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1. 发明授权

US09023478B2 Micropatterning of conductive graphite particles using microcontact printing 有权
标题翻译：使用微接触印刷的导电石墨颗粒的微图案化
公开(公告)号：US09023478B2
公开(公告)日：2015-05-05
申请号：US13619696
申请日：2012-09-14
申请人： Ilsoon Lee , Lawrence T. Drzal , Jue Lu , Troy R. Hendricks
发明人： Ilsoon Lee , Lawrence T. Drzal , Jue Lu , Troy R. Hendricks
IPC分类号： B32B9/00 , G03F7/00 , B82Y10/00 , B82Y40/00 , H05K3/12 , C01B31/04
CPC分类号： G03F7/0002 , B82Y10/00 , B82Y40/00 , C01B32/20 , H05K1/0259 , H05K3/1275 , H05K2201/0323 , H05K2203/0108 , H05K2203/09 , H05K2203/105 , Y10T428/30
摘要： Methods involve a combination of polyelectrolyte multilayer (PEM) coating or silane self assembly on a substrate; microcontact printing; and conductive graphite particles, especially size controlled highly conductive exfoliated graphite nanoplatelets. The conductive graphite particles are coated with a charged polymer such as sulfonated polystyrene. The graphite particles are patterned using microcontact printing and intact pattern transfer on a substrate that has an oppositely-charged surface. The method allows for conductive organic patterning on both flat and curved surfaces and can be used in microelectronic device fabrication.
摘要翻译：方法涉及在基底上组合聚电解质多层（PEM）涂层或硅烷自组装; 微接触印刷; 和导电石墨颗粒，特别是尺寸控制的高导电性剥离石墨纳米片。导电石墨颗粒用带电聚合物如磺化聚苯乙烯涂覆。使用微接触印刷和在具有相反电荷的表面的基底上的完整图案转印来对石墨颗粒进行图案化。该方法允许在平坦和弯曲表面上的导电有机图案化，并且可以用于微电子器件制造。

2. 发明申请

US20100052995A1 MICROPATTERNING OF CONDUCTIVE GRAPHITE PARTICLES USING MICROCONTACT PRINTING 审中-公开
标题翻译：使用微孔印刷的导电石墨颗粒的微孔
公开(公告)号：US20100052995A1
公开(公告)日：2010-03-04
申请号：US12515232
申请日：2007-11-15
申请人： Ilsoon Lee , Lawrence T. Drzal , Jue Lu , Troy R. Hendricks
发明人： Ilsoon Lee , Lawrence T. Drzal , Jue Lu , Troy R. Hendricks
IPC分类号： H01Q1/38 , B05D5/12 , B28B3/00 , C09D11/10 , H01B1/24 , H05K1/00 , H05K9/00
CPC分类号： G03F7/0002 , B82Y10/00 , B82Y40/00 , C01B32/20 , H05K1/0259 , H05K3/1275 , H05K2201/0323 , H05K2203/0108 , H05K2203/09 , H05K2203/105 , Y10T428/30
摘要： Methods involve a combination of polyelectrolyte multilayer (PEM) coating or silane self assembly on a substrate; microcontact printing; and conductive graphite particles, especially size controlled highly conductive exfoliated graphite nanoplatelets. The conductive graphite particles are coated with a charged polymer such as sulfonated polystyrene. The graphite particles are patterned using microcontact printing and intact pattern transfer on a substrate that has an oppositely-charged surface. The method allows for conductive organic patterning on both flat and curved surfaces and can be used in microelectronic device fabrication.
摘要翻译：方法涉及在基底上组合聚电解质多层（PEM）涂层或硅烷自组装; 微接触印刷; 和导电石墨颗粒，特别是尺寸控制的高导电性剥离石墨纳米片。导电石墨颗粒用带电聚合物如磺化聚苯乙烯涂覆。使用微接触印刷和在具有相反电荷的表面的基底上的完整图案转印来对石墨颗粒进行图案化。该方法允许在平坦和弯曲表面上的导电有机图案化，并且可以用于微电子器件制造。

