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1. 发明授权

US5435821A Controlled release vegetation enhancement agents coated with sulfonated polymers, method of production and prcesses of use 失效
标题翻译：涂覆有磺化聚合物的控制释放植被增强剂，生产方法和使用方法
公开(公告)号：US5435821A
公开(公告)日：1995-07-25
申请号：US634363
申请日：1990-12-31
申请人： Ilan Duvdevani , Evelyn N. Drake , Warren A. Thaler , Pacifico V. Manalastas
发明人： Ilan Duvdevani , Evelyn N. Drake , Warren A. Thaler , Pacifico V. Manalastas
IPC分类号： C05G3/00 , C05C9/00 , B32B5/16 , B32B27/06
CPC分类号： C05G3/0029 , Y02P60/212 , Y10S71/902 , Y10T428/263
摘要： A vegetation enhancement composite including a vegetation enhancement agent consisting of a first member selected from the group consisting of at least one macronutrient, micronutrient, nitrogen fertilizer including an inhibitor of nitrification activity, slow release fertilizer, and mixtures of such members and a pesticide; and at least one first controlled release film including a sulfonated polymer coating at least a portion of a surface of the vegetation enhancement agent. A method of producing controlled release fertilizers involving providing a vegetation enhancement agent consisting of a first member selected from the group consisting of at least one macronutrient, micronutrient, nitrogen fertilizer including an inhibitor of urease, nitrogen fertilizer including an inhibitor of nitrification activity, slow release fertilizer, and mixtures of such members and a pesticide; and coating at least one surface of the vegetation enhancement agent with a sulfonated polymer dissolved in a solvent system including an organic liquid to form a controlled release coating on the vegetation enhancement agent. An agricultural process involving the application of a vegetable enhancement agent coated with a sulfonated polymer to plant growth medium to stimulate germination and enhance growth of vegetable matter.
摘要翻译：一种植被增强复合材料，其包括由选自至少一种大量营养素，微量营养素，包括硝化活性抑制剂的氮肥，缓释肥料以及这些成分和农药的混合物的第一成员组成的植物增强剂; 以及包含磺化聚合物的至少一个第一控释膜，其涂覆植物增强剂的表面的至少一部分。一种生产控释肥料的方法，其包括提供植物增强剂，其由选自至少一种大量营养素，微量营养素，氮肥，包括脲酶抑制剂的氮肥，包括硝化活性抑制剂的氮肥，缓释肥料，以及这些成员和农药的混合物; 并用溶解在包括有机液体的溶剂系统中的磺化聚合物涂覆植被增强剂的至少一个表面以在植被增强剂上形成控释层。涉及将涂覆有磺化聚合物的植物增强剂施用于植物生长培养基以刺激发芽并增强植物物质生长的农业方法。

2. 发明授权

US4701204A Composite comprising a substrate coated with polymeric complexes 失效
标题翻译：复合材料包括用聚合复合物涂覆的基材
公开(公告)号：US4701204A
公开(公告)日：1987-10-20
申请号：US808034
申请日：1985-12-12
申请人： Ilan Duvdevani , Pacifico V. Manalastas , Evelyn N. Drake , Warren A. Thaler
发明人： Ilan Duvdevani , Pacifico V. Manalastas , Evelyn N. Drake , Warren A. Thaler
IPC分类号： C05C9/00 , C05G3/00 , B32B5/16 , B32B27/06
CPC分类号： C05C9/005 , C05G3/0029 , Y10T428/263 , Y10T428/2998 , Y10T428/31692 , Y10T428/31917
摘要： A composite comprising a substrate and an elastomeric coating adhered to at least one surface of said substrate, said elastomeric coating having a thickness of about 1 to about 100 micrometers, wherein said elastomeric coating comprises an interpolymeric complex of a neutralized sulfonated polymer and an amine containing polymer, said neutralized sulfonated polymer having a sulfonate content of about 4 to about 200 meq. per 100 grams of said neutralized sulfonated polymer and said amine containing polymer containing basic nitrogen atoms wherein the basic nitrogen content ranges from about 4 to about 500 meq. per 100 grams of polymer.
摘要翻译：一种复合材料，其包含粘附到所述基材的至少一个表面上的基材和弹性体涂层，所述弹性体涂层具有约1至约100微米的厚度，其中所述弹性体涂层包含中和的磺化聚合物和含有聚合物，所述中和的磺化聚合物的磺酸盐含量为约4至约200meq。每100克所述中和的磺化聚合物和含有碱性氮原子的所述含胺聚合物，其中碱性氮含量为约4至约500meq。每100克聚合物。

