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1. 发明专利

JP2005074353A Method of preparing modified catalyst for manufacturing bisphenol a 审中-公开
标题翻译：制备改性催化剂制备双酚A的方法
公开(公告)号：JP2005074353A
公开(公告)日：2005-03-24
申请号：JP2003309606
申请日：2003-09-02
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： IWAHARA MASAHIRO , MASE ATSUSHI , MASUDA SHUICHI , SATO HIDEKI
IPC分类号： B01J31/08 , B01J31/10 , C07B61/00 , C07C37/20 , C07C39/16
CPC分类号： B01J31/08 , B01J2231/341 , C07C37/20 , C07C39/16
摘要： PROBLEM TO BE SOLVED: To provide a method of preparing a modified catalyst for manufacturing bisphenol A which causes no fracture of strongly acidic ion exchange resin, modifies the strongly acidic ion exchange resin uniformly and provides excellent catalyst performance.
SOLUTION: A modified catalyst for manufacturing bisphenol A is prepared by partially modifying the strongly acidic ion exchange resin with a sulfur-containing amine compound. The strongly acidic ion exchange resin is packed into a fixed bed reactor, to which a solution prepared by dissolving the sulfur-containing amine compound in an aqueous acid solution is filled. Subsequently, an aqueous acid solution similar to the above aqueous acid solution is filled and circulated in order to modify the strongly acidic ion exchange resin. The modification is performed until the concentration of the sulfur-containing amine compound in the aqueous acid solution at the outlet of the fixed bed reactor becomes uniform.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：为了提供制备双酚A的改性催化剂的方法，其不引起强酸性离子交换树脂的断裂，均匀地改性强酸性离子交换树脂并提供优异的催化剂性能。解决方案：通过用含硫胺化合物部分改性强酸性离子交换树脂制备用于制备双酚A的改性催化剂。将强酸性离子交换树脂填充到固定床反应器中，将通过将含硫胺化合物溶解在酸水溶液中而制备的溶液填充。随后，将与上述酸性水溶液相似的酸水溶液填充并循环，以改性强酸性离子交换树脂。进行修改，直到固定床反应器出口处的酸性水溶液中的含硫胺化合物的浓度变得均匀。版权所有（C）2005，JPO＆NCIPI

2. 发明专利

JP2007224010A Method for recovery of bisphenol a 有权
标题翻译：双酚A的回收方法
公开(公告)号：JP2007224010A
公开(公告)日：2007-09-06
申请号：JP2006288470
申请日：2006-10-24
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： KOHIRUMAKI JUN , MASUDA SHUICHI , KODAMA MASAHIRO , YOSHITOMI KAZUYUKI , YAMAZAKI HOKUTO
IPC分类号： C07C37/20 , C07C39/16
摘要： PROBLEM TO BE SOLVED: To provide a method for improving the recovering efficiency of bisphenol A in the production of bisphenol A by recovering powdery bisphenol A produced in a granulation step without extracting the powder from the system and efficiently utilizing the recovered powder as a product.
SOLUTION: In the production process of bisphenol A having a step to isomerize the total mother liquor, bisphenol A powder generated in a granulation step is recovered by heating and melting without extracting the powder from the system and the recovered bisphenol A is returned to at least one step before the granulation step of the bisphenol A production process.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：解决问题的方法：提供一种在双酚A生产中提高双酚A的回收效率的方法，通过回收在造粒步骤中生产的粉末状双酚A，而不从系统中提取粉末并有效利用回收的粉末作为一个产品。解决方案：在具有使总母液异构化的双酚A的制备方法中，在造粒步骤中产生的双酚A粉末通过加热和熔融回收，而不从体系中萃取出粉末并回收回收的双酚A 至双酚A制备方法的造粒步骤前至少一步。版权所有（C）2007，JPO＆INPIT