3. 发明授权

US08460785B2 Wrinkle-free nanomechanical film 有权
标题翻译：无皱纹纳米机械薄膜
公开(公告)号：US08460785B2
公开(公告)日：2013-06-11
申请号：US12515155
申请日：2007-11-15
申请人： Ilsoon Lee , Troy R. Hendricks
发明人： Ilsoon Lee , Troy R. Hendricks
IPC分类号： B32B5/12 , B32B5/16 , B05D1/38
CPC分类号： B81B3/0072 , A61K8/0208 , A61Q19/08 , B32B27/08 , B32B27/14 , B32B2307/50 , B32B2555/00 , Y10T428/24942 , Y10T428/25 , Y10T428/259 , Y10T428/31938
摘要： Methods to control and prevent polymer films from buckling are provided. Buckled morphologies are created by thermally cycling or mechanically compressing a substrate such as poly(dimethylsiloxane) (PDMS) coated with a polyelectrolyte multilayer film. By varying the dimensions of the surface topography relative to the buckling wavelength (e.g., pattern size is less than, equal to, and greater than the buckling wavelength) the orientation and the local morphology of the buckled films is controlled. Based on the information obtained, we demonstrate how to alleviate the unavoidable buckling by incorporating nanoparticles into the film. In addition, we studied the effect of the silica layer that results from oxygen plasma treatment and the critical temperature for permanent film buckling.
摘要翻译：提供了控制和防止聚合物膜翘曲的方法。通过热循环或机械压缩涂覆有聚电解质多层膜的基底（例如聚（二甲基硅氧烷）（PDMS））产生弯曲的形态。通过改变表面形貌相对于弯曲波长的尺寸（例如，图案尺寸小于，等于并且大于屈曲波长），控制屈曲膜的取向和局部形态。基于获得的信息，我们演示如何通过将纳米颗粒纳入薄膜来缓解不可避免的屈曲。此外，我们研究了氧等离子体处理产生的二氧化硅层的影响和永久膜屈曲的临界温度。

4. 发明申请

US20100143677A1 WRINKLE-FREE NANOMECHANICAL FILM 有权
标题翻译：无皱的纳米薄膜
公开(公告)号：US20100143677A1
公开(公告)日：2010-06-10
申请号：US12515155
申请日：2007-11-15
申请人： Ilsoon Lee , Troy R. Hendricks
发明人： Ilsoon Lee , Troy R. Hendricks
IPC分类号： B32B7/02 , B05D1/36 , B32B5/16 , B32B9/00 , B32B27/32
CPC分类号： B81B3/0072 , A61K8/0208 , A61Q19/08 , B32B27/08 , B32B27/14 , B32B2307/50 , B32B2555/00 , Y10T428/24942 , Y10T428/25 , Y10T428/259 , Y10T428/31938
摘要： Methods to control and prevent polymer films from buckling are provided. Buckled morphologies are created by thermally cycling or mechanically compressing a substrate such as poly(dimethylsiloxane) (PDMS) coated with a polyelectrolyte multilayer film. By varying the dimensions of the surface topography relative to the buckling wavelength (e.g., pattern size is less than, equal to, and greater than the buckling wavelength) the orientation and the local morphology of the buckled films is controlled. Based on the information obtained, we demonstrate how to alleviate the unavoidable buckling by incorporating nanoparticles into the film. In addition, we studied the effect of the silica layer that results from oxygen plasma treatment and the critical temperature for permanent film buckling.
摘要翻译：提供了控制和防止聚合物膜翘曲的方法。通过热循环或机械压缩涂覆有聚电解质多层膜的基底（例如聚（二甲基硅氧烷）（PDMS））产生弯曲的形态。通过改变表面形貌相对于弯曲波长的尺寸（例如，图案尺寸小于，等于并且大于屈曲波长），控制屈曲膜的取向和局部形态。基于获得的信息，我们演示如何通过将纳米颗粒纳入薄膜来缓解不可避免的屈曲。此外，我们研究了氧等离子体处理产生的二氧化硅层的影响和永久膜屈曲的临界温度。

