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1. 发明专利

JP2011214144A Method for production of nickel nanoparticle 审中-公开
标题翻译：生产镍纳米材料的方法
公开(公告)号：JP2011214144A
公开(公告)日：2011-10-27
申请号：JP2011056231
申请日：2011-03-15
申请人： Iwatani Internatl Corp , Nippon Steel Chem Co Ltd , Osaka Univ , 国立大学法人大阪大学 , 岩谷産業株式会社 , 新日鐵化学株式会社
发明人： YAMADA KATSUHIRO , INOUE SHUJI , NOMOTO HIDEAKI , YAMAUCHI TOMOHISA , WADA YUJI , TSUKAHARA YASUNORI
IPC分类号： B22F9/24 , B82Y40/00
摘要： PROBLEM TO BE SOLVED: To produce nickel nanoparticles which have appropriate dimension and distribution of grain size, and further have an improved sintering temperature by utilizing a liquid phase reaction technique.SOLUTION: There is provided a method for production of nickel nanoparticles, which comprises: a step of heating a mixture of nickel carboxylate with a primary amine to prepare a complexed reaction solution, and a step of irradiating the complexed reaction solution with a microwave thereby heating the complexed reaction solution at a temperature of ≥200°C to produce metal composite nickel nanoparticles containing a high melting point metal with a melting point higher than that of nickel. After the salt of the high melting metal is blended in any of the stage of preparing the mixture, the stage of the mixture or the stage of the complexed reaction solution at the latest before the irradiation with a microwave, heating with a microwave is performed. The nickel carboxylate is nickel acetate, the primary amine is oleylamine, and the high melting point metal salt is a tungsten salt or a molybdenum salt.
摘要翻译：要解决的问题：制备具有适当尺寸和粒度分布的镍纳米颗粒，并且通过利用液相反应技术进一步具有改进的烧结温度。解决方案：提供了一种生产镍纳米颗粒的方法，其包括：加热羧酸镍与伯胺的混合物以制备络合的反应溶液的步骤，以及用微波照射络合的反应溶液的步骤，从而在≥200℃的温度下加热络合的反应溶液以产生金属复合物含有熔点高于镍的高熔点金属的镍纳米粒子。在制备混合物的任何阶段中混合高熔点金属的盐之后，在微波照射之前，在微波加热下进行混合物的阶段或复合反应溶液的阶段。羧酸镍是乙酸镍，伯胺是油胺，高熔点金属盐是钨盐或钼盐。

2. 发明专利

JP2012193418A Method for producing ferrioxide-containing metal composite nickel nanoparticles, and ferrioxide-containing metal composite nickel nanoparticle 有权
标题翻译：含有含氧化铵的金属复合镍基纳米粒子的制备方法，含有金属氧化物的金属复合镍基纳米粒子
公开(公告)号：JP2012193418A
公开(公告)日：2012-10-11
申请号：JP2011058706
申请日：2011-03-17
申请人： Nippon Steel Chem Co Ltd , Osaka Univ , Iwatani Internatl Corp , 国立大学法人大阪大学 , 岩谷産業株式会社 , 新日鐵化学株式会社
发明人： INOUE SHUJI , YAMADA KATSUHIRO , NOMOTO HIDEAKI , YAMAUCHI TOMOHISA , WADA YUJI , TSUKAHARA YASUNORI , KAWABATA RYOJI , OKUMURA HARUKI
IPC分类号： B22F9/24 , B22F1/00 , C22C19/03
摘要： PROBLEM TO BE SOLVED: To obtain, in a liquid phase reaction technique, nickel nanoparticles having a properly high sintering temperature while securing proper size and distribution of the particle size.SOLUTION: The method for producing ferrioxide-containing metal composite nickel nanoparticles includes: a complexing reaction solution generation step of heating a mixture of nickel carboxylate, iron salt and primary amine to a temperature within the range of 100-165°C to obtain a reaction solution; and a nanoparticle slurry generation step of heating the reaction solution to a temperature of 170°C or higher by microwave irradiation to obtain a metal composite nickel nanoparticle slurry containing ferrioxide. In the nanoparticle containing ferrioxide, the total amount of nickel element, iron element and oxygen element is 95 pts.mass or more relative to 100 pts.mass of the metal composite nickel nanoparticle, the amount of iron element is within the range of 5-50 pts.mass relative to 100 pts.mass of the total amount of nickel element and iron element, the average particle size is within the range of 30-150 nm, and the ferrioxide is mainly composed of triiron tetraoxide.
摘要翻译：要解决的问题为了在液相反应技术中获得具有适当高的烧结温度的镍纳米颗粒，同时确保了适当的粒度和粒度的分布。解决方案：含有氧化亚铁的金属复合镍纳米颗粒的制造方法包括：将羧酸镍，铁盐和伯胺的混合物加热到100-165℃的温度范围内的络合反应溶液生成步骤，获得反应溶液; 以及通过微波照射将反应溶液加热至170℃以上的纳米粒子浆料生成工序，得到含有二氧化碳的金属复合镍纳米粒子浆料。在含有三氧化二铁的纳米粒子中，镍元素，铁元素和氧元素的总量比金属复合镍纳米粒子的100质量份高95个或更多，铁元素的量在5- 相对于镍元素和铁元素总量的100pts.mass，平均粒径为30〜150nm，氧化铁主要由四氧化三铁构成。版权所有（C）2013，JPO＆INPIT

