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1. 发明申请

US20100285326A1 ORE REDUCTION PROCESS AND TITANIUM OXIDE AND IRON METALLIZATION PRODUCT 审中-公开
标题翻译： ORE还原工艺和氧化钛和铁金属化产品
公开(公告)号：US20100285326A1
公开(公告)日：2010-11-11
申请号：US12838899
申请日：2010-07-19
申请人： JOHN JAMES BARNES , Stephen Erwin Lyke , Dat Nguyen , Mitsutaka Hino , Akira Uragami , Isao Kobayashi , Thomas Peter Battle , Joseph M. Shekiro, JR.
发明人： JOHN JAMES BARNES , Stephen Erwin Lyke , Dat Nguyen , Mitsutaka Hino , Akira Uragami , Isao Kobayashi , Thomas Peter Battle , Joseph M. Shekiro, JR.
IPC分类号： B32B15/04 , B22F9/20
CPC分类号： C21B13/105 , C21B3/04 , C21B13/0046 , C21B13/006 , Y02W30/542 , Y10T428/12056
摘要： The disclosure is directed to a process for producing separable iron and titanium oxides from an ore containing titanium oxide and ferric oxide, comprising: (a) forming agglomerates comprising carbon-based materials and the ore, the quantity of carbon of the agglomerates being sufficient for, at an elevated temperature, reducing ferric oxide to ferrous oxide and forming a ferrous oxide-rich molten slag, (b) introducing the agglomerates onto a carbon bed of a moving hearth furnace; (c) heating the agglomerates in the moving hearth furnace to a temperature sufficient for reducing and melting the agglomerates to produce a ferrous oxide-rich molten slag; (d) metallizing the ferrous oxide of the molten slag by reaction of the ferrous oxide and the carbon of the carbon bed at a furnace temperature sufficient for maintaining the slag in a molten state; and (e) solidifying the slag after metallization of the ferrous oxide to form a matrix of titanium oxide-rich slag having a plurality of metallic iron granules distributed there through; and (f) separating the metallic iron granules from the slag, the slag comprising greater than 85% titanium dioxide based on the entire weight of the matrix after separation of the metallic iron. The disclosure is also directed to a metallization product of a ferrous oxide-rich molten slag.
摘要翻译：本发明涉及从含有氧化钛和氧化铁的矿石中制备可分离的铁和钛氧化物的方法，其包括：（a）形成包含碳基材料和矿石的附聚物，附聚物的碳量足以在升高的温度下，将氧化亚铁还原成氧化亚铁，形成富含氧化亚铁的熔渣，（b）将附聚物引入移动的炉底炉的碳床上; （c）将移动的炉底炉中的附聚物加热至足以减少和熔化附聚物以产生富含氧化亚铁的熔渣的温度; （d）在足以使炉渣处于熔融状态的炉温下，通过氧化亚氮和碳床的碳的反应使熔渣的氧化亚铁金属化; 和（e）在氧化亚铁金属化之后固化炉渣，以形成富含氧化钛的炉渣的基体，其具有分布在其上的多个金属铁颗粒; 和（f）从矿渣中分离金属铁颗粒，在分离金属铁之后，炉渣基于基体的整个重量，包含大于85％的二氧化钛。本公开还涉及富含氧化亚铁的熔渣的金属化产物。

