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    • 8. 发明申请
    • INFRARED RADIATION ABSORBING ARTICLES AND METHOD OF MANUFACTURE
    • 红外辐射吸收制品及其制造方法
    • US20130224476A1
    • 2013-08-29
    • US13681791
    • 2012-11-20
    • Liping ZhengSteven M. GasworthJames E. PickettHaiying WangZhen LiuQueenie FuYang DongHongxia Xi
    • Liping ZhengSteven M. GasworthJames E. PickettHaiying WangZhen LiuQueenie FuYang DongHongxia Xi
    • C09D5/32
    • C09D5/32B82Y30/00C08G77/14C08G77/20C08G77/24C08K3/22C08K3/36C08K9/02C08K2003/2231C09D7/61C09D7/67C09D183/04C09D183/06C09D183/08Y10S977/773Y10T428/254
    • In an embodiment, a method for making an infrared radiation absorbing coating comprises: forming an ITO coating mixture comprising ITO and a first coating matrix, wherein the first coating matrix comprises the partial condensate of a silanol of the formula RnSi(OH)4-n, where n equals 1 or 2, and wherein R is selected from a C1-3 alkyl radical, a vinyl radical, a 3,3,3-trifluoropropyl radical, a gamma-glycidoxypropyl radical, and a gamma-methacryloxypropyl radical, wherein the ITO coating mixture is free of colloidal silica; forming a colloidal silica coating mixture comprising colloidal silica and a second coating matrix, wherein the second coating matrix comprises the partial condensate of a silanol of the formula RnSi(OH)4-n, where n equals 1 or 2, and wherein R is selected from an alkyl radical of 1 to 3 inclusive carbon atoms, a vinyl radical, a 3,3,3-trifluoropropyl radical, a gamma-glycidoxypropyl radical, and a gamma-methacryloxypropyl radical; and mixing the ITO coating mixture with the colloidal silica coating mixture to form a combined mixture. The combined mixture does not comprise a precipitate visible to the unaided eye after 2 weeks without stirring.
    • 在一个实施方案中,制备红外辐射吸收涂层的方法包括:形成包含ITO和第一涂层基质的ITO涂层混合物,其中第一涂层基质包含式RnSi(OH)4-n的硅烷醇的部分缩合物 其中n等于1或2,并且其中R选自C 1-3烷基,乙烯基,3,3,3-三氟丙基,γ-缩水甘油氧基丙基和γ-甲基丙烯酰氧基丙基,其中 ITO涂层混合物不含胶体二氧化硅; 形成包含胶体二氧化硅和第二涂层基质的胶态二氧化硅涂层混合物,其中所述第二涂层基质包含式R n Si(OH)4-n的硅烷醇的部分缩合物,其中n等于1或2,并且其中R选自 由1至3个包含碳原子的烷基,乙烯基,3,3,3-三氟丙基,γ-缩水甘油氧基丙基和γ-甲基丙烯酰氧基丙基; 并将ITO涂覆混合物与胶态二氧化硅涂层混合物混合以形成混合的混合物。 组合的混合物在不搅拌的情况下不含有肉眼可见的2周后的沉淀物。