3. 发明授权

US5188654A Coatings with ionically and covalently crosslinked neutralized carboxylated polymers 失效
标题翻译：具有离子交换中性羧基化聚合物的涂料
公开(公告)号：US5188654A
公开(公告)日：1993-02-23
申请号：US676606
申请日：1991-03-28
申请人： Pacifico V. Manalastas , Evelyn N. Drake , Warren A. Thaler , Edward N. Kresge , Chester W. Elspass , Albert J. Geiger , Vijay Swarup
发明人： Pacifico V. Manalastas , Evelyn N. Drake , Warren A. Thaler , Edward N. Kresge , Chester W. Elspass , Albert J. Geiger , Vijay Swarup
IPC分类号： A01N25/26 , C05G3/00
CPC分类号： C05G3/0029 , A01N25/26 , Y10T428/263
摘要： A composite comprising a substrate and a polymeric coating adhered to at least one surface of said substrate, said polymer coating having a thickness of about 1 to about 100 micrometers, wherein said polymer coating comprises an ionically and covalently crosslinked neutralized carboxylated polymer having a carboxylate content of about 5 to about 300 meq. per 100 grams of said ionically and covalently crosslinked neutralized carboxylated polymer.
摘要翻译：一种复合材料，其包含粘附到所述基底的至少一个表面上的基底和聚合物涂层，所述聚合物涂层具有约1至约100微米的厚度，其中所述聚合物涂层包含具有羧酸盐含量的离子和共价交联的中和的羧化聚合物约5至约300meq。每100克所述离子和共价交联的中和的羧化聚合物。

4. 发明授权

US4988377A Coatings with sulfonated polymers 失效
标题翻译：涂料与磺化聚合物
公开(公告)号：US4988377A
公开(公告)日：1991-01-29
申请号：US387059
申请日：1989-07-31
申请人： Pacifico V. Manalastas , Warren A. Thaler , Evelyn N. Drake , Israel S. Pasternak
发明人： Pacifico V. Manalastas , Warren A. Thaler , Evelyn N. Drake , Israel S. Pasternak
IPC分类号： C05C9/00 , C05G3/00
CPC分类号： C05G3/0029 , C05C9/005
摘要： A composite comprising a substrate and an elastomeric coating adhered to at least one surface of said substrate, said elastomeric coating having a thickness of about 1 to about 100 micrometers, wherein said elastomeric coating comprises a neutralized sulfonated polymer having a sulfonate content of about 4 to about 200 meq. per 100 grams of said neutralized sulfonated polymer.
摘要翻译：一种复合材料，其包括粘附到所述基材的至少一个表面上的基材和弹性体涂层，所述弹性体涂层具有约1至约100微米的厚度，其中所述弹性体涂层包含中和的磺化聚合物，其磺酸盐含量为约4至约200毫克每100克所述中和的磺化聚合物。

5. 发明授权

US5190797A Coating a substrate with an ionomer 失效
标题翻译：用离聚物涂覆基材
公开(公告)号：US5190797A
公开(公告)日：1993-03-02
申请号：US720042
申请日：1991-06-24
申请人： Warren A. Thaler , Cruise K. Jones , Evelyn N. Drake , Pacifico V. Manalastas , Edward N. Kresge
发明人： Warren A. Thaler , Cruise K. Jones , Evelyn N. Drake , Pacifico V. Manalastas , Edward N. Kresge
IPC分类号： B01J2/00 , B01J2/28 , C05G3/00
CPC分类号： B01J2/28 , B01J2/006 , C05G3/0029
摘要： The present invention relates to a process for the encapsulation of a solid substrate with a neutralized sulfonated polymer, which comprises the steps of: (a) forming a solution of a non-conjugated, diene polymer in a solvent selected from the group consisting of aliphatic, aromatic hydrocarbons and mixtures thereof; (b) contacting the solution of the unsaturated polymer with a sulfonating agent at a sufficient temperature and for a sufficient period of time to form a solution of a sulfonated polymer containing free acid; (c) forming a solution of a base selected from the group consisting of alkali metal hydroxides and mixtures thereof in a mixtrue of an aliphatic alcohol and a hydrocarbon, the hydrocarbon being selected from the group consisting of aliphatic and aromatic hydrocarbons and mixtures thereof; (d) adding the solution of base to the solution of sulfonated polymer in an amount sufficient to neutralize the polymer and the free acid, thereby forming a coating solution; (e) contacting the solid substrate with the coating solution while removing the solvent therefrom, thereby forming an encapsulated substrate. In a preferred embodiment, the solvent removed during step (e) is recovered and distilled to separate the solvent into at least two fractions, a fraction containing substantially hydrocarbon and an alcohol containing fraction. The separated solvents are then recycled to dissolve the polymer in step (a) and to dissolve the base in step (c).
摘要翻译：本发明涉及用中和的磺化聚合物包封固体基质的方法，其包括以下步骤：（a）在选自脂肪族的溶剂中的溶剂中形成非共轭二烯聚合物的溶液，芳族烃及其混合物; （b）在足够的温度下将不饱和聚合物的溶液与磺化剂接触足够的时间以形成含有游离酸的磺化聚合物的溶液; （c）在脂族醇和烃的混合物中形成选自碱金属氢氧化物及其混合物的碱的溶液，所述烃选自脂族和芳族烃及其混合物; （d）将碱溶液以足以中和聚合物和游离酸的量向磺化聚合物溶液中加入，从而形成涂布溶液; （e）将固体基质与涂布溶液接触，同时从其中除去溶剂，由此形成封装的基材。在优选的实施方案中，回收步骤（e）中除去的溶剂并蒸馏以将溶剂分离成至少两个馏分，基本上含有烃和含醇的馏分。然后将分离的溶剂再循环以在步骤（a）中溶解聚合物并在步骤（c）中溶解碱。

