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1. 发明授权

US06591841B1 Method of providing flavorful and aromatic tobacco suspension 失效
标题翻译：提供香味和芳香的烟草悬浮液的方法
公开(公告)号：US06591841B1
公开(公告)日：2003-07-15
申请号：US09993755
申请日：2001-11-14
申请人： Jackie Lee White , William Monroe Coleman, III , Thomas Albert Perfetti
发明人： Jackie Lee White , William Monroe Coleman, III , Thomas Albert Perfetti
IPC分类号： A24B310
CPC分类号： A24B15/18
摘要： Processes for producing flavorful and aromatic compounds from tobacco material are provided. The processes involve providing a tobacco suspension comprising finely ground tobacco material, and subjecting the tobacco suspension to heat treatment in an enclosed, pressure controlled, and generally inert environment at a temperature of at least 140° C.
摘要翻译：提供了从烟草材料生产香味和芳香族化合物的方法。该方法包括提供烟草悬浮液，其包括精细研磨的烟草材料，并在烟草悬浮液中在封闭的，压力控制的和通常在惰性的环境中在至少140℃的温度下进行热处理。

2. 发明授权

US06298858B1 Tobacco flavoring components of enhanced aromatic content and method of providing same 有权
标题翻译：烟草调味成分增强芳香含量及其提供方法
公开(公告)号：US06298858B1
公开(公告)日：2001-10-09
申请号：US09195753
申请日：1998-11-18
申请人： William Monroe Coleman, III , Thomas Albert Perfetti , Ronald Lewis Parks , Michael Francis Dube , Luis Mayan Dominguez
发明人： William Monroe Coleman, III , Thomas Albert Perfetti , Ronald Lewis Parks , Michael Francis Dube , Luis Mayan Dominguez
IPC分类号： A24B1518
CPC分类号： A24B15/306 , A24B3/08 , A24B3/12 , A24B3/18
摘要： Improved flavorful and aromatic tobacco materials and a method for producing flavorful and aromatic components from all natural tobacco materials are provided. A first tobacco material is contacted with a second tobacco material to form a tobacco blend. The first tobacco material has a higher content of nitrogen source and a lower content of sugar source than the second tobacco material. The moisture content in the first and second materials of the tobacco blend is increased to at least about 20%. The tobacco blend having an increased moisture content is then subjected to heat treatment in a substantially atmospheric environment for a time and under conditions sufficient to generate flavorful and aromatic substances in said first and second tobacco materials.
摘要翻译：本发明提供了改良的芳香和芳香烟草材料以及从所有天然烟草材料生产香味和芳香成分的方法。第一烟草材料与第二烟草材料接触以形成烟草混合物。第一种烟草材料具有比第二种烟草材料更高的氮源含量和更低的糖源含量。烟草混合物的第一和第二材料中的水分含量增加至至少约20％。然后将具有增加的水分含量的烟草混合物在基本上大气环境中进行一段时间和足以在所述第一和第二烟草材料中产生香味和芳香物质的条件下的热处理。

3. 发明授权

US07293564B2 Method for chemically modifying tobacco during curing 有权
标题翻译：固化期间化学改性烟草的方法
公开(公告)号：US07293564B2
公开(公告)日：2007-11-13
申请号：US10459123
申请日：2003-06-11
申请人： Thomas Albert Perfetti , Watson Minyard Dufour , Stephen Keith Cole , William Monroe Coleman, III , Marvin Glenn Riddick , Wennuan Liu , Paul Andrew Brinkley
发明人： Thomas Albert Perfetti , Watson Minyard Dufour , Stephen Keith Cole , William Monroe Coleman, III , Marvin Glenn Riddick , Wennuan Liu , Paul Andrew Brinkley
IPC分类号： A24B3/18
CPC分类号： A24B15/28 , A24B3/12
摘要： A method for chemically modifying a tobacco material during a curing process involves treating the tobacco material in a curing enclosure at a temperature and for a time sufficient to produce cured tobacco. The method also involves contacting the tobacco material with a chemical reagent before and/or during the time period that the tobacco material is cured so that the chemical reagent can interact with the tobacco material, thus resulting in further change in the chemical nature of the cured tobacco material. An exemplary chemical reagent is an ammonia source, which can be applied to a tobacco material in a variety of ways, including by spraying an aqueous ammonia source onto the tobacco or by introducing gaseous ammonia into the curing enclosure during the curing process.
摘要翻译：在固化过程中化学改性烟草材料的方法包括在足以产生硫化烟草的温度和时间内处理固化外壳中的烟草材料。该方法还包括在烟草材料固化之前和/或期间使烟草材料与化学试剂接触，使得化学试剂可与烟草材料相互作用，从而导致固化的化学性质的进一步变化烟草材料。示例性的化学试剂是氨源，其可以以各种方式施用于烟草材料，包括通过将氨水源喷射到烟草上或者在固化过程中将气态氨引入固化外壳中。