3. 发明专利

JP2007204433A Method for recovery of bisphenol-a and recovery equipment therefor 有权
标题翻译：二苯醚A及其回收设备的回收方法
公开(公告)号：JP2007204433A
公开(公告)日：2007-08-16
申请号：JP2006025720
申请日：2006-02-02
申请人： Idemitsu Kosan Co Ltd , Tsukishima Kikai Co Ltd , 出光興産株式会社 , 月島機械株式会社
发明人： YOSHITOMI KAZUYUKI , KODAMA MASAHIRO , MASUDA SHUICHI , TAKEGAMI KEIZO , SUDA HIDEKI
IPC分类号： C07C37/84 , C07C39/16
CPC分类号： C07C37/84 , B01D9/0013 , B01D9/005 , C07B63/00 , C07C39/16
摘要： PROBLEM TO BE SOLVED: To provide a method for recovery of bisphenol-A and a recovery equipment therefor.
SOLUTION: In the bisphenol-A recovery step from the isomerization treatment solution, the isomerization-treated solution is fed to an outer-jacketed crystallizer in the presence of phenol. Simultaneously, cooling water is allowed to flow through the outer jacket to crystallize the adduct of bisphenol-A and phenol in the presence of phenol in the recovery equipment.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供回收双酚A的方法及其回收设备。解决方案：在来自异构化处理溶液的双酚-A回收步骤中，异构化处理的溶液在苯酚存在下进料到外包层结晶器中。同时，允许冷却水流过外套，在回收设备中在苯酚存在下使双酚A和苯酚的加合物结晶。版权所有（C）2007，JPO＆INPIT

4. 发明专利

JP2007196171A Method and equipment for treating phenol-containing water 有权
标题翻译：用于处理含酚水的方法和设备
公开(公告)号：JP2007196171A
公开(公告)日：2007-08-09
申请号：JP2006019785
申请日：2006-01-27
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： YOSHITOMI KAZUYUKI , MASUDA SHUICHI , KODAMA MASAHIRO
IPC分类号： C02F1/04 , B01D3/36
CPC分类号： B01D3/36 , B01D3/4216 , C02F1/048 , C02F2101/322 , C02F2103/36
摘要： PROBLEM TO BE SOLVED: To provide a method and equipment for treating phenol-containing water, in each of which the operation of an azeotropic distillation column is controlled by monitoring the phenol concentration in the waste water to be discharged from a settler arranged in the top part of the azeotropic distillation column and finding out the fluctuation of the phenol concentration in the waste water in early stages to stably keep low the phenol concentration in the waste water without using liquid-liquid extraction equipment (an extractive distillation column) or the like on the downstream side of the azeotropic distillation column, in the azeotropic distillation column in which phenol-containing water is treated by azeotropic distillation using an azeotropic agent for forming an azeotrope with water.
SOLUTION: An automatic gas chromatography apparatus 7 is arranged on a waste water line from the settler tank 3 arranged in the top part of the azeotropic distillation column 1 in which phenol-containing water is treated by azeotropic distillation using the azeotropic agent for forming the azeotrope with water. The phenol concentration in the waste water is continuously measured and monitored by the automatic gas chromatography apparatus 7 to control the operation of the azeotropic distillation column 1.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：待解决的问题：提供一种处理含苯酚的水的方法和设备，其中共沸蒸馏塔的操作通过监测排出的沉降器排出的废水中的苯酚浓度来控制在共沸蒸馏塔的顶部，发现早期废水中苯酚浓度的波动，在不使用液 - 液萃取设备（萃取蒸馏塔）的条件下稳定地降低废水中的苯酚浓度，或者在共沸蒸馏塔的共沸蒸馏塔中，使用共沸剂与水共沸来共沸蒸馏处理含苯酚的水。解决方案：自动气相色谱装置7设置在设置在共沸蒸馏塔1的顶部的沉降池3的废水管线上，其中通过共沸蒸馏处理含苯酚的水，使用共沸剂与水形成共沸物。通过自动气相色谱装置7连续测量和监测废水中的苯酚浓度，以控制共沸蒸馏塔1的操作。（C）2007，JPO＆INPIT

