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1. 发明申请

US20120077983A1 LEAD-FREE PRIMARY EXPLOSIVE COMPOSITION 有权
标题翻译：无铅主要爆炸组合物
公开(公告)号：US20120077983A1
公开(公告)日：2012-03-29
申请号：US13282547
申请日：2011-10-27
申请人： JOHN W. FRONABARGER , MICHAEL D. WILLIAMS , WILLIAM B. SANBORN
发明人： JOHN W. FRONABARGER , MICHAEL D. WILLIAMS , WILLIAM B. SANBORN
IPC分类号： C07F1/08
CPC分类号： C06B49/00 , C07D257/06
摘要： Embodiments of the present subject matter provide a compound and material that may be used as a lead-free primary explosive. An embodiment of the present subject matter provides the compound copper(I) nitrotetrazolate. Certain embodiments of the present subject matter provide methods for preparing lead-free primary explosives. The method includes: providing cuprous salt; providing water; providing 5-nitrotetrazolate salt; combining the cuprous salt, water and 5-nitrotetrazolate salt to form a mixture; and heating the mixture. The method may also include providing cuprous chloride and providing sodium 5-nitrotetrazolate. Certain embodiments of the present subject matter also provide methods for preparing copper(I) nitrotetrazolate. The method includes: providing cuprous salt; providing water; providing 5-nitrotetrazolate salt; combining the cuprous salt, water and 5-nitrotetrazolate salt to form a mixture; and heating the mixture. The method may also include providing cuprous chloride and providing sodium 5-nitrotetrazolate.
摘要翻译：本主题的实施方案提供可用作无铅初级炸药的化合物和材料。本主题的一个实施方案提供了复合铜（I）硝基四氮烯酸盐。本主题的某些实施例提供了制备无铅初级炸药的方法。该方法包括：提供亚铜盐; 提供水; 提供5-硝基四氮唑盐; 结合亚铜盐，水和5-硝基四氮唑盐形成混合物; 并加热混合物。该方法还可以包括提供氯化亚铜和提供5-硝基四氮唑钠。本发明的某些实施方案还提供了制备硝基四氮烯酸铜（I）的方法。该方法包括：提供亚铜盐; 提供水; 提供5-硝基四氮唑盐; 结合亚铜盐，水和5-硝基四氮唑盐形成混合物; 并加热混合物。该方法还可以包括提供氯化亚铜和提供5-硝基四氮唑钠。

2. 发明申请

US20110108172A1 LEAD-FREE PRIMARY EXPLOSIVE COMPOSITION AND METHOD OF PREPARATION 有权
标题翻译：无铅主要爆炸组合物和制备方法
公开(公告)号：US20110108172A1
公开(公告)日：2011-05-12
申请号：US12900531
申请日：2010-10-08
申请人： JOHN W. FRONABARGER , Michael D. Williams , William B. Sanborn
发明人： JOHN W. FRONABARGER , Michael D. Williams , William B. Sanborn
IPC分类号： C06B21/00
CPC分类号： C06B49/00 , C07D257/06
摘要： Embodiments of the present subject matter provide a compound and material that may be used as a lead-free primary explosive. An embodiment of the present subject matter provides the compound copper(I) nitrotetrazolate. Certain embodiments of the present subject matter provide methods for preparing lead-free primary explosives. The method includes: providing cuprous salt; providing water; providing 5-nitrotetrazolate salt; combining the cuprous salt, water and 5-nitrotetrazolate salt to form a mixture; and heating the mixture. The method may also include providing cuprous chloride and providing sodium 5-nitrotetrazolate. Certain embodiments of the present subject matter also provide methods for preparing copper(I) nitrotetrazolate. The method includes: providing cuprous salt; providing water; providing 5-nitrotetrazolate salt; combining the cuprous salt, water and 5-nitrotetrazolate salt to form a mixture; and heating the mixture. The method may also include providing cuprous chloride and providing sodium 5-nitrotetrazolate.
摘要翻译：本主题的实施方案提供可用作无铅初级炸药的化合物和材料。本主题的一个实施方案提供了复合铜（I）硝基四氮烯酸盐。本主题的某些实施例提供了制备无铅初级炸药的方法。该方法包括：提供亚铜盐; 提供水; 提供5-硝基四氮唑盐; 结合亚铜盐，水和5-硝基四氮唑盐形成混合物; 并加热混合物。该方法还可以包括提供氯化亚铜和提供5-硝基四氮唑钠。本发明的某些实施方案还提供了制备硝基四氮烯酸铜（I）的方法。该方法包括：提供亚铜盐; 提供水; 提供5-硝基四氮唑盐; 结合亚铜盐，水和5-硝基四氮唑盐形成混合物; 并加热混合物。该方法还可以包括提供氯化亚铜和提供5-硝基四氮唑钠。