4. 发明申请

US20110174323A1 TOBACCO-DERIVED COMPONENTS AND MATERIALS 有权
标题翻译：烟草衍生的成分和材料
公开(公告)号：US20110174323A1
公开(公告)日：2011-07-21
申请号：US12688294
申请日：2010-01-15
申请人： William Monroe Coleman, III , Michael Francis Dube , Darlene Madeline Lawson
发明人： William Monroe Coleman, III , Michael Francis Dube , Darlene Madeline Lawson
IPC分类号： A24B15/26 , A24B15/24 , A24B15/18 , A24B15/20
CPC分类号： A24B15/302 , A24B15/24 , A24B15/307
摘要： The invention provides a tobacco composition for use in a smoking article or a smokeless tobacco composition that includes an additive derived from a flower of the Nicotiana species. The additive can be a flower of the Nicotiana species or a portion thereof in particulate form or in the form of flower isolate derived from a flower of the Nicotiana species. In certain embodiments, the flower isolate is in the form of an extract from a flower of the Nicotiana species or in the form of a chemically transformed flower isolate, the chemical transformation being selected from acid/base reaction, hydrolysis, thermal treatment, and enzymatic treatment. The invention also provides smoking articles and smokeless tobacco compositions that include the flower additives described herein, and methods for preparing an additive derived from a flower of the Nicotiana species for addition to a tobacco composition.
摘要翻译：本发明提供一种用于吸烟制品或无烟烟草组合物的烟草组合物，其包含衍生自烟草属种的花的添加剂。添加剂可以是烟草属物种的花或其一部分为颗粒形式，或者为来自烟草属种的花的分离物的形式。在某些实施方案中，花分离物是烟草属物种的提取物的形式或化学转化的花分离物的形式，化学转化选自酸/碱反应，水解，热处理和酶治疗。本发明还提供了吸烟制品和无烟烟草组合物，其包括本文所述的花添加剂，以及用于制备从烟草种类的花中衍生的添加剂用于添加到烟草组合物中的添加剂的方法。

5. 发明申请

US20130014771A1 TOBACCO-DERIVED COMPONENTS AND MATERIALS 审中-公开
标题翻译：烟草衍生的成分和材料
公开(公告)号：US20130014771A1
公开(公告)日：2013-01-17
申请号：US13547760
申请日：2012-07-12
申请人： William Monroe Coleman, III , Michael Francis Dube , Darlene Madeline Lawson
发明人： William Monroe Coleman, III , Michael Francis Dube , Darlene Madeline Lawson
IPC分类号： A24B15/24 , A24B15/26 , A24B13/00
CPC分类号： A24B15/303 , A24B15/20 , A24B15/24 , A24B15/26 , A24B15/30
摘要： The invention provides a tobacco composition for use in a smoking article or a smokeless tobacco composition that includes an additive derived from a flower of the Nicotiana species. The additive can be a flower isolate derived from a flower of the Nicotiana species. In certain embodiments, the flower isolate is in the form of an extract from a flower of the Nicotiana species or in the form of a chemically transformed flower isolate, the chemical transformation being selected from acid/base reaction, hydrolysis, thermal treatment, and enzymatic treatment, the chemical transformation releasing at least a portion of a glycosidically bound compound in the flower of the Nicotiana species. The invention also provides smoking articles and smokeless tobacco compositions that include the flower additives described herein, and methods for preparing an additive derived from a flower of the Nicotiana species for addition to a tobacco composition.
摘要翻译：本发明提供一种用于吸烟制品或无烟烟草组合物的烟草组合物，其包含衍生自烟草属种的花的添加剂。添加剂可以是衍生自烟草属的花的花分离物。在某些实施方案中，花分离物是烟草属物种的提取物的形式或化学转化的花分离物的形式，所述化学转化选自酸/碱反应，水解，热处理和酶处理，化学转化释放烟草属植物花中至少一部分糖苷结合化合物。本发明还提供了吸烟制品和无烟烟草组合物，其包括本文所述的花添加剂，以及用于制备从烟草种类的花中衍生的添加剂用于添加到烟草组合物中的添加剂的方法。

