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1. 发明申请

US20120114929A1 HIGH PURITY CERAMIC ABRADABLE COATINGS 有权
标题翻译：高纯度陶瓷不可磨损涂料
公开(公告)号：US20120114929A1
公开(公告)日：2012-05-10
申请号：US12960107
申请日：2010-12-03
申请人： Liangde Xie , Mitchell Dorfman , Richard Schmid , Jacobus C. Doesburg , Matthew Gold
发明人： Liangde Xie , Mitchell Dorfman , Richard Schmid , Jacobus C. Doesburg , Matthew Gold
IPC分类号： B32B18/00 , B32B15/04 , B32B5/22 , B32B33/00
CPC分类号： C04B35/486 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3246 , C04B2235/72 , C23C4/11 , C23C14/083 , C23C30/00 , F01D5/288 , Y02T50/67 , Y02T50/672 , Y10T428/12611 , Y10T428/12618 , Y10T428/12667 , Y10T428/24 , Y10T428/24471 , Y10T428/24997 , Y10T428/25 , Y10T428/252 , Y10T428/26 , Y10T428/2982
摘要： The invention is directed to a material and method for obtaining a ceramic abradable system for high temperature applications. High purity partially stabilized zirconia and/or hafnia base material has higher sintering resistance compared to conventional 6-9 weight percent yttria stabilized zirconia systems. The benefits of these systems are higher service lifetime and low thermal conductivity to achieve high operating temperatures. System includes a superalloy substrate, oxidation resistant bond coat and a thick ceramic abradable top coat. Total coating thickness is about 0.5-5 mm. In some applications an intermediate layer of high purity partially stabilized zirconia or a partially stabilized YSZ/MCrAlY cermet is applied over the oxidation resistant bond coat. In other applications an abradable system is applied on top of a grid. Additional benefits should be reduced blade wear at high operating conditions.
摘要翻译：本发明涉及用于获得用于高温应用的陶瓷耐磨系统的材料和方法。与常规6-9重量％的氧化钇稳定的氧化锆体系相比，高纯度部分稳定的氧化锆和/或铪基材料具有更高的耐烧结性。这些系统的优点是更高的使用寿命和较低的热导率，以达到高的工作温度。系统包括超合金基材，抗氧化粘合涂层和厚陶瓷耐磨面漆。总涂层厚度约为0.5-5毫米。在一些应用中，将高纯度部分稳定的氧化锆或部分稳定的YSZ / MCrAlY金属陶瓷的中间层涂覆在抗氧化粘合涂层上。在其他应用中，可磨损系统应用于网格顶部。额外的好处应该是在高操作条件下减少刀片磨损。