2. 发明授权

US07780756B2 Ore reduction process and titanium oxide and iron metallization product 有权
标题翻译：矿石还原工艺和氧化钛和铁金属化产品
公开(公告)号：US07780756B2
公开(公告)日：2010-08-24
申请号：US12430261
申请日：2009-04-27
申请人： John James Barnes , Stephen Erwin Lyke , Dat Nguyen , Akira Uragami , Isao Kobayashi , Mitsutaka Hino , Thomas Peter Battle , Joseph M. Shekiro, Jr.
发明人： John James Barnes , Stephen Erwin Lyke , Dat Nguyen , Akira Uragami , Isao Kobayashi , Mitsutaka Hino , Thomas Peter Battle , Joseph M. Shekiro, Jr.
IPC分类号： C22B1/14 , C22B1/00 , C22B1/16 , C21B3/04 , C21B13/10
CPC分类号： C21B13/105 , C21B3/04 , C21B13/0046 , C21B13/006 , Y02W30/542 , Y10T428/12056
摘要： The disclosure is directed to a process for producing separable iron and titanium oxides from an ore containing titanium oxide and ferric oxide, comprising: (a) forming agglomerates comprising carbon-based materials and the ore, the quantity of carbon of the agglomerates being sufficient for, at an elevated temperature, reducing ferric oxide to ferrous oxide and forming a ferrous oxide-rich molten slag, (b) introducing the agglomerates onto a carbon bed of a moving hearth furnace; (c) heating the agglomerates in the moving hearth furnace to a temperature sufficient for reducing and melting the agglomerates to produce a ferrous oxide-rich molten slag; (d) metallizing the ferrous oxide of the molten slag by reaction of the ferrous oxide and the carbon of the carbon bed at a furnace temperature sufficient for maintaining the slag in a molten state; and (e) solidifying the slag after metallization of the ferrous oxide to form a matrix of titanium oxide-rich slag having a plurality of metallic iron granules distributed there through; and (f) separating the metallic iron granules from the slag, the slag comprising greater than 85% titanium dioxide based on the entire weight of the matrix after separation of the metallic iron. The disclosure is also directed to a metallization product of a ferrous oxide-rich molten slag.
摘要翻译：本发明涉及从含有氧化钛和氧化铁的矿石中制备可分离的铁和钛氧化物的方法，其包括：（a）形成包含碳基材料和矿石的附聚物，附聚物的碳量足以在升高的温度下，将氧化亚铁还原成氧化亚铁，形成富含氧化亚铁的熔渣，（b）将附聚物引入移动的炉底炉的碳床上; （c）将移动的炉底炉中的附聚物加热至足以减少和熔化附聚物以产生富含氧化亚铁的熔渣的温度; （d）在足以使炉渣处于熔融状态的炉温下，通过氧化亚氮和碳床的碳的反应使熔渣的氧化亚铁金属化; 和（e）在氧化亚铁金属化之后固化炉渣，以形成富含氧化钛的炉渣的基体，其具有分布在其上的多个金属铁颗粒; 和（f）从矿渣中分离金属铁颗粒，在分离金属铁之后，炉渣基于基体的整个重量，包含大于85％的二氧化钛。本公开还涉及富含氧化亚铁的熔渣的金属化产物。

3. 发明申请

US20090217784A1 ORE REDUCTION PROCESS AND TITANIUM OXIDE AND IRON METALLIZATION PRODUCT 有权
标题翻译： ORE还原工艺和氧化钛和铁金属化产品
公开(公告)号：US20090217784A1
公开(公告)日：2009-09-03
申请号：US12430261
申请日：2009-04-27
申请人： John James Barnes , Stephen Erwin Lyke , Dat Nguyen , Mitsutaka Hino , Akira Uragami , Isao Kobayashi , Thomas Peter Battle , Joseph M. Shekiro, JR.
发明人： John James Barnes , Stephen Erwin Lyke , Dat Nguyen , Mitsutaka Hino , Akira Uragami , Isao Kobayashi , Thomas Peter Battle , Joseph M. Shekiro, JR.
IPC分类号： C22B1/14
CPC分类号： C21B13/105 , C21B3/04 , C21B13/0046 , C21B13/006 , Y02W30/542 , Y10T428/12056
摘要： The disclosure is directed to a process for producing separable iron and titanium oxides from an ore containing titanium oxide and ferric oxide, comprising: (a) forming agglomerates comprising carbon-based materials and the ore, the quantity of carbon of the agglomerates being sufficient for, at an elevated temperature, reducing ferric oxide to ferrous oxide and forming a ferrous oxide-rich molten slag, (b) introducing the agglomerates onto a carbon bed of a moving hearth furnace; (c) heating the agglomerates in the moving hearth furnace to a temperature sufficient for reducing and melting the agglomerates to produce a ferrous oxide-rich molten slag; (d) metallizing the ferrous oxide of the molten slag by reaction of the ferrous oxide and the carbon of the carbon bed at a furnace temperature sufficient for maintaining the slag in a molten state; and (e) solidifying the slag after metallization of the ferrous oxide to form a matrix of titanium oxide-rich slag having a plurality of metallic iron granules distributed there through; and (f) separating the metallic iron granules from the slag, the slag comprising greater than 85% titanium dioxide based on the entire weight of the matrix after separation of the metallic iron. The disclosure is also directed to a metallization product of a ferrous oxide-rich molten slag.
摘要翻译：本发明涉及从含有氧化钛和氧化铁的矿石中制备可分离的铁和钛氧化物的方法，其包括：（a）形成包含碳基材料和矿石的附聚物，附聚物的碳量足以在升高的温度下，将氧化亚铁还原成氧化亚铁，形成富含氧化亚铁的熔渣，（b）将附聚物引入移动的炉底炉的碳床上; （c）将移动的炉底炉中的附聚物加热至足以减少和熔化附聚物以产生富含氧化亚铁的熔渣的温度; （d）在足以使炉渣处于熔融状态的炉温下，通过氧化亚氮和碳床的碳的反应使熔渣的氧化亚铁金属化; 和（e）在氧化亚铁金属化之后固化炉渣，以形成富含氧化钛的炉渣的基体，其具有分布在其上的多个金属铁颗粒; 和（f）从矿渣中分离金属铁颗粒，在分离金属铁之后，炉渣基于基体的整个重量，含有大于85％的二氧化钛。本公开还涉及富含氧化亚铁的熔渣的金属化产物。

