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1. 发明授权

US3849503A Diphenylethers having herbicidal properties 失效
标题翻译：具有除草性能的二苯醚
公开(公告)号：US3849503A
公开(公告)日：1974-11-19
申请号：US31715572
申请日：1972-12-21
申请人： ISHIHARA MINING & CHEMICAL CO
发明人： YOKOMICHI I , KIMURA F , TAKAGI H , NASU R , TAKAHASHI R , TOKI T , SHIGEHARA I , NISHIYAMA R , SOMEYA S
IPC分类号： C07C6/12 , C07C7/13 , C07C205/38 , C07C43/20
CPC分类号： C07C6/126 , C07C7/13 , C07C201/12 , C07C15/02 , C07C205/38
摘要： 1. A PROCESS FOR PRODUCING A DIPHENYLETHER HAVING THE GENERAL FORMULA:

Y-(3-X,Z-1,4-PHENYLENE)-O-(3-(R-O-)-1,4-PHENYLENE)-NO2

WHEREIN X REPRESENTS A HALOGEN ATOM OR A METHYL RADICAL IN THE 2-POSITION; Y REPRESENTS A HALOGEN ATOM OR AN ALKYL RADICAL HAVING UP TO 3 CARBON ATOMS IN THE 4-POSITION; Z REPRESENTS HYDROGEN OR HALOGEN IN THE 5- AND 6POSITIONS, WHEREIN BOTH THE 5- AND 6-POSITIONS MAY BE HYDROGEN, BUT ONLY ONE OF THE 5- OR 6-POSITIONS MAY BE HALOGEN; AND R REPRESENTS A SATURATED OR AN UNSATURATED HYDROCARBON HAVING UP TO 3 CARBON ATOMS, METHOXYETHYL OR AN ETHOXYETHYL RADICAL, WHICH COMPRISES REACTING IN THE PRESENCE OF AN ALKALI METHYL HYDROXIDE OR CARBONATE A 2,4-DIHALONITROBENZENE HAVING THE GENERAL FORMULA:

1-(O2N-),2,4-DI(HAL-)-BENZENE

WHEREIN HAL IS A HALOGEN ATOM, WITH A SUBSTITUTED PHENOL HAVING THE GENERAL FORMULA:

Y-(3-X,Z-1,4-PHENYLENE)-O-(4-(O2N-)-1,3-PHENYLENE)-O-

2-X,4-Y,Z-PHENOL WHEREIN THE MOLAR RATIO OF THE PHENOL TO THE 2,4-DIHALONITROBENZENE IS AT LEAST 2:1, AT A TEMPERATURE OF FROM 130* C. TO 160* C. TO PRODUCE A 2,4-BIS(SUBSTITUTED PHENOXY) NITRO BENZENE HAVING THE GENERAL FORMULA: 1-(O2N-),2,4-BIS((2-X,4-Y,Z-PHENYL)-O-)BENZENE THEN REACTING SAID 2,4-BIS(SUBSTITUTED PHENOXY) NITROBENZENE (IV) IN THE PRESENCE OF AN ALKALI METAL HYDROXIDE WITH AN ALCOHOL OF THE FORMULA ROH WHEREIN R IS AS DEFINED ABOVE AT A TEMPERATURE OF 20-100* C. TO PRODUCE SAID DIPHENYLETHER (I) AND A SUBSTITUTED PHENOL (III) AND THEREAFTER ISOLATING SAID DIPHENYLETHER (I).

2. 发明授权

US3755366A Piperonyl carbamate herbicides 失效
标题翻译： PIPERONYL CARBAMATE除草剂
公开(公告)号：US3755366A
公开(公告)日：1973-08-28
申请号：US3755366D
申请日：1971-02-22
申请人： ISHIHARA MINING & CHEMICAL CO
发明人： NISHIYAMA R , TOKI T , TAKAHASHI R , HAGA T
IPC分类号： A01N47/12 , C07D317/56 , C07D317/62 , C07D13/10
CPC分类号： C07D317/62 , C07D317/56 , Y10S514/937 , Y10S514/951
摘要： HERBICIDES, HAVING THE GENERAL FORMULA:

5-((R)2-N-C(=X)-S-CH2-),6-Y-1,3-BENZODIOXOLE

WHEREIN X REPRESENTS OXYGEN OR SULFUR; Y REPRESENTS HYDROGEN OR HALOGEN AND R REPRESENTS A LOWER ALKYL GROUP, HAVE BEEN PREPARED AND HAVE BEEN FOUND TO POSSESS REMARKABLE SELECTIVE GROWTH CONTROLLING PROPERTIES.