5. 发明申请

US20120321841A1 ARRAY OF ALIGNED AND DISPERSED CARBON NANOTUBES AND METHOD OF PRODUCING THE ARRAY 有权
公开(公告)号：US20120321841A1
公开(公告)日：2012-12-20
申请号：US13472928
申请日：2012-05-16
申请人： Ilia N. Ivanov , John T. Simpson , Troy R. Hendricks
发明人： Ilia N. Ivanov , John T. Simpson , Troy R. Hendricks
IPC分类号： B32B3/12 , B82Y30/00
CPC分类号： B32B9/04 , B32B2313/04 , B32B2457/20 , B82Y30/00 , B82Y40/00 , C01B32/168 , C01B2202/08 , C04B35/16 , C04B35/6224 , C04B35/803 , C04B2235/3201 , C04B2235/5288 , D01D5/00 , D01F9/12 , H01J1/304 , H01J9/025 , H01J2201/30469 , Y10S977/734 , Y10S977/742 , Y10S977/773 , Y10S977/902 , Y10T428/24157 , Y10T428/24994 , Y10T428/249942 , Y10T428/249945 , Y10T428/2918
摘要： An array of aligned and dispersed carbon nanotubes includes an elongate drawn body including a plurality of channels extending therethrough from a first end to a second end of the body, where the channels have a number density of at least about 100,000 channels/mm2 over a transverse cross-section of the body. A plurality of carbon nanotubes are disposed in each channel, and the carbon nanotubes are sufficiently dispersed and aligned along a length of the channels for the array to comprise an average resistivity per channel of about 9700 Ωm or less.

6. 发明授权

US08202749B1 Array of aligned and dispersed carbon nanotubes and method of producing the array 有权
标题翻译：排列和分散的碳纳米管阵列及其制备方法
公开(公告)号：US08202749B1
公开(公告)日：2012-06-19
申请号：US12642166
申请日：2009-12-18
申请人： Ilia N. Ivanov , John T. Simpson , Troy R. Hendricks
发明人： Ilia N. Ivanov , John T. Simpson , Troy R. Hendricks
IPC分类号： H01L21/00 , H01J19/24
CPC分类号： B32B9/04 , B32B2313/04 , B32B2457/20 , B82Y30/00 , B82Y40/00 , C01B32/168 , C01B2202/08 , C04B35/16 , C04B35/6224 , C04B35/803 , C04B2235/3201 , C04B2235/5288 , D01D5/00 , D01F9/12 , H01J1/304 , H01J9/025 , H01J2201/30469 , Y10S977/734 , Y10S977/742 , Y10S977/773 , Y10S977/902 , Y10T428/24157 , Y10T428/24994 , Y10T428/249942 , Y10T428/249945 , Y10T428/2918
摘要： An array of aligned and dispersed carbon nanotubes includes an elongate drawn body including a plurality of channels extending therethrough from a first end to a second end of the body, where the channels have a number density of at least about 100,000 channels/mm2 over a transverse cross-section of the body. A plurality of carbon nanotubes are disposed in each channel, and the carbon nanotubes are sufficiently dispersed and aligned along a length of the channels for the array to comprise an average resistivity per channel of about 9700 Ωm or less.
摘要翻译：排列和分散的碳纳米管的阵列包括细长的拉伸体，其包括从主体的第一端延伸穿过其中的多个通道，其中通道在横向上具有至少约100,000通道/ mm 2的数密度横截面的身体。在每个通道中设置多个碳纳米管，并且碳纳米管沿着用于阵列的通道的长度被充分地分散和排列，以包括每个通道的平均电阻率为约9700＆OHgrm以下。

