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1. 发明申请

WO2009122023A3 MESOSTRUCTURED MATERIAL HAVING A HIGH ALUMINIUM CONTENT AND COMPOSED OF SPHERICAL PARTICLES OF SPECIFIC SIZE 审中-公开
标题翻译：具有高铝含量并由特定尺寸的球形颗粒组成的多晶结构材料
公开(公告)号：WO2009122023A3
公开(公告)日：2009-11-26
申请号：PCT/FR2009000210
申请日：2009-02-26
申请人： INST FRANCAIS DU PETROLE , CHAUMONNOT ALEXANDRA , COUPE AURELIE , SANCHEZ CLEMENT , BOISSIERE CEDRIC , MARTIN MICHEL
发明人： CHAUMONNOT ALEXANDRA , COUPE AURELIE , SANCHEZ CLEMENT , BOISSIERE CEDRIC , MARTIN MICHEL
IPC分类号： C01B39/00 , C01B37/00 , C01B39/04
CPC分类号： C01B39/04 , C01B37/00 , C01B39/00
摘要： A mesostructured material is described that is composed of at least two elementary spherical particles, each of said particles comprising a mesostructured matrix based on aluminium oxide, said matrix having a pore diameter between 1.5 and 30 nm and an aluminium oxide content that represents more than 46% by weight relative to the weight of said matrix, which matrix has amorphous walls of thickness between 1 and 30 nm, said elementary spherical particles having a diameter D greater than 10 µm and less than or equal to 100 µm (10 100). Said mesostructured matrix may also contain silicon oxide. Each of the spherical particles of the mesostructured material may also contain zeolite nanocrystals so as to form a material having a mixed porosity of both mesostructured and zeolitic nature. The preparation of said material is also described.
摘要翻译：描述了由至少两个基本球形颗粒组成的介孔结构材料，每个所述颗粒包含基于氧化铝的介孔结构基质，所述基质具有1.5-30nm的孔直径和代表大于46的氧化铝含量所述基质具有厚度在1和30nm之间的无定形壁，所述基本球形颗粒的直径D大于10μm并且小于或等于100μm（10 100）。所述介孔结构化基质还可以含有氧化硅。介孔结构材料的每个球形颗粒还可以含有沸石纳米晶体，从而形成具有介孔结构和沸石性质的混合孔隙率的材料。还描述了所述材料的制备。

2. 发明申请

WO2009056710A3 AMORPHOUS MATERIAL HAVING A HIERARCHISED POROSITY AND COMPRISING SILICON 审中-公开
标题翻译：具有分层孔隙和包含硅的非晶材料
公开(公告)号：WO2009056710A3
公开(公告)日：2009-07-30
申请号：PCT/FR2008001198
申请日：2008-08-18
申请人： INST FRANCAIS DU PETROLE , CHAUMONNOT ALEXANDRA , COUPE AURELIE , SANCHEZ CLEMENT , BOISSIERE CEDRIC
发明人： CHAUMONNOT ALEXANDRA , COUPE AURELIE , SANCHEZ CLEMENT , BOISSIERE CEDRIC
IPC分类号： C01B37/00 , B01J21/06 , B01J29/00 , B01J29/06 , B01J37/00 , C01B33/113 , C01B37/02 , C01B39/00
CPC分类号： C01B39/00 , B01J20/0288 , B01J20/18 , B01J20/28019 , B01J20/28057 , B01J20/2808 , B01J20/28083 , B01J20/28085 , B01J20/28092 , B01J21/08 , B01J21/12 , B01J29/035 , B01J29/08 , B01J29/40 , B01J29/7007 , B01J35/1061 , B01J35/1066 , B01J35/109 , B01J37/0045 , B01J37/033 , C01B37/00 , C01B37/02 , C07C4/18 , Y02P20/52 , Y10T428/2982 , C07C15/04 , C07C11/06
摘要： The invention relates to a material having a hierarchised porosity and consisting of at least two elementary spherical particles having a maximum diameter of 200 microns, at least one of said spherical particles comprising at least one matrix based on silicon oxide. Said material has a macroporous volume measured by mercury porosimetry of between 0.05 and 1 ml/g, a mesoporous volume measured by nitrogen volumetry of between 0.03 and 0.4 ml/g, and the matrix comprises amorphous walls. The invention also relates to the preparation of the material.
摘要翻译：本发明涉及一种具有等级孔隙率并由至少两个最大直径为200微米的基本球形颗粒组成的材料，至少一种所述球形颗粒包含至少一种基于氧化硅的基体。所述材料具有通过0.05至1ml / g的水银孔率法测量的大孔体积，通过氮体积测量的介孔体积为0.03至0.4ml / g，并且所述基质包括非晶壁。本发明还涉及材料的制备。