4. 发明申请

US20070068344A1 Ore reduction process and titanium oxide and iron metallization product 审中-公开
标题翻译：矿石还原工艺和氧化钛和铁金属化产品
公开(公告)号：US20070068344A1
公开(公告)日：2007-03-29
申请号：US11512993
申请日：2006-08-30
申请人： John Barnes , Stephen Lyke , Dat Nguyen , Akira Uragami , Isao Kobayashi , Mitsutaka Hino
发明人： John Barnes , Stephen Lyke , Dat Nguyen , Akira Uragami , Isao Kobayashi , Mitsutaka Hino
IPC分类号： C21B3/04 , C21B11/08
CPC分类号： C21B13/105 , C21B3/04 , C21B13/0046 , C21B13/006 , Y02W30/542 , Y10T428/12056
摘要： The disclosure is directed to a process for producing separable iron and titanium oxides from an ore containing titanium oxide and ferric oxide, comprising: (a) forming agglomerates comprising carbon-based materials and the ore, the quantity of carbon of the agglomerates being sufficient for, at an elevated temperature, reducing ferric oxide to ferrous oxide and forming a ferrous oxide-rich molten slag, (b) introducing the agglomerates onto a carbon bed of a moving hearth furnace; (c) heating the agglomerates in the moving hearth furnace to a temperature sufficient for reducing and melting the agglomerates to produce a ferrous oxide-rich molten slag; (d) metallizing the ferrous oxide of the molten slag by reaction of the ferrous oxide and the carbon of the carbon bed at a furnace temperature sufficient for maintaining the slag in a molten state; and (e) solidifying the slag after metallization of the ferrous oxide to form a matrix of titanium oxide-rich slag having a plurality of metallic iron granules distributed there through; and (f) separating the metallic iron granules from the slag, the slag comprising greater than 85% titanium dioxide based on the entire weight of the matrix after separation of the metallic iron. The disclosure is also directed to a metallization product of a ferrous oxide-rich molten slag.
摘要翻译：本发明涉及从含有氧化钛和氧化铁的矿石中制备可分离的铁和钛氧化物的方法，其包括：（a）形成包含碳基材料和矿石的附聚物，附聚物的碳量足以在升高的温度下，将氧化亚铁还原为氧化亚铁，形成富含氧化亚铁的熔渣，（b）将附聚物引入移动的炉底炉的碳床上; （c）将移动的炉底炉中的附聚物加热至足以减少和熔化附聚物以产生富含氧化亚铁的熔渣的温度; （d）在足以使炉渣处于熔融状态的炉温下，通过氧化亚氮和碳床的碳的反应使熔渣的氧化亚铁金属化; 和（e）在氧化亚铁金属化之后固化炉渣，以形成富含氧化钛的炉渣的基体，其具有分布在其上的多个金属铁颗粒; 和（f）从矿渣中分离金属铁颗粒，在分离金属铁之后，炉渣基于基体的整个重量，包含大于85％的二氧化钛。本公开还涉及富含氧化亚铁的熔渣的金属化产物。