6. 发明授权

US4997470A Biodegradable barrier films of ionomer polymer 失效
标题翻译：离聚物聚合物的可生物降解阻隔膜
公开(公告)号：US4997470A
公开(公告)日：1991-03-05
申请号：US380248
申请日：1989-07-17
申请人： Warren A. Thaler , Pacifico V. Manalastas , Evelyn N. Drake , Robert D. Lundberg
发明人： Warren A. Thaler , Pacifico V. Manalastas , Evelyn N. Drake , Robert D. Lundberg
IPC分类号： A01N25/10 , C08F8/30 , C08G81/02 , C09D123/32
CPC分类号： C08G81/024 , A01N25/10 , C08F8/44 , C09D123/32 , C08F2800/20
摘要： An encapsulated water soluble fertilizer which comprises a polymeric film of about 2 to about 100 micrometers coated on a surface of said fertilizer, said polymeric film comprising a sulfonated polymer having about 10 to about 200 meq of sulfonate groups per 100 grams of said sulfonated polymer, said sulfonate groups being neutralized with a polycaprolactone polymer being characterized by the formula ##STR1## wherein R.sub.1 and R.sub.2 is an alkyl, cycloalkyl or aryl group; R.sub.3, R.sub.4 and R.sub.5 are a hydrogen or alkyl, cycloalkyl, or aryl groups; m equals 1 to 20 and n equals 1 to 500.
摘要翻译：一种包封的水溶性肥料，其包含涂覆在所述肥料表面上的约2至约100微米的聚合物膜，所述聚合物膜包含每100克所述磺化聚合物约10至约200毫克磺酸盐基团的磺化聚合物，所述磺酸酯基团用聚己内酯聚合物中和，其特征在于下式：其中R 1和R 2是烷基，环烷基或芳基; R3，R4和R5是氢或烷基，环烷基或芳基; m等于1到20，n等于1到500。

7. 发明授权

US5256181A Coatings with ionically and covalently crosslinked sulfonated polymers 失效
标题翻译：具有离子交换和共价交联的磺化聚合物的涂料
公开(公告)号：US5256181A
公开(公告)日：1993-10-26
申请号：US676684
申请日：1991-03-28
申请人： Pacifico V. Manalastas , Evelyn N. Drake , Warren A. Thaler , Edward N. Kresge , Chester W. Elspass , Albert J. Geiger , Vijay Swarup
发明人： Pacifico V. Manalastas , Evelyn N. Drake , Warren A. Thaler , Edward N. Kresge , Chester W. Elspass , Albert J. Geiger , Vijay Swarup
IPC分类号： A01N25/26 , C05G3/00 , C08F8/36 , C08F8/44 , C05C9/00 , C08F210/16 , C05G3/02 , C05G5/00
CPC分类号： A01N25/26 , C05G3/0029 , C08F8/00 , C08F8/36 , C09D123/16 , C09D123/22 , C08F2800/10 , C08F2800/20 , C08F2810/20 , C08K3/0016
摘要： A composite comprising a urea substrate and ionically and covalently crosslinked, neutralized, sulfonated EPDM elastomeric coating encapsulating the urea.
摘要翻译：包含尿素底物和包封尿素的离子且共价交联的中和磺化EPDM弹性体涂层的复合材料。