3. 发明申请

WO2009122022A3 MESOSTRUCTURED ALUMINOSILICATE MATERIAL FORMED FROM SPHERICAL PARTICLES OF SPECIFIC SIZE 审中-公开
标题翻译：由特定尺寸的球形颗粒形成的结构化的铝酸盐材料
公开(公告)号：WO2009122022A3
公开(公告)日：2009-12-10
申请号：PCT/FR2009000209
申请日：2009-02-26
申请人： INST FRANCAIS DU PETROLE , CHAUMONNOT ALEXANDRA , COUPE AURELIE , SANCHEZ CLEMENT , BOISSIERE CEDRIC , MARTIN MICHEL
发明人： CHAUMONNOT ALEXANDRA , COUPE AURELIE , SANCHEZ CLEMENT , BOISSIERE CEDRIC , MARTIN MICHEL
IPC分类号： C01B39/04 , B01J29/04 , B01J35/02 , B01J35/10
CPC分类号： C01B39/04 , B01J20/18 , B01J20/28004 , B01J20/28019 , B01J20/28057 , B01J20/28083 , B01J21/12 , B01J29/041 , B01J35/1057 , B01J35/1061 , B01J35/109 , Y10T428/2991 , Y10T428/2993
摘要： A mesostructured aluminosilicate material is described that is composed of at least two elementary spherical particles, each of said spherical particles being composed of a matrix based on silicon oxide and aluminium oxide, said matrix having a pore diameter between 1.5 and 30 nm, an Si/Al molar ratio at least equal to 1 and having amorphous walls of thickness between 1 and 30 nm, said elementary spherical particles having a diameter D such that 10
摘要翻译：描述了由至少两个基本球形颗粒组成的介孔结构的硅铝酸盐材料，每个所述球形颗粒由基于氧化硅和氧化铝的基体组成，所述基体的孔径在1.5至30nm之间，Si / Al摩尔比至少等于1，并且具有1至30nm厚度的非晶壁，所述基本球形颗粒的直径D使得10

4. 发明申请

WO2009060143A2 CRYSTALLISED MATERIAL WITH HIERARCHISED POROSITY AND CONTAINING SILICON 审中-公开
标题翻译：具有分层孔隙度和含硅的结晶材料
公开(公告)号：WO2009060143A2
公开(公告)日：2009-05-14
申请号：PCT/FR2008001215
申请日：2008-08-29
申请人： INST FRANCAIS DU PETROLE , CHAUMONNOT ALEXANDRA , COUPE AURELIE , SANCHEZ CLEMENT , BOISSIERE CEDRIC
发明人： CHAUMONNOT ALEXANDRA , COUPE AURELIE , SANCHEZ CLEMENT , BOISSIERE CEDRIC
IPC分类号： C01B37/02 , B01J20/02 , B01J21/06 , B01J29/00 , B01J29/06 , B01J37/00 , C01B33/113 , C01B37/00 , C01B39/00
CPC分类号： C01B37/00 , B01J20/18 , B01J20/28019 , B01J20/28057 , B01J20/2808 , B01J20/28083 , B01J20/28085 , B01J21/08 , B01J21/12 , B01J29/035 , B01J29/084 , B01J29/40 , B01J29/7007 , B01J35/1057 , B01J35/1061 , B01J35/1066 , B01J35/1095 , B01J37/0045 , B01J37/10 , C01B37/02 , C01B39/00
摘要： The invention relates to a material having a hierarchised porosity and made of at least two elementary spherical particles having a maximum diameter of 200 microns, at least one of said spherical particles including at least one matrix containing silicon oxide and having crystallised walls, wherein said material has a macroporous volume as measured by mercury porosimetry of between 0.05 and 1 ml/g, and a mesoporous volume as measured by nitrogen volumetric analysis of between 0.03 and 0.4 ml/g. The invention also relates to the preparation of this material and to the use thereof as an adsorbent or an acidic solid.
摘要翻译：本发明涉及一种具有层状孔隙率并由至少两个最大直径为200微米的基本球形颗粒制成的材料，至少一种所述球形颗粒包括至少一种含有氧化硅的基质并具有结晶的壁，其中所述材料具有通过0.05至1ml / g的水银孔隙率法测量的大孔体积，以及通过0.03至0.4ml / g的氮气体积分析测量的介孔体积。本发明还涉及该材料的制备及其作为吸附剂或酸性固体的用途。