5. 发明申请

US20120006449A1 METHOD FOR PRODUCING METALLIC IRON 审中-公开
标题翻译：生产金属铁的方法
公开(公告)号：US20120006449A1
公开(公告)日：2012-01-12
申请号：US13258250
申请日：2010-04-06
申请人： Mitsutaka Hino , Isao Kobayashi , Akira Uragami , Takuya Negami
发明人： Mitsutaka Hino , Isao Kobayashi , Akira Uragami , Takuya Negami
IPC分类号： H01F1/047
CPC分类号： C21B13/105 , C21B13/0006 , C21B13/0046 , C21B13/0066 , C21B13/0073 , Y02P10/136
摘要： The present invention provides a method for producing metallic iron, which is operable at low temperature. The present invention relates to a method for producing a metallic iron, which comprises heating and reducing a raw material mixture containing a carbonaceous reducing agent and an iron oxide-containing material to produce the metallic iron, wherein the carbonaceous reducing agent has a volatile content of 20 to 60 mass %, a gas derived from the carbonaceous reducing agent is a CO—CO2—H2 gas, and the method comprises forming solid Fe3C by heating the raw material mixture in an atmosphere containing the CO—CO2—H2 gas, melting the Fe3C, and carburizing a reduced iron through the molten Fe3C.
摘要翻译：本发明提供一种在低温下可操作的金属铁的制造方法。金属铁的制造方法技术领域本发明涉及一种金属铁的制造方法，其特征在于，将含有碳质还原剂的原料混合物和含铁氧化物的原料混合，制成金属铁，其中，所述碳质还原剂的挥发成分为 20〜60质量％，来自碳质还原剂的气体为CO-CO 2·H 2气体，该方法包括通过在含有CO-CO 2 -H 2气体的气氛中加热原料混合物来形成固体Fe 3 C， Fe3C，并通过熔融的Fe3C渗碳还原铁。

6. 发明申请

US20090282950A1 PROCESS FOR PRODUCING METALLIC IRON 审中-公开
标题翻译：生产金属铁的工艺
公开(公告)号：US20090282950A1
公开(公告)日：2009-11-19
申请号：US12094607
申请日：2006-11-30
申请人： Akira Uragami , Isao Kobayashi , Mitsutaka Hino
发明人： Akira Uragami , Isao Kobayashi , Mitsutaka Hino
IPC分类号： C21B15/00
CPC分类号： C21B13/0046 , C21B13/0066 , C21B13/008 , C21B13/105 , Y02P10/136
摘要： A method for manufacturing metallic iron from a raw material mixture containing a carbonaceous reducing agent and an iron oxide-containing material, has a step of determining a target temperature of initial molten slag formation corresponding to a predetermined target carbon concentration in the metallic iron, the initial molten slag containing a gangue component, an unreduced iron oxide, and an ash component of the carbonaceous reducing agent, and being first produced in the raw material mixture by heating thereof; a step of preparing the raw material mixture producing a composition of the initial molten slag corresponding to the target temperature; and a step of heating the raw material mixture to reduce and melt the raw material mixture and to produce the initial molten slag. By this manufacturing method, metallic iron having a target carbon concentration can be efficiently manufactured.
摘要翻译：从含有碳质还原剂和含铁氧化物的原料混合物制造金属铁的方法具有如下步骤：根据金属铁中预定的目标碳浓度确定初始熔渣形成的目标温度，含有ang石成分的初始熔融渣，未还原铁氧化物和碳质还原剂的灰分，首先通过加热在原料混合物中制造; 制备原料混合物的步骤，产生对应于目标温度的初始熔渣的组成; 以及加热原料混合物以减少和熔化原料混合物并产生初始熔融炉渣的步骤。通过该制造方法，可以有效地制造具有目标碳浓度的金属铁。