6. 发明申请

US20120192882A1 POLYMERIC MATERIALS DERIVED FROM TOBACCO 有权
标题翻译：从烟草衍生的聚合材料
公开(公告)号：US20120192882A1
公开(公告)日：2012-08-02
申请号：US13015912
申请日：2011-01-28
申请人： Michael Francis Dube , William Monroe Coleman, III
发明人： Michael Francis Dube , William Monroe Coleman, III
IPC分类号： A24D3/08 , A24F47/00 , A24D1/02 , C08F2/48 , C08F136/04 , C08F2/60 , C08F4/48 , A24B15/10 , C08F2/46
CPC分类号： C08L9/00 , A24B15/24 , A24B15/302 , A24D3/06 , A24D3/08 , C08F36/045
摘要： The invention provides a polymer prepared from a substituted 1,3-butadiene (such as neophytadiene) derived from a plant of the Nicotiana species. The invention also provides smoking articles and smokeless tobacco compositions that include the polymers described herein. Further, the invention provides a method of polymerizing a substituted 1,3-butadiene derived from a plant of the Nicotiana species, the method including reacting a substituted 1,3-butadiene derived from a plant of the Nicotiana species with one or more reagents selected from the group consisting of an anionic initiator, a radical initiator, and a Ziegler-Natta catalyst.
摘要翻译：本发明提供由衍生自烟草属植物的取代的1,3-丁二烯（如新戊二烯）制备的聚合物。本发明还提供了包含本文所述的聚合物的吸烟制品和无烟烟草组合物。此外，本发明提供了一种聚合衍生自烟草属植物的取代1,3-丁二烯的方法，该方法包括将衍生自烟草属植物的取代1,3-丁二烯与选自一种或多种试剂由阴离子引发剂，自由基引发剂和齐格勒 - 纳塔催化剂组成。

7. 发明申请

US20110259353A1 Tobacco Seed-Derived Components and Materials 有权
标题翻译：烟草种子成分和材料
公开(公告)号：US20110259353A1
公开(公告)日：2011-10-27
申请号：US12764613
申请日：2010-04-21
申请人： William Monroe Coleman, III , Michael Francis Dube , Darlene Madeline Lawson
发明人： William Monroe Coleman, III , Michael Francis Dube , Darlene Madeline Lawson
IPC分类号： A24B15/00
CPC分类号： A24B15/307 , A24B15/24 , A24B15/302 , C12P7/22 , C12P7/6409 , C12P7/6427 , C12P7/6445 , C12P13/04
摘要： A tobacco composition for use in a smoking article or a smokeless tobacco composition is provided, the composition including a component derived from a seed of the Nicotiana species. The component can be a seed of the Nicotiana species or a portion thereof in particulate form or in the form of seed isolate derived from a seed of the Nicotiana species. In certain embodiments, the seed isolate is in the form of a chemically transformed seed isolate, the chemical transformation being selected from hydrogenation, acid/base reaction, hydrolysis, thermal treatment, and enzymatic treatment. The invention also provides smoking articles and smokeless tobacco compositions that include the seed components described herein, and methods for preparing a component derived from a seed of the Nicotiana species for addition to a tobacco composition.
摘要翻译：提供了用于吸烟制品或无烟烟草组合物的烟草组合物，该组合物包括衍生自烟草属种子的成分。该组分可以是烟草属物种的种子或其一部分为颗粒形式或以种子分离物的形式来自烟草种子的种子。在某些实施方案中，种子分离物是化学转化的种子分离物的形式，化学转化选自氢化，酸/碱反应，水解，热处理和酶处理。本发明还提供了包含本文所述的种子成分的吸烟制品和无烟烟草组合物，以及用于制备衍生自烟草种子的成分的成分的方法，用于添加到烟草组合物中。