3. 发明专利

JP2011214143A Method for production of nickel nanoparticle 审中-公开
标题翻译：生产镍纳米材料的方法
公开(公告)号：JP2011214143A
公开(公告)日：2011-10-27
申请号：JP2011056230
申请日：2011-03-15
申请人： Iwatani Internatl Corp , Nippon Steel Chem Co Ltd , Osaka Univ , 国立大学法人大阪大学 , 岩谷産業株式会社 , 新日鐵化学株式会社
发明人： YAMADA KATSUHIRO , INOUE SHUJI , NOMOTO HIDEAKI , YAMAUCHI TOMOHISA , WADA YUJI , TSUKAHARA YASUNORI
IPC分类号： B22F9/24
摘要： PROBLEM TO BE SOLVED: To provide a method for production of nickel nanoparticles, for obtaining nickel nanoparticles which has appropriate dimension and distribution of grain sizes and high dispersibility.SOLUTION: The method for production of nickel nanoparticles comprises: a first step of preparing a mixture of nickel carboxylate with a primary amine; a second step of heating the mixture to produce a nickel complex, thereby preparing a complexed reaction solution; and a third step of heating the complexed reaction solution at a temperature of ≥200°C with a microwave to produce a nickel nanoparticle slurry. In the third step, the heating is carried out in the presence of polycarboxylic acid having three or more valencies in the complexed reaction solution. Preferably, nickel carboxylate is nickel acetate, the primary amine is oleylamine, and the polycarboxylic acid is acyclic carboxylic acid.
摘要翻译：要解决的问题：提供一种制备镍纳米颗粒的方法，用于获得具有适当尺寸和分布的粒径和高分散性的镍纳米颗粒。溶液：制备镍纳米颗粒的方法包括：制备混合物的第一步骤的羧酸镍与伯胺反应; 加热混合物以制备镍络合物，从而制备络合的反应溶液的第二步骤; 以及第三步骤，在微波下，在≥200℃的温度下加热络合的反应溶液，生成镍纳米颗粒浆液。在第三步骤中，在络合的反应溶液中，在具有三价以上的多元羧酸的存在下进行加热。优选地，羧酸镍是乙酸镍，伯胺是油胺，多元羧酸是无环羧酸。