7. 发明授权

US07938883B2 Method and apparatus for making metallic iron 有权
标题翻译：制造金属铁的方法和装置
公开(公告)号：US07938883B2
公开(公告)日：2011-05-10
申请号：US11855793
申请日：2007-09-14
申请人： Takuya Negami , Kazuo Kunii , Shinichi Inaba , Masataka Shimizu , Isao Kobayashi , Yoshimichi Takenaka , Toshihide Matsumura , Akira Uragami , Takashi Kujirai , Osamu Tsuchiya , Kimio Sugiyama , Shuzo Ito , Shoichi Kikuchi
发明人： Takuya Negami , Kazuo Kunii , Shinichi Inaba , Masataka Shimizu , Isao Kobayashi , Yoshimichi Takenaka , Toshihide Matsumura , Akira Uragami , Takashi Kujirai , Osamu Tsuchiya , Kimio Sugiyama , Shuzo Ito , Shoichi Kikuchi
IPC分类号： C21B13/00 , C21B13/08 , C21B13/10
CPC分类号： C21B13/0046 , C21B13/105 , Y02P10/136 , Y10T428/2991
摘要： A method of making metallic iron in which a compact, containing iron oxide such as iron ore or the like and a carbonaceous reductant such as coal or the like, is used as material, and the iron oxide is reduced through the application of heat, thereby making metallic iron. In the course of this reduction, a shell composed of metallic iron is generated and grown on the surface of the compact, and slag aggregates inside the shell. This reduction continues until substantially no iron oxide is present within the metallic iron shell. Subsequently, heating is further performed to melt the metallic iron and slag. Molten metallic iron and molten slag are separated one from the other, thereby obtaining metallic iron with a relatively high metallization ratio. Through the employment of an apparatus for making metallic iron of the present invention, the above-described method is efficiently carried out, and metallic iron having a high iron purity can be made continuously as well as productively not only from iron oxide having a high iron content but also from iron oxide having a relatively low iron content.
摘要翻译：制造金属铁的方法，其中使用含有铁矿石等铁氧化物的致密物和煤等碳质还原剂的材料，通过加热使氧化铁还原，制作金属铁。在这种还原过程中，在压实体的表面上产生并生长由金属铁组成的壳，并且炉渣中的炉渣聚集。该还原继续，直到金属铁壳内基本上不存在氧化铁。随后，进一步加热以熔化金属铁和炉渣。熔融的金属铁和熔渣彼此分离，从而获得具有相对高的金属化比的金属铁。通过使用本发明的金属铁制造装置，能够有效地进行上述的制造方法，能够连续生产铁纯度高的金属铁，并且不仅可以生产出具有高铁的铁氧化物含量也来自铁含量较低的氧化铁。

8. 发明授权

US06432533B1 Metallic iron containing slag 有权
标题翻译：含金属铁渣
公开(公告)号：US06432533B1
公开(公告)日：2002-08-13
申请号：US09478409
申请日：2000-01-06
申请人： Takuya Negami , Kazuo Kunii , Shinichi Inaba , Masataka Shimizu , Isao Kobayashi , Yoshimichi Takenaka , Toshihide Matsumura , Akira Uragami , Takashi Kujirai , Osamu Tsuchiya , Kimio Sugiyama , Shuzo Ito , Shoichi Kikuchi
发明人： Takuya Negami , Kazuo Kunii , Shinichi Inaba , Masataka Shimizu , Isao Kobayashi , Yoshimichi Takenaka , Toshihide Matsumura , Akira Uragami , Takashi Kujirai , Osamu Tsuchiya , Kimio Sugiyama , Shuzo Ito , Shoichi Kikuchi
IPC分类号： B32B516
CPC分类号： C21B13/0046 , C21B13/105 , Y02P10/136 , Y10T428/2991
摘要： A method of making metallic iron in which a compact, containing iron oxide such as iron ore or the like and a carbonaceous reductant such as coal or the like, is used as material, and the iron oxide is reduced through the application of heat, thereby making metallic iron. In the course of this reduction, a shell composed of metallic iron is generated and grown on the surface of the compact, and slag aggregates inside the shell. This reduction continues until substantially no iron oxide is present within the metallic iron shell. Subsequently, heating is further performed to melt the metallic iron and slag. Molten metallic iron and molten slag are separated one from the other, thereby obtaining metallic iron with a relatively high metallization ratio. Through the employment of an apparatus for making metallic iron of the present invention, the above-described method is efficiently carried out, and metallic iron having a high iron purity can be made continuously as well as productively not only from iron oxide having a high iron content but also from iron oxide having a relatively low iron content.
摘要翻译：制造金属铁的方法，其中使用含有铁矿石等铁氧化物的致密物和煤等碳质还原剂的材料，通过加热使氧化铁还原，制作金属铁。在这种还原过程中，在压实体的表面上产生并生长由金属铁组成的壳，并且炉渣中的炉渣聚集。该还原继续，直到金属铁壳内基本上不存在氧化铁。随后，进一步加热以熔化金属铁和炉渣。熔融的金属铁和熔渣彼此分离，从而获得具有相对高的金属化比的金属铁。通过使用本发明的金属铁制造装置，能够有效地进行上述的制造方法，能够连续生产铁纯度高的金属铁，并且不仅可以生产出具有高铁的铁氧化物含量也来自铁含量较低的氧化铁。