8. 发明授权

US5110486A Breaker chemical encapsulated with a crosslinked elastomer coating 失效
标题翻译：破碎的化学品用交联的弹性体涂层包裹
公开(公告)号：US5110486A
公开(公告)日：1992-05-05
申请号：US676662
申请日：1991-03-28
申请人： Pacifico V. Manalastas , Evelyn N. Drake , Edward N. Kresge , Warren A. Thaler , Lee A. McDougall , John C. Newlove , Vijay Swarup , Albert J. Geiger
发明人： Pacifico V. Manalastas , Evelyn N. Drake , Edward N. Kresge , Warren A. Thaler , Lee A. McDougall , John C. Newlove , Vijay Swarup , Albert J. Geiger
IPC分类号： C09K8/62 , C09K8/92 , E21B43/26
CPC分类号： C09K8/92 , C09K8/62 , Y10S507/902 , Y10S507/921 , Y10S507/922 , Y10T428/2987
摘要： An encapsulated breaker chemical composition used in an oil or gas stimulation operation which comprises: a breaker chemical; and a pinhole free coating of an ionically and covalently crosslinked neutralized sulfonated elastomeric polyer of about 2 to about 80 microns thick deposited onto the surface of the breaker chemical, wherein said polymer encapsulates the breaker chemical, wherein the polymer is permeable to the breaker chemical and the polymer is non-reactive to the breaker chemical.
摘要翻译：一种用于油或气体刺激操作的包封的破碎剂化学组合物，其包括：破碎剂化学品; 以及沉积在破碎剂化学品表面上的约2至约80微米厚的离子和共价交联的中和的磺化弹性体聚合物的无针孔涂层，其中所述聚合物封装破碎剂化学品，其中聚合物对断路器化学品是可渗透的，并且该聚合物与断路器化学品无反应性。

9. 发明授权

US5187011A Composition comprising encapsulated substrate with thermoplastic polymer overcoating 失效
标题翻译：包含热塑性聚合物过滤的封装基材的组合物
公开(公告)号：US5187011A
公开(公告)日：1993-02-16
申请号：US819304
申请日：1992-01-09
申请人： Pacifico V. Manalastas , Evelyn N. Drake , Edward N. Kresge , Warren A. Thaler , Lee A. McDougall , John C. Newlove , Vijay Swarup , Albert J. Geiger
发明人： Pacifico V. Manalastas , Evelyn N. Drake , Edward N. Kresge , Warren A. Thaler , Lee A. McDougall , John C. Newlove , Vijay Swarup , Albert J. Geiger
IPC分类号： B32B27/00 , B32B27/06 , C09K8/60
CPC分类号： C09K8/60 , Y10T428/263 , Y10T428/2989 , Y10T428/2991 , Y10T428/2998 , Y10T428/31855 , Y10T428/31917
摘要： An encapsulated breaker chemical composition used in an oil or gas stimulation operation which comprises: a breaker chemical; and a pinhole free coating of an ionically and covalently crosslinked neutralized sulfonated elastomeric polymer of about 2 to about 80 microns thick deposited onto the surface of the breaker chemical, wherein said polymer encapsulates the breaker chemical, wherein the polymer is permeable to the breaker chemical and the polymer is non-reactive to the breaker chemical.
摘要翻译：一种用于油或气体刺激操作的包封的破碎剂化学组合物，其包括：破碎剂化学品; 以及沉积在破碎剂化学品表面上的约2至约80微米厚的离子和共价交联的中和磺化弹性体聚合物的无针孔涂层，其中所述聚合物封装破碎剂化学品，其中聚合物可渗透破碎剂化学品，该聚合物与断路器化学品无反应性。

10. 发明授权

US4788081A Biodegradable coatings of ionomer polymer 失效
公开(公告)号：US4788081A
公开(公告)日：1988-11-29
申请号：US151179
申请日：1988-02-01
申请人： Warren A. Thaler , Pacifico V. Manalastas , Evelyn N. Drake , Robert D. Lundberg
发明人： Warren A. Thaler , Pacifico V. Manalastas , Evelyn N. Drake , Robert D. Lundberg
IPC分类号： A01N25/10 , C08F8/30 , C08G81/02 , C09D123/32 , B05D7/00 , A01N25/00
CPC分类号： C08G81/024 , A01N25/10 , C08F8/44 , C09D123/32 , C08F2800/20
摘要： A polymeric composite comprising a (a) urea; (b) a coating of sulfonated polymer which has about 10 to about 200 meq. of sulfonate groups per 100 grams of said sulfonated polymer, said sulfonate groups being neutralized with a polycaprolactone polymer having the formula: ##STR1## wherein R.sub.1 or R.sub.2 is an alkyl, cycloalkyl or aryl group; R.sub.3, R.sub.4 and R.sub.5 are a hydrogen or alkyl, cycloalkyl, or aryl groups; m equals 1 to 20 and n equals 1 to 500, wherein said coating is deposited on the surface of said urea.

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