4. 发明专利

JP2011214142A Method for production of nickel nanoparticle 审中-公开
标题翻译：生产镍纳米材料的方法
公开(公告)号：JP2011214142A
公开(公告)日：2011-10-27
申请号：JP2011056229
申请日：2011-03-15
申请人： Iwatani Internatl Corp , Nippon Steel Chem Co Ltd , Osaka Univ , 国立大学法人大阪大学 , 岩谷産業株式会社 , 新日鐵化学株式会社
发明人： YAMADA KATSUHIRO , INOUE SHUJI , NOMOTO HIDEAKI , YAMAUCHI TOMOHISA , WADA YUJI , TSUKAHARA YASUNORI
IPC分类号： B22F9/24
摘要： PROBLEM TO BE SOLVED: To provide a method for production of nickel nanoparticles which can suitably obtain nickel nanoparticles with a particle diameter of ≤50 nm by a simple process using liquid phase reaction.SOLUTION: The method for production of nickel nanoparticles comprises the steps of: heating a mixture of straight-chain nickel carboxylate having 1 to 3 carbon atoms with a primary amine to produce a nickel complex, thereby preparing a complexed reaction solution; adding the complexed reaction solution with one or more metal salts selected from the group consisting of a palladium salt, a silver salt, a platinum salt and a gold salt; and heating the complexed reaction solution admixed with the metal salt with a microwave to produce nickel nanoparticles.
摘要翻译：要解决的问题：提供一种能够通过使用液相反应的简单方法适当地获得粒径为≤50nm的镍纳米粒子的镍纳米颗粒的制造方法。解决方案：制备镍纳米粒子的方法包括以下步骤：：将具有1至3个碳原子的直链羧酸镍的混合物与伯胺加热以制备镍络合物，从而制备络合的反应溶液; 将络合的反应溶液与一种或多种选自钯盐，银盐，铂盐和金盐的金属盐相加; 并用微波加热与金属盐混合的复合反应溶液以制备镍纳米颗粒。

5. 发明专利

JP2010064983A Method for producing nickel particle and nickel complex suitably used therein 审中-公开
标题翻译：用于生产镍颗粒和镍复合物的方法
公开(公告)号：JP2010064983A
公开(公告)日：2010-03-25
申请号：JP2008232863
申请日：2008-09-11
申请人： Iwatani Internatl Corp , Nippon Steel Chem Co Ltd , Osaka Univ , 国立大学法人大阪大学 , 岩谷産業株式会社 , 新日鐵化学株式会社
发明人： TSUKAHARA YASUNORI , WADA YUJI , YAMAUCHI TOMOHISA , BABA AKIO , YASUDA MAKOTO , SAKAMOTO TETSUO , KONO TAKUMI , KAWABATA RYOJI
IPC分类号： C07C211/03 , B22F9/24 , B22F9/30 , C07C53/06 , C07F15/04
摘要： PROBLEM TO BE SOLVED: To provide nickel particles suitably used in various applications such as catalysts, magnetic materials, and substrates for electrodes, particularly MLCC electrodes.
SOLUTION: A nickel complex is represented by formula (1): Ni(HCOO)
2 (L
1 )(L
2 ) (wherein L
1 and L
2 are each a Lewis base ligand and may be the same or different) and the nickel particles are produced by heating a solution including nickel formate dihydrate, a Lewis base such as an aliphatic amine, and a solvent.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供适用于各种应用的镍颗粒，例如催化剂，磁性材料和用于电极，特别是MLCC电极的基底。解决方案：镍络合物由式（1）表示：Ni（HCOO）2 SBS（L SP SP 2）（L SP SP 2）（其中L 1 和L 2 各自为路易斯碱配体，可以相同或不同），并且镍颗粒通过加热包括甲酸镍二水合物，路易斯碱如脂族胺和溶剂。版权所有（C）2010，JPO＆INPIT

