operable to longitudinally open the carbon nanotubes. In some embodiments, the reacting step takes place in the presence of at least one acid. In some embodiments, the reacting step takes place in the presence of at least one protective agent. Various embodiments of the present disclosure also include methods for producing reduced graphene nanoribbons by reacting oxidized graphene nanoribbons with at least one reducing agent. Oxidized graphene nanoribbons, reduced graphene nanoribbons and compositions and articles derived therefrom are also disclosed herein.
摘要翻译：本文公开了生产宏观量的氧化石墨烯纳米带的方法。所述方法包括提供多个碳纳米管并使多个碳纳米管与至少一种氧化剂反应以形成氧化石墨烯纳米带。至少一种氧化剂可操作以纵向打开碳纳米管。在一些实施方案中，反应步骤在至少一种酸的存在下进行。在一些实施方案中，反应步骤在至少一种保护剂的存在下进行。本公开的各种实施方案还包括通过使氧化石墨烯纳米带与至少一种还原剂反应来生产还原的石墨烯纳米带的方法。氧化石墨烯纳米带，还原石墨烯纳米带以及由其衍生的组合物和制品也在本文中公开。

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