5. 发明专利

JP2005074332A Method of preparing modified catalyst for manufacturing bisphenol a 有权
标题翻译：制备改性催化剂制备双酚A的方法
公开(公告)号：JP2005074332A
公开(公告)日：2005-03-24
申请号：JP2003308990
申请日：2003-09-01
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： IWAHARA MASAHIRO , MASE ATSUSHI , MASUDA SHUICHI , SATO HIDEKI
IPC分类号： B01J31/08 , B01J31/10
CPC分类号： B01J31/08 , B01J2231/347
摘要： PROBLEM TO BE SOLVED: To provide a method of preparing a modified catalyst for manufacturing bisphenol A which causes no fracture of strongly acidic ion exchange resin, modifies the strongly acidic ion exchange resin uniformly and provides excellent catalyst performance. SOLUTION: A modified catalyst for manufacturing bisphenol A is prepared by partially modifying the strongly acidic ion exchange resin with a sulfur-containing amine compound. The strongly acidic ion exchange resin is packed into a fixed bed reactor, to which an aqueous acid solution and the sulfur-containing amine compound of such a concentration as to be in equilibrium with the aqueous acid solution are filled and, thereby, the strongly acidic ion exchange resin is modified. COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：为了提供制备双酚A的改性催化剂的方法，其不引起强酸性离子交换树脂的断裂，均匀地改性强酸性离子交换树脂并提供优异的催化剂性能。解决方案：通过用含硫胺化合物部分改性强酸性离子交换树脂制备用于制备双酚A的改性催化剂。将强酸性离子交换树脂填充到固定床反应器中，将酸水溶液和浓度与酸水溶液平衡的含硫胺化合物填充到其中，由此强酸性离子交换树脂被改性。版权所有（C）2005，JPO＆NCIPI

6. 发明专利

JP2007308408A Method and apparatus for manufacturing high purity bisphenol a 有权
标题翻译：制备高纯度双酚A的方法和装置
公开(公告)号：JP2007308408A
公开(公告)日：2007-11-29
申请号：JP2006138103
申请日：2006-05-17
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： YOSHITOMI KAZUYUKI , KODAMA MASAHIRO , MASUDA SHUICHI , KOHIRUMAKI JUN , YAMAZAKI HOKUTO
IPC分类号： C07C37/20 , B01D9/02 , C07B61/00 , C07C37/84 , C07C39/16
CPC分类号： C07C37/20 , B01D9/0059 , C07C37/00 , C07C37/84 , C07C37/86 , C07C39/16
摘要： PROBLEM TO BE SOLVED: To provide a method of manufacturing a bisphenol A superior in transparency or hue.
SOLUTION: The processes for manufacturing the bisphenol A comprises a condensation reaction process (A) of phenol and acetone in the presence of an acid catalyst; a concentration process (B) of the reaction mixture; a crystallization/solid-liquid separation process (C) for separating an adduct of bisphenol A and phenol from a mother liquor; an isomerization process (D) for isomerizing the whole of the mother liquor with an isomerizing catalyst, and circulating the isomerized liquid to the process (A) and/or the process (B); also at need, a recovery process (E) for recovering the adduct of bisphenol A and phenol from a part of the isomerized liquid treated in the process (D); an adduct decomposing process (F) for removing phenol from the adduct obtained in the process (C) to make a bisphenol A melt; and a granulation process (G) for granulating the bisphenol A melt to be a product prill, wherein a free acid removing process is provided in the process (D) for removing a free acid existing in the mother liquor or the isomerized liquid.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种制造透明度或色相优异的双酚A的方法。解决方案：制备双酚A的方法包括在酸催化剂存在下苯酚和丙酮的缩合反应方法（A）; 反应混合物的浓缩方法（B）; 用于从母液中分离双酚A和苯酚的加合物的结晶/固液分离方法（C）; 异构化方法（D），用异构化催化剂使整个母液异构化，并将异构化的液体循环到方法（A）和/或方法（B）; （D）中处理的部分异构化液体中回收双酚A和苯酚的加合物的回收方法（E）; 用于从方法（C）中得到的加合物中除去苯酚以使双酚A熔融的加合物分解方法（F）以及用于将双酚A熔体造粒为产品颗粒的造粒方法（G），其中在用于除去存在于母液或异构化液体中的游离酸的方法（D）中提供游离酸去除方法。版权所有（C）2008，JPO＆INPIT

