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1. 发明专利

AU3578195A Process for producing crystalline microporous body 未知
公开(公告)号：AU3578195A
公开(公告)日：1996-12-11
申请号：AU3578195
申请日：1995-09-28
申请人： JAPAN AS REPRESENTED BY DIRECTOR GENERAL OF AGENCY OF INDUSTRIAL SCIENCE AND TECH , KUBOTA KK
发明人： SHIMIZU SHINICHI , MIZUKAMI FUJIO , KIYOZUMI YOSHIMICHI
IPC分类号： B01J29/035 , B01J29/072 , B01J29/40 , B01J37/02 , C01B37/02 , C01B39/02 , C01B39/04 , C01B39/26 , C01B39/38 , C01B39/46 , C01B39/36
摘要： A method of manufacturing crystalline microporous material suitable for manufacturing a variety of crystalline microporous material under mild reaction conditions and under safe working environmental conditions by using simple installation. The crystalline microporous materials obtained by the present invention may be used as adsorbent agent, catalyst or separating material. According to the characterizing features of the manufacturing method of the present invention, there are provided a method of using cation compound or amine as crystallizing modifier and using, in combination, raw material including canemite or silicon dioxide and a further method using raw material including silicon dioxide and aluminum salt. The method includes a step of mixing these components, a solid-liquid separating step for separating produced fine particles, and a crystallizing step for crystallizing the separated solid component. The invention achieves improvement in safety, economy and so on, in comparison with the coventionally practiced hydrothermal synthesis method which requires severe reaction conditions of high-temperature, high-pressure and strong alkaline. Further, the method allows freedom in adjustment of the pore diameter and allows a higher proportion of porous structure to be maitained in a product when the material is formed into a molded product.

2. 发明公开

EP0773190A4 PROCESS FOR PRODUCING CRYSTALLINE MICROPOROUS BODY 失效
标题翻译：用于生产的结晶微孔BODY
公开(公告)号：EP0773190A4
公开(公告)日：1997-07-30
申请号：EP95932937
申请日：1995-09-28
申请人： KUBOTA KK , AGENCY IND SCIENCE TECHN
发明人： SHIMIZU SHINICHI , MIZUKAMI FUJIO , KIYOZUMI YOSHIMICHI
IPC分类号： B01J29/035 , B01J29/072 , B01J29/40 , B01J37/02 , C01B37/02 , C01B39/02 , C01B39/04 , C01B39/26 , C01B39/38 , C01B39/46 , C01B39/36
CPC分类号： B01J29/40 , B01J29/035 , B01J29/072 , B01J37/0236 , B01J2229/26 , B01J2229/36 , B01J2229/42 , C01B37/02 , C01B39/02 , C01B39/04 , C01B39/265 , C01B39/38 , C01B39/46 , Y10S423/22 , Y10S423/25 , Y10S423/29
摘要： A process for producing a crystalline microporous body under mild conditions using simple equipment in a highly safe state, which process is suited for producing various crystalline microporous bodies usable as adsorbents, catalysts and separating materials. The process is characterized by the use of a crystallization regulator comprising a cationic compound or an amine and the starting material containing a silicate having an ideal compositional formula of NaHSi2O5 or silicon dioxide or the use of the starting material containing silicon dioxide and an aluminum salt, and comprises the step of mixing the reactants, the step of conducting solid-liquid separation of the fine particles thus formed, and the step of crystallizing the solid component thus separted. As compared with the conventional hydrothermal synthesis process requiring such severe conditions as high temperature, pressure and alkalinity, this process is improved in safety and economy, serves to control the pore diameters arbitrarily, and gives a molded body retaining a high content of the porous structure.

3. 发明专利

DE69510550T2 未知
公开(公告)号：DE69510550T2
公开(公告)日：2000-01-20
申请号：DE69510550
申请日：1995-09-28
申请人： KUBOTA KK , AGENCY IND SCIENCE TECHN
发明人： SHIMIZU SHINICHI , MIZUKAMI FUJIO , KIYOZUMI YOSHIMICHI
IPC分类号： B01J29/035 , B01J29/072 , B01J29/40 , B01J37/02 , C01B37/02 , C01B39/02 , C01B39/04 , C01B39/26 , C01B39/38 , C01B39/46 , C01B39/36
摘要： A method of manufacturing crystalline microporous material suitable for manufacturing a variety of crystalline microporous material under mild reaction conditions and under safe working environmental conditions by using simple installation. The crystalline microporous materials obtained by the present invention may be used as adsorbent agent, catalyst or separating material. According to the characterizing features of the manufacturing method of the present invention, there are provided a method of using cation compound or amine as crystallizing modifier and using, in combination, raw material including canemite or silicon dioxide and a further method using raw material including silicon dioxide and aluminum salt. The method includes a step of mixing these components, a solid-liquid separating step for separating produced fine particles, and a crystallizing step for crystallizing the separated solid component. The invention achieves improvement in safety, economy and so on, in comparison with the coventionally practiced hydrothermal synthesis method which requires severe reaction conditions of high-temperature, high-pressure and strong alkaline. Further, the method allows freedom in adjustment of the pore diameter and allows a higher proportion of porous structure to be maitained in a product when the material is formed into a molded product.