5. 发明申请

WO2009056711A3 AMORPHOUS MATERIAL COMPRISING SILICON AND HAVING AN ORGANISED AND HIERARCHISED POROSITY 审中-公开
标题翻译：包含硅并具有组织和分级孔隙的非晶态材料
公开(公告)号：WO2009056711A3
公开(公告)日：2009-07-30
申请号：PCT/FR2008001199
申请日：2008-08-19
申请人： INST FRANCAIS DU PETROLE , CHAUMONNOT ALEXANDRA , PEGA STEPHANIE , SANCHEZ CLEMENT , BOISSIERE CEDRIC
发明人： CHAUMONNOT ALEXANDRA , PEGA STEPHANIE , SANCHEZ CLEMENT , BOISSIERE CEDRIC
IPC分类号： C01B37/02 , C01B33/46 , C01B39/02
CPC分类号： C01B37/02 , C01B33/46 , C01B39/02 , Y10T428/2982 , Y10T428/2991 , Y10T428/2993
摘要： The invention relates to a material having a hierarchised porosity and consisting of at least two elementary spherical particles. Each of said particles comprises a mesostructured matrix based on silicon oxide, the diameter of the mesopores being between 1.5 and 30 nm, and amorphous and microporous walls having a thickness of between 1.5 and 50 nm, the elementary spherical paricules having a maximum diameter of 200 microns. The matrix based on silicon oxide can contain aluminium. The invention also relates to the preparation of said material.
摘要翻译：本发明涉及具有分级孔隙率并由至少两个初级球形颗粒组成的材料。每个所述颗粒包含基于氧化硅的介孔结构基质，介孔的直径介于1.5和30nm之间，以及非晶和微孔介质的厚度介于1.5和50nm之间，基本球形介质的最大直径为200 微米。基于氧化硅的基质可以包含铝。本发明还涉及所述材料的制备。

6. 发明申请

WO2009060144A3 CRYSTALLISED MATERIAL CONTAINING SILICON WITH HIERARCHISED AND ORGANISED POROSITY 审中-公开
标题翻译：含有结晶硅和有机硅多孔结晶材料
公开(公告)号：WO2009060144A3
公开(公告)日：2009-07-30
申请号：PCT/FR2008001216
申请日：2008-08-29
申请人： INST FRANCAIS DU PETROLE , CHAUMONNOT ALEXANDRA , PEGA STEPHANIE , SANCHEZ CLEMENT , BOISSIERE CEDRIC
发明人： CHAUMONNOT ALEXANDRA , PEGA STEPHANIE , SANCHEZ CLEMENT , BOISSIERE CEDRIC
IPC分类号： C01B37/00 , C01B37/02 , C01B39/00
CPC分类号： C01B37/005 , C01B37/02 , C01B39/00
摘要： The invention relates to a material having a hierarchised and organised porosity in terms of microporosity and mesoporosity, that comprises at least two elementary spherical particles, each of said particles including a meso-structured silicon-oxide-containing matrix having a mesopore diameter of between 1.5 and 30 nm and having microporous crystallised walls with a thickness of between 1 and 60 nm, wherein said elementary spherical particles have a maximum diameter of 200 microns. The invention also relates to the preparation of said material.
摘要翻译：本发明涉及一种在微孔率和中孔率方面具有分级和组织孔隙率的材料，其包含至少两个初级球形颗粒，每个所述颗粒包括介孔直径在1.5以下的含内消旋结构的含硅氧化物基质 30nm，并且具有厚度为1至60nm的微孔结晶壁，其中所述基本球形颗粒具有200微米的最大直径。本发明还涉及所述材料的制备。