7. 发明专利

JP2007217301A Method for producing bisphenol a 有权
标题翻译：生产双酚A的方法
公开(公告)号：JP2007217301A
公开(公告)日：2007-08-30
申请号：JP2006036829
申请日：2006-02-14
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： YOSHITOMI KAZUYUKI , KODAMA MASAHIRO , MASUDA SHUICHI
IPC分类号： C07C37/48 , C07B61/00 , C07C37/20 , C07C39/16
CPC分类号： C07C37/84 , C07C37/00 , C07C37/20 , C07C37/685 , C07C37/70 , C07C37/74 , C07C37/86 , C07C39/16
摘要： PROBLEM TO BE SOLVED: To provide a method for producing bisphenol A in a good efficiency by extending the life of an isomerization reaction catalyst in the production method of the bisphenol A, having the isomerization reaction process.
SOLUTION: This method for producing the bisphenol A is provided by setting 0.2 to 0.9 mass% water concentration of liquid containing bis(hydroxyphenyl)propanes in the case of isomerizing the bis(hydroxyphenyl)propanes other than the bisphenol A [2,2-bis(4-hydroxyphenyl)propane], to the bisphenol A by making the liquid containing the bis(hydroxyphenyl)propanes in contact with a strongly acidic cation exchange resin.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：解决的问题：通过在具有异构化反应方法的双酚A的制备方法中延长异构化反应催化剂的寿命，提供一种以高效率生产双酚A的方法。解决方案：制备双酚A的方法是通过在除双酚A以外的双（羟基苯基）丙烷异构化的情况下，通过设定含有双（羟基苯基）丙烷的液体的0.2〜0.9质量％的水分浓度[ 通过使含有双（羟基苯基）丙烷的液体与强酸性阳离子交换树脂接触，向双酚A施加2-双（4-羟基苯基）丙烷]。版权所有（C）2007，JPO＆INPIT

8. 发明专利

JP2007197391A Method for producing bisphenol a prill 审中-公开
标题翻译：生产双酚A的方法
公开(公告)号：JP2007197391A
公开(公告)日：2007-08-09
申请号：JP2006019790
申请日：2006-01-27
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： YOSHITOMI KAZUYUKI , MASUDA SHUICHI , KODAMA MASAHIRO
IPC分类号： C07C37/70 , C07C39/16
CPC分类号： C07C37/70 , C07C37/20 , C07C37/685 , C07C37/74 , C07C37/84 , C07C37/86 , C07C39/16
摘要： PROBLEM TO BE SOLVED: To provide a method for continuously producing high-quality bisphenol A prill in good efficiency and stably for a long period by solving problems such as the reduction of heat conductivity by the formation of an attachment at a heat exchanger in a granulation process, and the increase of differential pressure by the formation of the attachment at a granulation column or the heat exchanger when producing the the bisphenol A prill from the molten bisphenol A.
SOLUTION: The method for producing the bisphenol A prill involves regulating the concentration of phenol in a circulation gas so as to be ≤50 vol. ppm when producing the bisphenol A prill from the molten bisphenol A by using a granulation apparatus having the granulation column for granulating the molten bisphenol A by spraying the molten bisphenol A and bringing the sprayed bisphenol A into contact with the circulation gas, a powder-removing installation for removing the powder of the bisphenol A in the circulation gas, a circulation gas cooler for regulating the temperature of the circulation gas, and a blower for circulating the circulation gas.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：待解决的问题：提供一种通过解决诸如通过在热交换器上形成附件而导致的导热性降低的问题而长时间连续生产高品质双酚A颗粒的方法。在造粒过程中，以及当从熔融双酚A制备双酚A颗粒时，通过在造粒塔或热交换器处形成附着物而产生的压差增加。解决方案：双酚A的制备方法颗粒包括调节循环气体中酚的浓度，使其≤50体积。通过使用具有造粒塔的造粒装置，通过喷雾熔融的双酚A并使喷雾的双酚A与循环气体接触来制造熔融双酚A的造粒装置，从熔融的双酚A制备双酚A颗粒，用于除去循环气体中的双酚A的粉末的装置，用于调节循环气体的温度的循环气体冷却器和用于循环循环气体的鼓风机。版权所有（C）2007，JPO＆INPIT