4. 发明专利

NZ293360A PROCESS FOR PREPARING CRYSTALLINE MICROPOROUS SILICATES 未知
公开(公告)号：NZ293360A
公开(公告)日：1997-11-24
申请号：NZ29336095
申请日：1995-09-28
申请人： KUBOTA KK , AGENCY IND SCIENCE TECHN
发明人： SHIMIZU SHINICHI , MIZUKAMI FUJIO , KIYOZUMI YOSHIMICHI
IPC分类号： B01J29/035 , B01J29/072 , B01J29/40 , B01J37/02 , C01B37/02 , C01B39/02 , C01B39/04 , C01B39/26 , C01B39/38 , C01B39/46 , C01B33/20 , B01J20/30
摘要： A method of manufacturing crystalline microporous material suitable for manufacturing a variety of crystalline microporous material under mild reaction conditions and under safe working environmental conditions by using simple installation. The crystalline microporous materials obtained by the present invention may be used as adsorbent agent, catalyst or separating material. According to the characterizing features of the manufacturing method of the present invention, there are provided a method of using cation compound or amine as crystallizing modifier and using, in combination, raw material including canemite or silicon dioxide and a further method using raw material including silicon dioxide and aluminum salt. The method includes a step of mixing these components, a solid-liquid separating step for separating produced fine particles, and a crystallizing step for crystallizing the separated solid component. The invention achieves improvement in safety, economy and so on, in comparison with the coventionally practiced hydrothermal synthesis method which requires severe reaction conditions of high-temperature, high-pressure and strong alkaline. Further, the method allows freedom in adjustment of the pore diameter and allows a higher proportion of porous structure to be maitained in a product when the material is formed into a molded product.

5. 发明专利

AT181713T 未知
公开(公告)号：AT181713T
公开(公告)日：1999-07-15
申请号：AT95932937
申请日：1995-09-28
申请人： KUBOTA KK , AGENCY IND SCIENCE TECHN
发明人： SHIMIZU SHINICHI , MIZUKAMI FUJIO , KIYOZUMI YOSHIMICHI
IPC分类号： B01J29/035 , B01J29/072 , B01J29/40 , B01J37/02 , C01B37/02 , C01B39/02 , C01B39/04 , C01B39/26 , C01B39/38 , C01B39/46 , C01B39/36
摘要： A method of manufacturing crystalline microporous material suitable for manufacturing a variety of crystalline microporous material under mild reaction conditions and under safe working environmental conditions by using simple installation. The crystalline microporous materials obtained by the present invention may be used as adsorbent agent, catalyst or separating material. According to the characterizing features of the manufacturing method of the present invention, there are provided a method of using cation compound or amine as crystallizing modifier and using, in combination, raw material including canemite or silicon dioxide and a further method using raw material including silicon dioxide and aluminum salt. The method includes a step of mixing these components, a solid-liquid separating step for separating produced fine particles, and a crystallizing step for crystallizing the separated solid component. The invention achieves improvement in safety, economy and so on, in comparison with the coventionally practiced hydrothermal synthesis method which requires severe reaction conditions of high-temperature, high-pressure and strong alkaline. Further, the method allows freedom in adjustment of the pore diameter and allows a higher proportion of porous structure to be maitained in a product when the material is formed into a molded product.

6. 发明专利

AU6873100A Novel compound and microporous material and method for production thereof 未知
公开(公告)号：AU6873100A
公开(公告)日：2001-04-17
申请号：AU6873100
申请日：2000-09-06
申请人： KUBOTA KK
发明人： YOKOTA MASAO , YAMAMOTO TAKUHISA , LIN SUI WEN , SHIMIZU SHINICHI , HIRANO TAKENORI
IPC分类号： B01D53/86 , B01D53/94 , B01J20/16 , B01J29/04 , B01J29/072 , C01B37/02 , C01B33/36 , C01B39/02