2. 发明授权

US07955708B2 Optimized high temperature thermal barrier 有权
标题翻译：优化的高温热障
公开(公告)号：US07955708B2
公开(公告)日：2011-06-07
申请号：US11520044
申请日：2006-09-13
申请人： Jacobus C. Doesburg , Liangde Xie , Richard Schmid , Matthew Gold
发明人： Jacobus C. Doesburg , Liangde Xie , Richard Schmid , Matthew Gold
IPC分类号： B32B18/00 , C04B41/87
CPC分类号： C04B35/486 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3246 , C04B2235/72 , C23C4/11 , C23C14/083 , C23C30/00 , F01D5/288 , Y02T50/67 , Y02T50/672 , Y10T428/12611 , Y10T428/12618 , Y10T428/12667 , Y10T428/24 , Y10T428/24471 , Y10T428/24997 , Y10T428/25 , Y10T428/252 , Y10T428/26 , Y10T428/2982
摘要： The invention is directed to high purity zirconia-based and/or hafnia-based materials and coatings for high temperature cycling applications. Thermal barrier coatings made from the invention high purity material was found to have significantly improved sintering resistance relative to coatings made from current materials of lower purity. The invention materials are high purity zirconia and/or hafnia partially or fully stabilized by one or any combinations of the following stabilizers: yttria, ytterbia, scandia, lanthanide oxide and actinide oxide. Limits for impurity oxide, oxides other than the intended ingredients, that lead to significantly improved sintering resistance were discovered. High purity coating structures suitable for high temperature cycling applications and for application onto a substrate were provided. In one structure, the coating comprises a ceramic matrix, porosity and micro cracks. In another structure, the coating comprises a ceramic matrix, porosity, macro cracks and micro cracks. In another structure, the coating comprises ceramic columns and gaps between the columns. In another structure, the coating comprises ceramic columns, gaps between the columns and nodules distributing randomly in the gaps and columns.
摘要翻译：本发明涉及用于高温循环应用的高纯度氧化锆基和/或基于铪的材料和涂层。发现由本发明的高纯度材料制成的热障涂层相对于由现有低纯度材料制成的涂层具有显着改善的耐烧结性。本发明的材料是由以下稳定剂的一种或任何组合部分或完全稳定的高纯度氧化锆和/或铪：氧化钇，镱，钪，氧化镧和锕系氧化物。发现了杂质氧化物，除目标成分以外的氧化物，导致显着提高耐烧结性的限制。提供了适用于高温循环应用和应用于基底的高纯度涂层结构。在一种结构中，涂层包括陶瓷基体，孔隙和微裂纹。在另一种结构中，涂层包括陶瓷基体，多孔性，宏观裂纹和微裂纹。在另一种结构中，涂层包括陶瓷柱和柱之间的间隙。在另一种结构中，涂层包括陶瓷柱，柱之间的间隙和结节随机分布在间隙和柱中。

3. 发明申请

US20110003119A1 OPTIMIZED HIGH TEMPERATURE THERMAL BARRIER 有权
标题翻译：优化高温热障
公开(公告)号：US20110003119A1
公开(公告)日：2011-01-06
申请号：US11520044
申请日：2006-09-13
申请人： Jacobus C. Doesburg , Liangde Xie , Richard Schmid , Matthew Gold
发明人： Jacobus C. Doesburg , Liangde Xie , Richard Schmid , Matthew Gold
IPC分类号： B32B3/00 , B32B15/04
CPC分类号： C04B35/486 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3246 , C04B2235/72 , C23C4/11 , C23C14/083 , C23C30/00 , F01D5/288 , Y02T50/67 , Y02T50/672 , Y10T428/12611 , Y10T428/12618 , Y10T428/12667 , Y10T428/24 , Y10T428/24471 , Y10T428/24997 , Y10T428/25 , Y10T428/252 , Y10T428/26 , Y10T428/2982
摘要： The invention is directed to high purity zirconia-based and/or hafnia-based materials and coatings for high temperature cycling applications. Thermal barrier coatings made from the invention high purity material was found to have significantly improved sintering resistance relative to coatings made from current materials of lower purity. The invention materials are high purity zirconia and/or hafnia partially or fully stabilized by one or any combinations of the following stabilizers: yttria, ytterbia, scandia, lanthanide oxide and actinide oxide. Limits for impurity oxide, oxides other than the intended ingredients, that lead to significantly improved sintering resistance were discovered. High purity coating structures suitable for high temperature cycling applications and for application onto a substrate were provided. In one structure, the coating comprises a ceramic matrix, porosity and micro cracks. In another structure, the coating comprises a ceramic matrix, porosity, macro cracks and micro cracks. In another structure, the coating comprises ceramic columns and gaps between the columns. In another structure, the coating comprises ceramic columns, gaps between the columns and nodules distributing randomly in the gaps and columns.
摘要翻译：本发明涉及用于高温循环应用的高纯度氧化锆基和/或基于铪的材料和涂层。发现由本发明的高纯度材料制成的热障涂层相对于由现有低纯度材料制成的涂层具有显着改善的耐烧结性。本发明的材料是由以下稳定剂的一种或任何组合部分或完全稳定的高纯度氧化锆和/或铪：氧化钇，镱，钪，氧化镧和锕系氧化物。发现了杂质氧化物，除目标成分以外的氧化物，导致显着提高耐烧结性的限制。提供了适用于高温循环应用和应用于基底的高纯度涂层结构。在一种结构中，涂层包括陶瓷基体，孔隙和微裂纹。在另一种结构中，涂层包括陶瓷基体，多孔性，宏观裂纹和微裂纹。在另一种结构中，涂层包括陶瓷柱和柱之间的间隙。在另一种结构中，涂层包括陶瓷柱，柱之间的间隙和结节随机分布在间隙和柱中。