9. 发明授权

US06210462B1 Method and apparatus for making metallic iron 有权
标题翻译：制造金属铁的方法和装置
公开(公告)号：US06210462B1
公开(公告)日：2001-04-03
申请号：US09176311
申请日：1998-10-22
申请人： Shoichi Kikuchi , Akira Uragami , Isao Kobayashi , Yasuhiro Tanigaki , Eiichi Ito , Koji Tokuda , Osamu Tsuchiya , Shuzo Ito
发明人： Shoichi Kikuchi , Akira Uragami , Isao Kobayashi , Yasuhiro Tanigaki , Eiichi Ito , Koji Tokuda , Osamu Tsuchiya , Shuzo Ito
IPC分类号： C21B1108
CPC分类号： C21B13/105 , C21B13/10 , Y02P10/216
摘要： A method of making metallic iron includes heating a mixed powder containing iron oxide and a carbonaceous reducing agent on a hearth to reduce the iron oxide and melt the reduced iron. Preliminary molding of the mixed powder starting material into pellets is not required. The resulting metallic iron contains extremely low concentrations of slag ingredients, even when the mixed powder starting material contains only low concentrations of iron oxide.
摘要翻译：制造金属铁的方法包括在炉膛上加热含有氧化铁和碳质还原剂的混合粉末以减少氧化铁并熔化还原铁。不需要将混合粉末起始材料初步模制成颗粒。所得到的金属铁含有极低浓度的炉渣成分，即使混合粉末原料仅含有低浓度的氧化铁。

10. 发明授权

US06036744A Method and apparatus for making metallic iron 失效
公开(公告)号：US06036744A
公开(公告)日：2000-03-14
申请号：US818954
申请日：1997-03-14
申请人： Takuya Negami , Kazuo Kunii , Shinichi Inaba , Masataka Shimizu , Isao Kobayashi , Yoshimichi Takenaka , Toshihide Matsumura , Akira Uragami , Takashi Kujirai , Osamu Tsuchiya , Kimio Sugiyama , Shuzo Ito , Shoichi Kikuchi
发明人： Takuya Negami , Kazuo Kunii , Shinichi Inaba , Masataka Shimizu , Isao Kobayashi , Yoshimichi Takenaka , Toshihide Matsumura , Akira Uragami , Takashi Kujirai , Osamu Tsuchiya , Kimio Sugiyama , Shuzo Ito , Shoichi Kikuchi
IPC分类号： C21B13/00 , C21B13/10 , C21B15/00 , C21B11/06 , C22B1/20
CPC分类号： C21B13/0046 , C21B13/105 , Y02P10/136 , Y10T428/2991
摘要： A method of making metallic iron in which a compact, containing iron oxide such as iron ore or the like and a carbonaceous reductant such as coal or the like, is used as material, and the iron oxide is reduced through the application of heat, thereby making metallic iron. In the course of this reduction, a shell composed of metallic iron is generated and grown on the surface of the compact, and slag aggregates inside the shell. This reduction continues until substantially no iron oxide is present within the metallic iron shell. Subsequently, heating is further performed to melt the metallic iron and slag. Molten metallic iron and molten slag are separated one from the other, thereby obtaining metallic iron with a relatively high metallization ratio. Through the employment of an apparatus for making metallic iron of the present invention, the above-described method is efficiently carried out, and metallic iron having a high iron purity can be made continuously as well as productively not only from iron oxide having a high iron content but also from iron oxide having a relatively low iron content.

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