6. 发明专利

JP2013007070A Apparatus and method of continuously producing nickel nanoparticles 审中-公开
标题翻译：连续生产镍基纳米粒子的装置及方法
公开(公告)号：JP2013007070A
公开(公告)日：2013-01-10
申请号：JP2011138767
申请日：2011-06-22
申请人： Nippon Steel & Sumikin Chemical Co Ltd , 新日鉄住金化学株式会社 , Osaka Univ , 国立大学法人大阪大学 , Iwatani Internatl Corp , 岩谷産業株式会社
发明人： YAMADA KATSUHIRO , NOMOTO HIDEAKI , INOUE SHUJI , TAKEKOSHI TETSUHITO , HIGUCHI MASAKAZU , KONO TAKUMI , TSUKAHARA YASUNORI , YAMAUCHI TOMOHISA , WADA YUJI , OKUMURA HARUKI
IPC分类号： B22F9/24 , H01B13/00
摘要： PROBLEM TO BE SOLVED: To provide a practically useful continuous production apparatus and continuous production method, capable of synthesizing nickel nanoparticles in a large amount.SOLUTION: In the continuous production apparatus 100, raw materials namely a complexed reaction solution and a metal salt are continuously or intermittently supplied via a raw material introduction member 1B into a reaction vessel 1 separately or in a mixed state. A microwave generated by a microwave generating part 10 is introduced into the reaction vessel 1 from a microwave introduction part 1A to irradiate a mixed reaction solution comprising nickel acetate and a metal salt. Thereby, the metal salt is reduced by heating to form fine particles of metal such as silver, and nickel acetate is reduced to allow metallic nickel to grow on nuclei, i.e., the resulting fine particles, whereby nickel nanoparticles are formed.
摘要翻译：要解决的问题：提供能够大量合成镍纳米颗粒的实用有用的连续制备装置和连续制备方法。解决方案：在连续生产设备100中，将原料即复合反应溶液和金属盐经由原料引入构件1B连续或间歇地分别供入反应容器1或混合状态。由微波产生部10产生的微波从微波导入部1A引入反应容器1，照射包含乙酸镍和金属盐的混合反应液。由此，金属盐通过加热而还原，形成细小的金属如银，并且还原乙酸镍以使金属镍在核上生长，即所得细小颗粒，从而形成镍纳米颗粒。版权所有（C）2013，JPO＆INPIT

7. 发明专利

JP2011212567A Composite catalyst for microwave reaction field and method of manufacturing the same, and method of manufacturing ester using the catalyst 审中-公开
标题翻译：用于微波反应的复合催化剂领域及其制备方法以及使用催化剂制备酯的方法
公开(公告)号：JP2011212567A
公开(公告)日：2011-10-27
申请号：JP2010082227
申请日：2010-03-31
申请人： Microwave Chemical Co Ltd , Nippon Steel Chem Co Ltd , Osaka Univ , マイクロ波環境化学株式会社 , 国立大学法人大阪大学 , 新日鐵化学株式会社
发明人： TSUKAHARA YASUNORI , WADA YUJI , YAMAUCHI TOMOHISA , BABA AKIO , YASUDA MAKOTO , KONO TAKUMI , NOMOTO HIDEAKI , ONISHI KIYOTAKA , HIGUCHI MASAKAZU , YOSHINO IWAO , ISHIZUKA AKINORI
IPC分类号： B01J27/20 , B01J37/34 , C07B61/00 , C07C67/08 , C07C69/58 , C10L1/02 , C11C3/08
CPC分类号： Y02E50/13
摘要： PROBLEM TO BE SOLVED: To provide a solid acid catalyst excellent in mass productivity, and to provide a method of manufacturing an ester excellent in mass productivity using the solid acid catalyst.SOLUTION: A composite catalyst for microwave reaction field comprises a functional group and a carbon structure having a pore structure suitable for a matter transport and sorbing microwaves. The pore structure has many meso pores, and has a total pore surface area of ≥10 m/g and ≤2,000 m/g and a meso pore area of ≥10% and ≤100% to the total pore surface area.
摘要翻译：要解决的问题：提供一种优异的批量生产率的固体酸催化剂，提供一种使用固体酸催化剂制备质量优良的酯的方法。微波反应领域的复合催化剂包括官能团和碳结构具有适于物质运输和吸附微波的孔结构。孔结构具有许多介孔孔，总孔表面积≥10m/ g，≤2,000m/ g，中孔面积占总孔面积的10％〜100％。