8. 发明申请

US20100037903A1 Method for Preparing Flavorful and Aromatic Compounds 审中-公开
标题翻译：芳香和芳香化合物的制备方法
公开(公告)号：US20100037903A1
公开(公告)日：2010-02-18
申请号：US12191751
申请日：2008-08-14
申请人： William Monroe Coleman, III , Anthony Richard Gerardi
发明人： William Monroe Coleman, III , Anthony Richard Gerardi
IPC分类号： A24B15/38 , B01D3/40
CPC分类号： A24B15/38 , A24B15/306
摘要： The invention provides a method of preparing a purified, pyrazine-containing aqueous composition by mixing a reducing sugar, a base, and an amino acid in water to produce a mixture; heating the mixture for a time and under conditions conducive to Maillard reactions such that a flavorful and aromatic aqueous solution is formed, the aqueous solution comprising a plurality of pyrazines and a first 4-methylimidazole concentration; distilling the aqueous solution to produce an aqueous distillate comprising a plurality of pyrazines and having a second 4-methylimidazole concentration lower than the first 4-methylimidazole concentration; and collecting the aqueous distillate. The invention also includes flavorful and aromatic aqueous compositions formed by this inventive method, as well as tobacco products (e.g., smokable materials, smoking articles, and smokeless tobacco) incorporating the flavorful and aromatic composition.
摘要翻译：本发明提供了一种通过将还原糖，碱和氨基酸混合在水中混合制备含有吡嗪的含水组合物的方法，将混合物加热一段时间并在有利于美拉德反应的条件下，形成香味和芳香族水溶液，所述水溶液包含多个吡嗪和第一4-甲基咪唑浓度; 蒸馏该水溶液以产生包含多个吡嗪并且具有低于第一4-甲基咪唑浓度的第二4-甲基咪唑浓度的含水馏出物; 并收集含水馏出物。本发明还包括通过本发明方法形成的美味和芳香的含水组合物，以及掺入美味和芳香组合物的烟草制品（例如可吸烟材料，吸烟制品和无烟烟草）。

9. 发明授权

US06695924B1 Method of improving flavor in smoking article 有权
标题翻译：改善吸烟制品风味的方法
公开(公告)号：US06695924B1
公开(公告)日：2004-02-24
申请号：US09624820
申请日：2000-07-25
申请人： Michael Francis Dube , Luis Mayan Dominguez , Chi-Kuen Shu , Elwood Lee Williams, Jr. , Kenneth Wayne Smith , William Monroe Coleman, III
发明人： Michael Francis Dube , Luis Mayan Dominguez , Chi-Kuen Shu , Elwood Lee Williams, Jr. , Kenneth Wayne Smith , William Monroe Coleman, III
IPC分类号： A24B1500
CPC分类号： A24B15/306 , Y10S127/01
摘要： A method for improving the flavor and aroma characters of a smoking article is provided. A mixture consisting essentially of a reducing sugar and optionally a hydroxide of an alkali metal is subjected to heat treatment for a time and under conditions sufficient to produce a flavorful composition. The flavorful composition is then applied to tobacco leaves or cut filler made thereof, and smoking articles are prepared from the tobacco leaves or cut filler.
摘要翻译：提供了一种用于改善吸烟制品的风味和香气特征的方法。基本上由还原糖和任选的碱金属的氢氧化物组成的混合物在足以产生美味组合物的时间和条件下进行热处理。然后将有味的组合物施用于由其制成的烟叶或切割填料，并且从烟叶或切割填料制备吸烟制品。

10. 发明授权

US09402415B2 Tobacco seed-derived components and materials 有权
标题翻译：烟草种子衍生的成分和材料
公开(公告)号：US09402415B2
公开(公告)日：2016-08-02
申请号：US12764613
申请日：2010-04-21
申请人： William Monroe Coleman, III , Michael Francis Dube , Darlene Madeline Lawson
发明人： William Monroe Coleman, III , Michael Francis Dube , Darlene Madeline Lawson
IPC分类号： A24D1/00 , A24B15/30
CPC分类号： A24B15/307 , A24B15/24 , A24B15/302 , C12P7/22 , C12P7/6409 , C12P7/6427 , C12P7/6445 , C12P13/04
摘要： A tobacco composition for use in a smoking article or a smokeless tobacco composition is provided, the composition including a component derived from a seed of the Nicotiana species. The component can be a seed of the Nicotiana species or a portion thereof in particulate form or in the form of seed isolate derived from a seed of the Nicotiana species. In certain embodiments, the seed isolate is in the form of a chemically transformed seed isolate, the chemical transformation being selected from hydrogenation, acid/base reaction, hydrolysis, thermal treatment, and enzymatic treatment. The invention also provides smoking articles and smokeless tobacco compositions that include the seed components described herein, and methods for preparing a component derived from a seed of the Nicotiana species for addition to a tobacco composition.
摘要翻译：提供了用于吸烟制品或无烟烟草组合物的烟草组合物，该组合物包括衍生自烟草属种子的成分。该组分可以是烟草属物种的种子或其一部分为颗粒形式或以种子分离物的形式来自烟草种子的种子。在某些实施方案中，种子分离物是化学转化的种子分离物的形式，化学转化选自氢化，酸/碱反应，水解，热处理和酶处理。本发明还提供了包含本文所述的种子成分的吸烟制品和无烟烟草组合物，以及用于制备衍生自烟草种子的成分的成分的方法，用于添加到烟草组合物中。

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