4. 发明授权

US08187717B1 High purity ceramic abradable coatings 有权
标题翻译：高纯陶瓷耐磨涂层
公开(公告)号：US08187717B1
公开(公告)日：2012-05-29
申请号：US12960107
申请日：2010-12-03
申请人： Liangde Xie , Mitchell Dorfman , Richard Schmid , Jacobus C. Doesburg , Matthew Gold
发明人： Liangde Xie , Mitchell Dorfman , Richard Schmid , Jacobus C. Doesburg , Matthew Gold
IPC分类号： B32B18/00 , B05D1/36
CPC分类号： C04B35/486 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3246 , C04B2235/72 , C23C4/11 , C23C14/083 , C23C30/00 , F01D5/288 , Y02T50/67 , Y02T50/672 , Y10T428/12611 , Y10T428/12618 , Y10T428/12667 , Y10T428/24 , Y10T428/24471 , Y10T428/24997 , Y10T428/25 , Y10T428/252 , Y10T428/26 , Y10T428/2982
摘要： The invention is directed to a material and method for obtaining a ceramic abradable system for high temperature applications. High purity partially stabilized zirconia and/or hafnia base material has higher sintering resistance compared to conventional 6-9 weight percent yttria stabilized zirconia systems. The benefits of these systems are higher service lifetime and low thermal conductivity to achieve high operating temperatures. System includes a superalloy substrate, oxidation resistant bond coat and a thick ceramic abradable top coat. Total coating thickness is about 0.5-5 mm. In some applications an intermediate layer of high purity partially stabilized zirconia or a partially stabilized YSZ/MCrAlY cermet is applied over the oxidation resistant bond coat. In other applications an abradable system is applied on top of a grid. Additional benefits should be reduced blade wear at high operating conditions.
摘要翻译：本发明涉及用于获得用于高温应用的陶瓷耐磨系统的材料和方法。与常规6-9重量％的氧化钇稳定的氧化锆体系相比，高纯度部分稳定的氧化锆和/或铪基材料具有更高的耐烧结性。这些系统的优点是更高的使用寿命和较低的热导率，以达到高的工作温度。系统包括超合金基材，抗氧化粘合涂层和厚陶瓷耐磨面漆。总涂层厚度约为0.5-5毫米。在一些应用中，将高纯度部分稳定的氧化锆或部分稳定的YSZ / MCrAlY金属陶瓷的中间层涂覆在抗氧化粘合涂层上。在其他应用中，可磨损系统应用于网格顶部。额外的好处应该是在高操作条件下减少刀片磨损。