8. 发明专利

JP2011208083A Method for producing polyimide resin 审中-公开
标题翻译：生产聚酰胺树脂的方法
公开(公告)号：JP2011208083A
公开(公告)日：2011-10-20
申请号：JP2010079469
申请日：2010-03-30
申请人： Nippon Steel Chem Co Ltd , Osaka Univ , 国立大学法人大阪大学 , 新日鐵化学株式会社
发明人： YAMADA KATSUHIRO , TSUKAHARA YASUNORI , YAMAUCHI TOMOHISA
IPC分类号： C08L79/08 , C08G73/10 , C08K3/22 , H05K9/00
摘要： PROBLEM TO BE SOLVED: To provide a ferrite particle-containing polyimide resin capable of producing an electromagnetic wave absorber excellent in electromagnetic wave absorption properties.SOLUTION: When an anhydrous carboxylic acid and a diamine are dissolved in an organic solvent and ferrite particles are dispersed in the organic solvent, a polyamic acid solution wherein the ferrite particles are dispersed is obtained. Then, when heat treatment is carried out on the polyamic acid solution to polymerize the polyamic acid, the polyimide resin, wherein the ferrite particles are dispersed, is obtained.
摘要翻译：要解决的问题：提供一种能够制造电磁波吸收性优异的电磁波吸收体的含铁素体粒子的聚酰亚胺树脂。溶解度：将无水羧酸和二胺溶解在有机溶剂中时，铁素体粒子分散在得到有机溶剂，其中分散铁氧体颗粒的聚酰胺酸溶液。然后，当对聚酰胺酸溶液进行热处理以聚合聚酰胺酸时，得到其中分散铁氧体颗粒的聚酰亚胺树脂。

9. 发明专利

JP2011207731A Ferrite particle and method for manufacturing the same 审中-公开
标题翻译：微粒及其制造方法
公开(公告)号：JP2011207731A
公开(公告)日：2011-10-20
申请号：JP2010079468
申请日：2010-03-30
申请人： Nippon Steel Chem Co Ltd , Osaka Univ , 国立大学法人大阪大学 , 新日鐵化学株式会社
发明人： YAMADA KATSUHIRO , JIN TOMOSHI , TSUKAHARA YASUNORI , YAMAUCHI TOMOHISA , CHIKADA TSUKASA
IPC分类号： C01G49/00
摘要： PROBLEM TO BE SOLVED: To provide novel ferrite particles, which are in a nm order, are sufficiently fine and uniform, and have sufficient magnetic properties.SOLUTION: The ferrite particles are configured so that the average particle diameter is 5 to 30 nm; and the imaginary part of the complex permeability assumes a frequency dependency, and exhibits a peak in the frequency region of ≥1 GHz.
摘要翻译：要解决的问题：为了提供一个nm级的新颖的铁氧体颗粒，它们是足够细小和均匀的，并且具有足够的磁性能。解决方案：铁氧体颗粒的结构使得平均粒径为5〜30nm; 并且复磁导率的虚部呈现频率依赖性，并且在≥1GHz的频率区域中呈现峰值。

10. 发明专利

JP2009091254A METHOD FOR PRODUCING β-DICARBONYL COMPOUND DERIVATIVE 有权
标题翻译：生产β-二氯苯酚化合物衍生物的方法
公开(公告)号：JP2009091254A
公开(公告)日：2009-04-30
申请号：JP2007260216
申请日：2007-10-03
申请人： Nippon Steel Chem Co Ltd , Osaka Univ , 国立大学法人大阪大学 , 新日鐵化学株式会社
发明人： YASUDA MAKOTO , BABA AKIO , ARULANANDA BABU , WADA YUJI , TSUKAHARA YASUNORI , YAMAUCHI TOMOHISA , SAKAMOTO TETSUO , KONO TAKUMI
IPC分类号： C07C45/68 , B01J27/08 , B01J27/10 , B01J27/128 , B01J27/13 , B01J27/132 , B01J31/02 , C07B61/00 , C07C49/215 , C07C49/233 , C07C67/343 , C07C69/616 , C07C69/738 , C07C69/757
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a β-dicarbonyl compound derivative by using easily available raw materials and an inexpensive catalyst in a short reaction time while hardly forming a compound having problems on the environment such as a halogen compound and a carboxylic acid salt.
SOLUTION: The method for producing the β-dicarbonyl compound derivative includes reacting an alcohol having a phenyl group in the molecule or 2-cyclohexenyl alcohol with a β-dicarbonyl compound in the presence of a catalyst containing a 3-5d transition element or indium while heating the reaction mixture with microwave radiation.
COPYRIGHT: (C)2009,JPO&INPIT

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