7. 发明申请

WO2008132314A3 METHOD FOR THE SYNTHESIS OF CUBIC METAL NANOPARTICLES IN THE PRESENCE OF TWO REDUCERS 审中-公开
标题翻译：在两种还原剂存在下合成金属纳米颗粒的方法
公开(公告)号：WO2008132314A3
公开(公告)日：2008-12-31
申请号：PCT/FR2008000294
申请日：2008-03-05
申请人： INST FRANCAIS DU PETROLE , BISSON LAURENT , THOMAZEAU CECILE , SANCHEZ CLEMENT , BOISSIERE CEDRIC
发明人： BISSON LAURENT , THOMAZEAU CECILE , SANCHEZ CLEMENT , BOISSIERE CEDRIC
IPC分类号： B01J23/40 , B01J23/44 , B01J35/00 , B01J37/03 , B22F9/24 , C10G45/40
CPC分类号： B01J35/0013 , B01J23/40 , B01J23/44 , B01J37/03 , B22F1/0018 , B22F9/24 , B22F9/26 , B22F2001/0037 , B22F2998/00 , B22F2999/00 , B82Y30/00 , C10G45/34 , C10G45/36 , C10G45/40 , B22F2201/013 , B22F1/0025
摘要： The invention relates to a method for preparing cubic metal nanoparticles, comprising: a) the preparation of an aqueous solution containing a source of a metal from group VIII, a reducing compound R1 and a stabiliser; b) the preparation of an aqueous solution containing a source of a metal from group VIII and a stabiliser at a temperature strictly above 70ºC and below or equal to 80ºC; c) the mixing of at least one part of the aqueous solution obtained in step (a) with the aqueous solution obtained in step (b) so as to produce, in the presence of reducer R2, cubic metal nanoparticles representing at least 70% by number of all of the metal nanoparticles formed; and d) the deposition of the metal nanoparticles produced in step (c) on a substrate.
摘要翻译：本发明涉及一种制备立方晶粒纳米颗粒的方法，包括：a）制备含有VIII族金属源，还原性化合物R1和稳定剂的水溶液; b）在严格高于70℃且低于或等于80℃的温度下制备含有VIII族金属源和稳定剂的水溶液; c）将步骤（a）中获得的至少一部分水溶液与步骤（b）中获得的水溶液混合，以在还原剂R2存在下，制备代表至少70％的立方晶系纳米颗粒，形成的所有金属纳米粒子数; 和d）将步骤（c）中制备的金属纳米颗粒沉积在基底上。

8. 发明申请

WO2007057551A3 OXYFLUORIDE IN THE FORM OF A FILM AND PREPARATION METHOD 审中-公开
标题翻译：膜中的氧化物和制备方法
公开(公告)号：WO2007057551A3
公开(公告)日：2007-12-06
申请号：PCT/FR2006002510
申请日：2006-11-13
申请人： UNIV PARIS CURIE , CENTRE NAT RECH SCIENT , GROSSO DAVID , BOISSIERE CEDRIC , SANCHEZ CLEMENT
发明人： GROSSO DAVID , BOISSIERE CEDRIC , SANCHEZ CLEMENT
IPC分类号： C01F5/28 , C01B9/08 , C04B35/553 , G02B1/11
CPC分类号： C01B9/08 , C01F5/28 , C01P2006/14 , C01P2006/60 , C09K11/645 , C09K11/7733 , G02B1/02 , G02B1/113 , Y10T428/249953 , Y10T428/249979 , Y10T428/24999
摘要： The invention relates to a porous nanostructured oxyfluoride film deposited on a substrate, a method for producing the same, and various applications. The oxyfluoride has a porous semi-crystalline structure and a refraction index of between 1.08 and 1.25, measured in the visible range for a relative humidity rate lower than 80 %. The chemical composition thereof corresponds to the formula (Mg (1-x) Ca x ) (1-y) My F (2+(n-2)y-2z-t) O z (OH) t M' w wherein n is the valency of M, n being between 1 and 4, M represents at least one element selected from Al, Si, Ge, and Ga, M' represents at least one element selected from the group consisting of Co, Cr Ni, Fe, Cu, Sb, Ag, Pd, Cd, Au, Sn, Pb, Ce, Nd, Pr, Eu, Yb, Tb, Dy, Er and Gd, and 0 = w 0 and t
摘要翻译：本发明涉及沉积在基底上的多孔纳米结构氟氧化物膜，其制备方法和各种应用。氟氧化物具有多孔半晶体结构，折射率在1.08和1.25之间，在相对湿度低于80％的可见光范围内测量。其化学组成对应于式（Mg（1-x）2）x（x） 2+（n-2）y-2z-t）其中n是（OH） M的化合价n为1〜4，M为选自Al，Si，Ge，Ga中的至少一种元素，M'表示选自Co，Cr Ni，Fe，Cu中的至少一种元素，Sb，Ag，Pd，Cd，Au，Sn，Pb，Ce，Nd，Pr，Eu，Yb，Tb，Dy，Er和Gd，0 = w < 0 = x = 1; 0 = y = 0.5; z <1，z + t> 0和t <2。