7. 发明申请

US20120135233A1 ARRAY OF ALIGNED AND DISPERSED CARBON NANOTUBES AND METHOD OF PRODUCING THE ARRAY 有权
标题翻译：对准和分散的碳纳米管的阵列和产生阵列的方法
公开(公告)号：US20120135233A1
公开(公告)日：2012-05-31
申请号：US12642166
申请日：2009-12-18
申请人： Ilia N. Ivanov , John T. Simpson , Troy R. Hendricks
发明人： Ilia N. Ivanov , John T. Simpson , Troy R. Hendricks
IPC分类号： B32B9/04 , B29C59/02 , B32B17/02
CPC分类号： B32B9/04 , B32B2313/04 , B32B2457/20 , B82Y30/00 , B82Y40/00 , C01B32/168 , C01B2202/08 , C04B35/16 , C04B35/6224 , C04B35/803 , C04B2235/3201 , C04B2235/5288 , D01D5/00 , D01F9/12 , H01J1/304 , H01J9/025 , H01J2201/30469 , Y10S977/734 , Y10S977/742 , Y10S977/773 , Y10S977/902 , Y10T428/24157 , Y10T428/24994 , Y10T428/249942 , Y10T428/249945 , Y10T428/2918
摘要： An array of aligned and dispersed carbon nanotubes includes an elongate drawn body including a plurality of channels extending therethrough from a first end to a second end of the body, where the channels have a number density of at least about 100,000 channels/mm2 over a transverse cross-section of the body. A plurality of carbon nanotubes are disposed in each channel, and the carbon nanotubes are sufficiently dispersed and aligned along a length of the channels for the array to comprise an average resistivity per channel of about 9700 Ωm or less.
摘要翻译：排列和分散的碳纳米管的阵列包括细长的拉伸体，其包括从主体的第一端延伸穿过其中的多个通道，其中通道在横向上具有至少约100,000通道/ mm 2的数密度横截面的身体。在每个通道中设置多个碳纳米管，并且碳纳米管沿着用于阵列的通道的长度被充分地分散和排列，以包括每个通道的平均电阻率为约9700＆OHgrm以下。

8. 发明授权

US09245671B2 Electrically isolated, high melting point, metal wire arrays and method of making same 有权
标题翻译：电隔离，高熔点，金属丝阵列及其制造方法
公开(公告)号：US09245671B2
公开(公告)日：2016-01-26
申请号：US13420205
申请日：2012-03-14
申请人： John T. Simpson , Joseph P. Cunningham , Brian R. D'Urso , Troy R. Hendricks , Daniel A. Schaeffer
发明人： John T. Simpson , Joseph P. Cunningham , Brian R. D'Urso , Troy R. Hendricks , Daniel A. Schaeffer
IPC分类号： H01B13/14
CPC分类号： H01B13/14 , Y10T156/1002 , Y10T156/1084
摘要： A method of making a wire array includes the step of providing a tube of a sealing material and having an interior surface, and positioning a wire in the tube, the wire having an exterior surface. The tube is heated to soften the tube, and the softened tube is drawn and collapsed by a mild vacuum to bring the interior surface of the tube into contact with the wire to create a coated wire. The coated wires are bundled. The bundled coated wires are heated under vacuum to fuse the tube material coating the wires and create a fused rod with a wire array embedded therein. The fused rod is cut to form a wire array. A wire array is also disclosed.
摘要翻译：制造线阵列的方法包括提供密封材料的管并具有内表面的步骤，并将线定位在管中，所述线具有外表面。管被加热以软化管，并且软化的管被温和的真空拉伸和折叠，以使管的内表面与线接触以产生涂覆的线。涂层电线捆扎。捆扎的涂层线材在真空下被加热以熔化涂覆线材的管材料并产生嵌入其中的线阵列的熔丝棒。将熔断棒切割成线阵列。还公开了一种线阵列。

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