9. 发明专利

JP2007112763A Method for producing bisphenol a having good hue 审中-公开
标题翻译：用于生产具有良好色泽的双酚A的方法
公开(公告)号：JP2007112763A
公开(公告)日：2007-05-10
申请号：JP2005307650
申请日：2005-10-21
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： YOSHITOMI KAZUYUKI , KODAMA MASAHIRO , MASUDA SHUICHI , KOHIRUMAKI JUN , YAMAZAKI HOKUTO
IPC分类号： C07C37/20 , C07B61/00 , C07C39/16
CPC分类号： C07C37/20 , C07C37/84 , C07C37/86 , C07C39/16
摘要： PROBLEM TO BE SOLVED: To provide a production method for profitably producing bisphenol A having a good hue in an apparatus for producing the bisphenol A from phenol and acetone. SOLUTION: This method for producing the bisphenol A having the good hue is characterized by using molybdenum-containing stainless steel as a metal material for portions contacting with reaction mixtures after (4) an adduct-decomposing process, controlling the liquid phase portions of a raw material system and reaction products to ≤180°C, and controlling the temperature of a thermal medium for heating them to ≤200°C, in the apparatus for producing the bisphenol A, comprising (1) a condensation reaction process for condensation-reacting an excessive amount of phenol with acetone, (2) a concentration process, (3) a crystallization/solid-liquid separation process, (4) an adduct-decomposing process, and (5) a granulation process. COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：解决问题的方法：提供一种在苯酚和丙酮生产双酚A的设备中有利地生产具有良好色调的双酚A的生产方法。解决方案：用于生产具有良好色调的双酚A的方法的特征在于，使用含钼不锈钢作为金属材料，用于在（4）加合分解过程之后与反应混合物接触的部分，控制液相部分的原料系统和反应产物至≤180℃，并且在用于生产双酚A的设备中控制将其加热至≤200℃的热介质的温度，包括（1）冷凝缩合反应方法 - 用丙酮反应过量的苯酚，（2）浓缩过程，（3）结晶/固液分离过程，（4）加合物分解过程，和（5）造粒过程。版权所有（C）2007，JPO＆INPIT

10. 发明专利

JP2007112762A Method for producing bisphenol a and method for judging ion exchange resin 审中-公开
标题翻译：用于生产双酚A的方法和用于判断离子交换树脂的方法
公开(公告)号：JP2007112762A
公开(公告)日：2007-05-10
申请号：JP2005307649
申请日：2005-10-21
申请人： Idemitsu Kosan Co Ltd , 出光興産株式会社
发明人： YOSHITOMI KAZUYUKI , KODAMA MASAHIRO , MASUDA SHUICHI , KOHIRUMAKI JUN , YAMAZAKI HOKUTO
IPC分类号： C07C37/20 , C07B61/00 , C07C39/16
CPC分类号： C07C37/20 , C07C39/16
摘要： PROBLEM TO BE SOLVED: To provide a method for producing bisphenol A, comprising condensing phenol with acetone in the presence of a strong acid type ion exchange resin catalyst to produce the bisphenol A, wherein a high quality strong acid type ion exchange resin not flowing out a left sulfonic acid is selected to stably produce the bisphenol A having a good hue.
SOLUTION: This method for producing the bisphenol A, comprising condensing phenol with acetone in the presence of a strong acid type ion exchange resin catalyst, is characterized by using a strong acid type ion exchange resin giving drained water having ≥5 pH at 25°C, when deionized water is passed through the strong acid type ion exchange resin in a volume of 3 volume times that that of the ion exchange resin at 25°C at a LHSV (liquid hour space velocity) of 1.0 hr
-1 .
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：解决问题的方案：提供一种双酚A的制造方法，其特征在于，在强酸型离子交换树脂催化剂的存在下，使苯酚与丙酮缩合生成双酚A，其中，优质强酸型离子交换树脂选择不流出左磺酸以稳定地生产具有良好色调的双酚A。解决方案：在强酸型离子交换树脂催化剂的存在下，使苯酚与丙酮缩合的双酚A的制造方法的特征在于使用强酸型离子交换树脂，得到≥5个pH的排水 25℃，当离子交换树脂以25℃的3倍体积倍的离子交换树脂以1.0小时的LHSV（液时空速）通过强酸型离子交换树脂时， -1 。版权所有（C）2007，JPO＆INPIT

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