5. 发明授权

US07955707B2 High purity ceramic abradable coatings 有权
标题翻译：高纯陶瓷耐磨涂层
公开(公告)号：US07955707B2
公开(公告)日：2011-06-07
申请号：US11520041
申请日：2006-09-13
申请人： Liangde Xie , Mitchell Dorfman , Richard Schmid , Jacobus C. Doesburg , Matthew Gold
发明人： Liangde Xie , Mitchell Dorfman , Richard Schmid , Jacobus C. Doesburg , Matthew Gold
IPC分类号： B32B18/00 , B05D1/36
CPC分类号： C04B35/486 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3246 , C04B2235/72 , C23C4/11 , C23C14/083 , C23C30/00 , F01D5/288 , Y02T50/67 , Y02T50/672 , Y10T428/12611 , Y10T428/12618 , Y10T428/12667 , Y10T428/24 , Y10T428/24471 , Y10T428/24997 , Y10T428/25 , Y10T428/252 , Y10T428/26 , Y10T428/2982
摘要： The invention is directed to a material and method for obtaining a ceramic abradable system for high temperature applications. High purity partially stabilized zirconia and/or hafnia base material has higher sintering resistance compared to conventional 6-9 weight percent yttria stabilized zirconia systems. The benefits of these systems are higher service lifetime and low thermal conductivity to achieve high operating temperatures. System includes a superalloy substrate, oxidation resistant bond coat and a thick ceramic abradable top coat. Total coating thickness is about 0.5-5 mm. In some applications an intermediate layer of high purity partially stabilized zirconia or a partially stabilized YSZ/MCrAlY cermet is applied over the oxidation resistant bond coat. In other applications an abradable system is applied on top of a grid. Additional benefits should be reduced blade wear at high operating conditions.
摘要翻译：本发明涉及用于获得用于高温应用的陶瓷耐磨系统的材料和方法。与常规6-9重量％的氧化钇稳定的氧化锆体系相比，高纯度部分稳定的氧化锆和/或铪基材料具有更高的耐烧结性。这些系统的优点是更高的使用寿命和较低的热导率，以达到高的工作温度。系统包括超合金基材，抗氧化粘合涂层和厚陶瓷耐磨面漆。总涂层厚度约为0.5-5毫米。在一些应用中，将高纯度部分稳定的氧化锆或部分稳定的YSZ / MCrAlY金属陶瓷的中间层涂覆在抗氧化粘合涂层上。在其他应用中，可磨损系统应用于网格顶部。额外的好处应该是在高操作条件下减少刀片磨损。

6. 发明申请

US20100311562A1 HIGH PURITY CERAMIC ABRADABLE COATINGS 有权
标题翻译：高纯度陶瓷不可磨损涂料
公开(公告)号：US20100311562A1
公开(公告)日：2010-12-09
申请号：US11520041
申请日：2006-09-13
申请人： Liangde Xie , Mitchell Dorfman , Richard Schmid , Jacobus C. Doesburg , Matthew Gold
发明人： Liangde Xie , Mitchell Dorfman , Richard Schmid , Jacobus C. Doesburg , Matthew Gold
IPC分类号： C04B35/48 , B05D3/02
CPC分类号： C04B35/486 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3246 , C04B2235/72 , C23C4/11 , C23C14/083 , C23C30/00 , F01D5/288 , Y02T50/67 , Y02T50/672 , Y10T428/12611 , Y10T428/12618 , Y10T428/12667 , Y10T428/24 , Y10T428/24471 , Y10T428/24997 , Y10T428/25 , Y10T428/252 , Y10T428/26 , Y10T428/2982
摘要： The invention is directed to a material and method for obtaining a ceramic abradable system for high temperature applications. High purity partially stabilized zirconia and/or hafnia base material has higher sintering resistance compared to conventional 6-9 weight percent yttria stabilized zirconia systems. The benefits of these systems are higher service lifetime and low thermal conductivity to achieve high operating temperatures. System includes a superalloy substrate, oxidation resistant bond coat and a thick ceramic abradable top coat. Total coating thickness is about 0.5-5 mm. In some applications an intermediate layer of high purity partially stabilized zirconia or a partially stabilized YSZ/MCrAlY cermet is applied over the oxidation resistant bond coat. In other applications an abradable system is applied on top of a grid. Additional benefits should be reduced blade wear at high operating conditions.
摘要翻译：本发明涉及用于获得用于高温应用的陶瓷耐磨系统的材料和方法。与常规6-9重量％的氧化钇稳定的氧化锆体系相比，高纯度部分稳定的氧化锆和/或铪基材料具有更高的耐烧结性。这些系统的优点是更高的使用寿命和较低的热导率，以达到高的工作温度。系统包括超合金基材，抗氧化粘合涂层和厚陶瓷耐磨面漆。总涂层厚度约为0.5-5毫米。在一些应用中，将高纯度部分稳定的氧化锆或部分稳定的YSZ / MCrAlY金属陶瓷的中间层涂覆在抗氧化粘合涂层上。在其他应用中，可磨损系统应用于网格顶部。额外的好处应该是在高操作条件下减少刀片磨损。