3. 发明申请

US20120215004A1 PREPARATION OF A LEAD-FREE PRIMARY EXPLOSIVE 有权
标题翻译：无铅一次爆炸的准备
公开(公告)号：US20120215004A1
公开(公告)日：2012-08-23
申请号：US13419455
申请日：2012-03-14
申请人： JOHN W. FRONABARGER , Michael D. Williams
发明人： JOHN W. FRONABARGER , Michael D. Williams
IPC分类号： C07D233/91
CPC分类号： C07D257/06 , C06B41/00 , C06C7/00 , C07F1/005
摘要： Described are compounds and materials that may be used as a lead-free primary explosive,such as copper(I) nitrotetrazolate. Copper(I) nitrotetrazolate may he prepared by a process comprising the steps of: combining cupric salt, water and 5-nitrotetrazolate salt to form a mixture, heating the mixture, adding a reducing agent and stirring with continued heating. The method may also include combining cupric chloride, sodium 5-nitrotetrazolate and sodium ascorbate.
摘要翻译：描述了可用作无铅初级炸药的化合物和材料，例如硝基四氮烯铜（I）。铜（I）硝基四氮酸盐可以通过包括以下步骤的方法制备：将铜盐，水和5-硝基四唑盐结合形成混合物，加热混合物，加入还原剂并继续加热搅拌。该方法还可以包括组合氯化铜，5-硝基四氮唑钠和抗坏血酸钠。

4. 发明申请

US20120145290A1 ALTERNATIVE TO TETRAZENE 有权
标题翻译：替代四氯化碳
公开(公告)号：US20120145290A1
公开(公告)日：2012-06-14
申请号：US13091708
申请日：2011-04-21
申请人： JOHN W. FRONABARGER , MICHAEL D. WILLIAMS
发明人： JOHN W. FRONABARGER , MICHAEL D. WILLIAMS
IPC分类号： C07D257/04 , C06B25/34
CPC分类号： C07D257/06 , C06B43/00 , C06C7/00
摘要： Embodiments of materials suitable for use as a replacement for Tetrazene and methods of preparing such materials are described. In one embodiment, the material comprises MTX-1, as well as simple salts or complexes derived therefrom. The methods of preparing such materials include combining Tetrazene and an acid to form a suspension, where the acid is nitric acid, sulfuric acid, perchloric acid, or hydrochloric acid. A nitrite salt may be added to the suspension, where the nitrite salt is sodium nitrite, lithium nitrite, potassium nitrite, an aqueous solution of sodium nitrite, an aqueous solution of lithium nitrite, or an aqueous solution of potassium nitrite. In some embodiments, the suspension is stirred until the suspension has a white appearance.
摘要翻译：描述适用于替代四氮烯的材料的实施方案及其制备方法。在一个实施方案中，该材料包含MTX-1，以及衍生自其的简单盐或复合物。制备这种材料的方法包括组合四嗪和酸形成悬浮液，其中酸是硝酸，硫酸，高氯酸或盐酸。亚硝酸盐可以加入到悬浮液中，其中亚硝酸盐是亚硝酸钠，亚硝酸锂，亚硝酸钾，亚硝酸钠水溶液，亚硝酸锂水溶液或亚硝酸钾水溶液。在一些实施方案中，搅拌悬浮液直到悬浮液具有白色外观。

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