9. 发明申请

WO2005003028A3 CALCIUM PHOSPHATE PARTICLES AND PRODUCTION THEREOF 审中-公开
标题翻译：磷酸钙颗粒及其生产
公开(公告)号：WO2005003028A3
公开(公告)日：2005-06-23
申请号：PCT/FR2004001666
申请日：2004-06-29
申请人： RHODIA CHIMIE SA , CHANE-CHING JEAN-YVES , BOISSIERE CEDRIC , MANN STEPHEN
发明人： CHANE-CHING JEAN-YVES , BOISSIERE CEDRIC , MANN STEPHEN
IPC分类号： C01B25/32
CPC分类号： C01B25/32
摘要： The invention relates to particles of calcium phosphate platelets with a monetite structure, the thickness of the platelets being 0.005 µm to 0.2 µm, the porous volume, corresponding to pores with a diameter less than 1 µm, measured with mercury, is at least 0.30 ml/g and having a mean diameter, d50, of 5 µm to 15 µm. Also disclosed are particles of calcium phosphate fibres with apatite structure, the porous volume of which, measured by mercury porosimetry and corresponding to the pores with diameter less than 1 micron, is at least 0.40 ml/g, the specific surface of which is at least 150 m /g and the means diameter, d50, is 5 µm to 15 µm. The invention further relates to a method for the production of said particles of calcium phosphate and the use of said particles, whereby the particles obtained are used as reinforcing filler, thermal insulation filler, pharmaceutical excipient, polishing agent, support material, construction materials, and additive for bucco-dental formulations such as toothpastes or as encapsulating agent.
摘要翻译：本发明涉及具有三斜磷钙石结构的磷酸钙血小板的颗粒，血小板的厚度为0.005μm至0.2μm，对应于用汞测量的直径小于1μm的孔的多孔体积为至少0.30ml / g并且具有5μm至15μm的平均直径d50。还公开了具有磷灰石结构的磷酸钙纤维颗粒，其孔隙体积通过水银孔隙率测量法测量并对应于直径小于1微米的孔隙，其至少0.40ml / g，其比表面至少为 150平方米/克，平均直径d50为5微米至15微米。本发明进一步涉及生产所述磷酸钙颗粒的方法和所述颗粒的用途，由此将所得颗粒用作增强填料，绝热填料，药物赋形剂，抛光剂，载体材料，建筑材料和颊牙用制剂的添加剂，例如牙膏或作为胶囊剂。

10. 发明专利

ZA201000910B Amorphous material having a hierarchised porosity and comprising silicon 未知
公开(公告)号：ZA201000910B
公开(公告)日：2010-10-27
申请号：ZA201000910
申请日：2010-02-08
申请人： INST FRANCAIS DU PETROLE
发明人： CHAUMONNOT ALEXANDRA , COUPE AURELIE , SANCHEZ CLEMENT , BOISSIERE CEDRIC
IPC分类号： B01J20060101 , C01B20060101
摘要： Hierarchical porous material comprises two spherical elementary particles having a maximum diameter of 200 microns, where at least one of the spherical particles comprise a silicon oxide based matrix and having amorphous walls, the material has a macroporous volume measured by mercury porosimetry of 0.05-1 ml/g, a mesoporous volume measured by nitrogen volumetry of 0.01-1 ml/g and a microporous volume measured by nitrogen volumetry of 0.03-0.4 ml/g. An independent claim is included for a preparation of the material, comprising preparing a clear solution containing precursor elements of zeolite germs, such as structuring agent, at least a silica precursor and optionally at least a precursor of an element X comprising aluminum, iron, boron, indium and gallium, mixing at least one surfactant and the clear solution into a solution, spraying the solution by aerosol obtained in the mixing step for the formation of spherical droplets, drying the droplets, and eliminating the structuring agent and the surfactant to obtain an amorphous material with hierarchical porosity in the range of microporosity, mesoporosity and macroporosity.

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