7. 发明申请

US20070082131A1 Optimized high purity coating for high temperature thermal cycling applications 审中-公开
标题翻译：用于高温热循环应用的优化的高纯度涂层
公开(公告)号：US20070082131A1
公开(公告)日：2007-04-12
申请号：US11520042
申请日：2006-09-13
申请人： Jacobus Doesburg , Liangde Xie , Richard Schmid , Matthew Gold
发明人： Jacobus Doesburg , Liangde Xie , Richard Schmid , Matthew Gold
IPC分类号： B05D1/36
CPC分类号： C04B35/486 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3246 , C04B2235/72 , C23C4/11 , C23C14/083 , C23C30/00 , F01D5/288 , Y02T50/67 , Y02T50/672 , Y02T50/6765 , Y10T428/12611 , Y10T428/12618 , Y10T428/12667 , Y10T428/24 , Y10T428/24471 , Y10T428/24997 , Y10T428/25 , Y10T428/252 , Y10T428/26 , Y10T428/2982
摘要： The invention is directed to a blended material and method for obtaining thermal barriers for high temperature cycling applications that have both high sintering resistance to achieve a high service lifetime and low thermal conductivity to achieve high operating temperatures. These materials are additionally suited for use in high temperature abradable (rub seal) coatings. The invention provides desired coating structures so that the changes in the coating microstructure over the in-service lifetime are either limited or beneficial.
摘要翻译：本发明涉及用于获得具有高耐烧结性以实现高使用寿命和低热导率以实现高工作温度的高温循环应用的热障的共混材料和方法。这些材料还适用于高温耐磨（摩擦密封）涂层。本发明提供所需的涂层结构，使得在使用寿命内的涂层微观结构的变化是有限的或有益的。

8. 发明申请

US20120177836A1 High-purity fused and crushed zirconia alloy powder and method of producing same 有权
标题翻译：高纯度熔融和粉碎的氧化锆合金粉末及其制备方法
公开(公告)号：US20120177836A1
公开(公告)日：2012-07-12
申请号：US11790430
申请日：2007-04-25
申请人： Jacobus C. Doesburg , Mitchell R. Dorfman , Liangde Xie
发明人： Jacobus C. Doesburg , Mitchell R. Dorfman , Liangde Xie
IPC分类号： C23C4/10 , B02C19/00 , C04B35/626 , C04B35/48
CPC分类号： C04B35/482 , C04B35/486 , C04B35/62665 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3246 , C04B2235/72 , C09D1/00 , C23C4/11 , C23C14/083 , C23C30/00 , F01D5/288 , Y10T428/24273 , Y10T428/24331 , Y10T428/24471
摘要： The present invention provides a high-purity fused and crushed stabilized zirconia powder. The powder—with or without further processing, such as plasma spheroidization—is used in thermal spray applications of thermal barrier coatings (TBCs) and high-temperature abradables. The resulting coatings have a significantly improved high temperature sintering resistance, which will enhance the durability and thermal insulation effect of the coating.
摘要翻译：本发明提供了一种高纯度熔融和破碎稳定的氧化锆粉末。具有或不进行进一步加工的粉末（例如等离子体球化）用于热障涂层（TBC）和高温耐磨材料的热喷涂应用中。所得涂层具有显着改善的耐高温烧结性，这将提高涂层的耐久性和隔热效果。