3. 发明专利

SE7511634L 未知
公开(公告)号：SE7511634L
公开(公告)日：1976-04-18
申请号：SE7511634
申请日：1975-10-16
申请人： ISHIHARA MINING & CHEMICAL CO
发明人： TAKAHASHI R , FUJIKAWA K , YOKOMICHI I , TSUJII Y , SAKASHITA N
IPC分类号： A01N39/02 , A01P13/02 , C07D213/63 , C07D213/64 , C07D213/643 , C07D213/75 , C07D521/00 , A01N43/40
摘要： 1491274 α - [4 - (5 - mono-substituted or 3,5 - di - substituted - pyridyl - 2 - oxy)phenoxy]- alkanecarboxylic acid derivatives ISHIHARA SANGYO KAISHA Ltd 10 Oct 1975 [17 Oct 1974 13 March 1975] 41560/75 Heading C2C Novel α - [4 - (5 - mono-substituted or 3,5 - di - substituted - pyridyl - 2 - oxy)- phenoxy] - alkanecarboxylic acid derivatives of the formula wherein X is a halogen atom; Y is a hydrogen atom, a halogen atom or a methyl group; R is a hydrogen atom or a straight or branched chain (C 1 -C 6 ) alkyl group; and R 1 is a hydroxy group; a (C 1 -C 9 ) alkoxy group in which the alkyl moiety thereof may have a straight or a branched chain and may be substituted with one or more of a halogen atom or a hydroxy group; an -(OC 2 H 4 ) n -O- (C 1 -C 4 ) alkyl group in which the alkyl moiety thereof may have a straight or a branched chain and n is 1, 2, 3, 4 or 5; a (C 1 -C 4 ) alkylthio group in which the alkyl moiety thereof may have a straight or a branched chain; a (C 2 -C 4 ) alkenyloxy group; a cyclohexyloxy group in which the cyclohexyl moiety thereof may be substituted with one or more of a halogen atom or a methyl group; a phenoxy group in which the aryl moiety thereof may be substituted with one or more of a halogen atom or a methyl group; a phenylthio group in which the aryl moiety thereof may be substituted with one or more of a halogen atom or a methyl group; a benzyloxy group in which the aryl moiety thereof may be substituted with one or more of a halogen atom or a methyl group; an amino group which may be substituted with one or more of a (C 1 -C 4 ) alkyl group in which the alkyl moiety thereof may have a straight or a branched chain and may be substituted with a hydroxy group; a mono-(C 1 -C 4 ) alkylamino group in which the alkyl moiety thereof may have a straight or a branched chain and is substituted with a -COOR 4 group in which R 4 is a hydrogen atom, a cation or a straight or branched chain (C 1 -C 4 ) alkyl group; an anilino group in which the aryl moiety thereof may be substituted with one or more of a halogen atom or a methyl group; a benzylamino group; an amino group substituted with a heterocyclic group in which the heterocyclic moiety thereof may be substituted with one or more of a halogen atom or a methyl group; a morpholino group; a piperidino group; an -OM group where M is a cation; or a halogen atom, are prepared by reacting a substituted pyridine of the formula with a substituted phenol of the formula wherein Z is a hydroxy group; a (C 1 -C 5 ) alkoxy group or a group of the formula wherein R 3 is a hydroxy group; a (C 1 -C 9 ) alkoxy group or an amino group, in the presence of an alkaline material in an amount of from 1 to 1À2 moles per mole of compound III at a temperature of at least 50‹ C. for 1 to 20 hours to give a substituted pyridyl phenyl ether of the formula and, when Z is other than optionally dealkylating the compound of Formula IV and reacting this compound with an α-haloalkanecarboxylic acid or a derivative thereof having the formula in the presence of an alkaline material in an amount of from 1 to 1À2 moles per mole of compound IV to give a compound of the formula and optionally converting the R 3 moiety into R 1 . The novel compounds possess herbicidal properties.

5. 发明专利

SE7508206L 未知
公开(公告)号：SE7508206L
公开(公告)日：1976-01-19
申请号：SE7508206
申请日：1975-07-17
申请人： ISHIHARA MINING & CHEMICAL CO
发明人： TAKAHASHI R , FUJIKAWA K , YOKOMICHI I , SOMEYA S , SAKASHITA N
IPC分类号： A01N39/02 , A01N43/40 , A01N43/647 , A01N43/653 , A01N47/34 , A01N53/08 , C07C51/367 , C07C51/41 , C07C59/68 , C07C59/70 , C07C69/65 , C07C69/712 , C07C69/76 , C07C233/00 , C07C233/02 , C07C275/50 , C07C327/22 , C07D213/64 , C07D213/75 , C07D249/14 , C07D295/185 , C07D295/32 , C07D521/00 , C07C59/25
摘要： alpha -[4-(4-Trifluoromethylphenoxy)phenoxy]alkanecarboxylic acids (the "4-trifluoromethylphenoxy group" of which may contain one chlorine atom as a substituent) and derivatives thereof useful as a herbicide, a herbicidal composition containing the compound, methods of controlling weeds and production thereof.

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