7. 发明专利

DE69510550D1 未知
公开(公告)号：DE69510550D1
公开(公告)日：1999-08-05
申请号：DE69510550
申请日：1995-09-28
申请人： KUBOTA KK , AGENCY IND SCIENCE TECHN
发明人： SHIMIZU SHINICHI , MIZUKAMI FUJIO , KIYOZUMI YOSHIMICHI
IPC分类号： B01J29/035 , B01J29/072 , B01J29/40 , B01J37/02 , C01B37/02 , C01B39/02 , C01B39/04 , C01B39/26 , C01B39/38 , C01B39/46 , C01B39/36
摘要： A method of manufacturing crystalline microporous material suitable for manufacturing a variety of crystalline microporous material under mild reaction conditions and under safe working environmental conditions by using simple installation. The crystalline microporous materials obtained by the present invention may be used as adsorbent agent, catalyst or separating material. According to the characterizing features of the manufacturing method of the present invention, there are provided a method of using cation compound or amine as crystallizing modifier and using, in combination, raw material including canemite or silicon dioxide and a further method using raw material including silicon dioxide and aluminum salt. The method includes a step of mixing these components, a solid-liquid separating step for separating produced fine particles, and a crystallizing step for crystallizing the separated solid component. The invention achieves improvement in safety, economy and so on, in comparison with the coventionally practiced hydrothermal synthesis method which requires severe reaction conditions of high-temperature, high-pressure and strong alkaline. Further, the method allows freedom in adjustment of the pore diameter and allows a higher proportion of porous structure to be maitained in a product when the material is formed into a molded product.

8. 发明专利

AU697270B2 Process for producing crystalline microporous body 未知
公开(公告)号：AU697270B2
公开(公告)日：1998-10-01
申请号：AU3578195
申请日：1995-09-28
申请人： KUBOTA KK , JP AGENCY OF IND
发明人： SHIMIZU SHINICHI , MIZUKAMI FUJIO , KIYOZUMI YOSHIMICHI
IPC分类号： B01J29/035 , B01J29/072 , B01J29/40 , B01J37/02 , C01B37/02 , C01B39/02 , C01B39/04 , C01B39/26 , C01B39/38 , C01B39/46 , C01B39/36
摘要： A method of manufacturing crystalline microporous material suitable for manufacturing a variety of crystalline microporous material under mild reaction conditions and under safe working environmental conditions by using simple installation. The crystalline microporous materials obtained by the present invention may be used as adsorbent agent, catalyst or separating material. According to the characterizing features of the manufacturing method of the present invention, there are provided a method of using cation compound or amine as crystallizing modifier and using, in combination, raw material including canemite or silicon dioxide and a further method using raw material including silicon dioxide and aluminum salt. The method includes a step of mixing these components, a solid-liquid separating step for separating produced fine particles, and a crystallizing step for crystallizing the separated solid component. The invention achieves improvement in safety, economy and so on, in comparison with the coventionally practiced hydrothermal synthesis method which requires severe reaction conditions of high-temperature, high-pressure and strong alkaline. Further, the method allows freedom in adjustment of the pore diameter and allows a higher proportion of porous structure to be maitained in a product when the material is formed into a molded product.

9. 发明专利

CA2176814A1 METHOD OF MANUFACTURING CRYSTALLINE MICROPOROUS MATERIAL 未知
公开(公告)号：CA2176814A1
公开(公告)日：1996-11-25
申请号：CA2176814
申请日：1995-09-28
申请人： KUBOTA KK , AGENCY IND SCIENCE TECHN
发明人： SHIMIZU SHINICHI , MIZUKAMI FUJIO , KIYOZUMI YOSHIMICHI
IPC分类号： B01J29/035 , B01J29/072 , B01J29/40 , B01J37/02 , C01B37/02 , C01B39/02 , C01B39/04 , C01B39/26 , C01B39/38 , C01B39/46 , B01J20/10
摘要： A process for producing a crystalline microporous body under mild conditions using simple equipment in a highly safe state, which process is suited for producing various crystalline microporous bodies usable as adsorbents, catalysts and separating materials. The process is characterized by the use of a crystallization regulator comprising a cationic compound or an amine and the starting material containing a silicate having an ideal compositional formula of NaHSi2O5 or silicon dioxide or the use of the starting material containing silicon dioxide and an aluminum salt, and comprises the step of mixing the reactants, the step of conducting solid-liquid separation of the fine particles thus formed, and the step of crystallizing the solid component thus separted. As compared with the conventional hydrothermal synthesis process requiring such severe conditions as high temperature, pressure and alkalinity, this process is improved in safety and economy, serves to control the pore diameters arbitrarily, and gives a molded body retaining a high content of the porous structure.

10. 发明专利

JP2000154014A PRODUCTION OF INTERMEDIATE OF CRYSTALLINE MICROPOROUS BODY 失效
公开(公告)号：JP2000154014A
公开(公告)日：2000-06-06
申请号：JP32789498
申请日：1998-11-18
申请人： KUBOTA KK
发明人： YOKOTA MASAO , YAMAMOTO TAKUHISA , SHIMIZU SHINICHI
IPC分类号： C01B33/12
摘要： PROBLEM TO BE SOLVED: To provide a method for producing the intermediate of a crystalline microporous body having good formability in which crosslinks are hardly formed among layers of a sheet silica structure. SOLUTION: This producing method includes a mixing process to mix at least one kind of crystallization controlling agent selected from ammonium ions (R4N+, wherein R is one kind selected from hydrogen, =9.0 and

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