9. 发明授权

US07723249B2 Ceramic material for high temperature service 有权
标题翻译：陶瓷材料用于高温服务
公开(公告)号：US07723249B2
公开(公告)日：2010-05-25
申请号：US11520043
申请日：2006-09-13
申请人： Jacobus C. Doesburg , Liangde Xie , Mitchell Dorfman
发明人： Jacobus C. Doesburg , Liangde Xie , Mitchell Dorfman
IPC分类号： C04B35/486 , C04B35/488 , B32B18/00
CPC分类号： C04B35/486 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3246 , C04B2235/72 , C23C4/11 , C23C14/083 , C23C30/00 , F01D5/288 , Y02T50/67 , Y02T50/672 , Y10T428/12611 , Y10T428/12618 , Y10T428/12667 , Y10T428/24 , Y10T428/24471 , Y10T428/24997 , Y10T428/25 , Y10T428/252 , Y10T428/26 , Y10T428/2982
摘要： The invention is directed to a ceramic material for use in thermal barriers for high temperature cycling applications and high temperature abradable coatings. The material is an alloy formed predominantly from ultra-pure zirconia (ZrO2) and/or hafnia (HfO2) that has uncharacteristically high sintering resistance to achieve a high service lifetime and low thermal conductivity to achieve high operating temperatures. In the material, oxide impurities such as soda (Na2O), silica (SiO2), alumina (Al2O3), titania (TiO2), hematite (Fe2O3), calcia (CaO), and magnesia (MgO) make up no more than 0.15 weight percent. The invention provides materials to produce a coating structure so that the changes in the coating microstructure over the in-service lifetime are either limited or beneficial.
摘要翻译：本发明涉及一种用于高温循环应用的热障层和高温耐磨涂层的陶瓷材料。该材料是主要由超纯氧化锆（ZrO2）和/或铪（HfO2）形成的合金，其具有非常高的耐烧结性，以实现高使用寿命和低热导率以实现高工作温度。在该材料中，诸如苏打（Na 2 O），二氧化硅（SiO 2），氧化铝（Al 2 O 3），二氧化钛（TiO 2），赤铁矿（Fe 2 O 3），氧化钙（CaO）和氧化镁（MgO）的氧化物杂质构成不超过0.15重量百分。本发明提供了用于生产涂层结构的材料，使得在使用寿命内的涂层微结构的变化是有限的或有益的。

10. 发明授权

US08603930B2 High-purity fused and crushed zirconia alloy powder and method of producing same 有权
标题翻译：高纯度熔融和粉碎的氧化锆合金粉末及其制备方法
公开(公告)号：US08603930B2
公开(公告)日：2013-12-10
申请号：US11790430
申请日：2007-04-25
申请人： Jacobus C. Doesburg , Mitchell R. Dorfman , Liangde Xie
发明人： Jacobus C. Doesburg , Mitchell R. Dorfman , Liangde Xie
IPC分类号： C04B35/48 , B02C19/00 , C23C4/10
CPC分类号： C04B35/482 , C04B35/486 , C04B35/62665 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3246 , C04B2235/72 , C09D1/00 , C23C4/11 , C23C14/083 , C23C30/00 , F01D5/288 , Y10T428/24273 , Y10T428/24331 , Y10T428/24471
摘要： The present invention provides a high-purity fused and crushed stabilized zirconia powder. The powder—with or without further processing, such as plasma spheroidization—is used in thermal spray applications of thermal barrier coatings (TBCs) and high-temperature abradables. The resulting coatings have a significantly improved high temperature sintering resistance, which will enhance the durability and thermal insulation effect of the coating.
摘要翻译：本发明提供了一种高纯度熔融和破碎稳定的氧化锆粉末。具有或不进行进一步加工的粉末（例如等离子体球化）用于热障涂层（TBC）和高温耐磨材料的热喷涂应用中。所得涂层具有显着改善的耐高温烧结性，这将提高涂层的耐久性和隔热效果。

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