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1. 发明专利

PL162476B1 METHOD OF TREATMENT OF EXTRAGRADE PANTAERYTHRITE 未知
公开(公告)号：PL162476B1
公开(公告)日：1993-12-31
申请号：PL28656490
申请日：1990-08-16
申请人： INST CIEZKIEJ SYNTEZY ORGA
发明人： TRYBULA STANISLAW , TERELAK KAZIMIERZ , WANTUCH WIESLAW , BORON KAZIMIERZ , BALCEROWIAK WOJCIECH , CYPCAR WIKTOR , PLOSZAJ ANTONI , PERS MICHAL , KROSZKE JANINA
IPC分类号： C07C31/24

2. 发明专利

PL162729B1 METHOD OF OBTAINING THRIMETHYL PROPANE 未知
公开(公告)号：PL162729B1
公开(公告)日：1994-01-31
申请号：PL28506490
申请日：1990-05-04
申请人： INST CIEZKIEJ SYNTEZY ORGA
发明人： TERELAK KAZIMIERZ , PERS MICHAL , MAJCHRZAK MARIA , TRYBULA STANISLAW , NOWAKOWSKI STANISLAW , ZIMOCH JOLANTA , PLOSZAJ ANTONI , WANTUCH WIESLAW , BORON KAZIMIERZ , GAJOS WLADYSLAW , CYPCAR WIKTOR
IPC分类号： C07C31/26
摘要： The method for obtaining trimethylolpropane from n-butane and formaldehyde in water solution, at the presence of strong-alkali-reaction anion exchangers as catalysts applied as a stationary layer, characterized in that the mixture is so prepared by dissolving n-butane in the post-synthesis mixture (from the previous synthesis) that the n-butane concentration is equal to 3-4% per weight, and then technical formalin is added to the solution, whereas formalin does not include more than 2% methanol per weight, and the amount of formalin is such that the n-butane/formaldehyde ratio per weight is 1:3.5-1:5, and preferably 1:4.0-1:4.5, and then the solution is stirred and left for stratification, and then the undissolved contamination is removed, and the purified synthesis mixture is applied on a catalyst bed in such amount that the catalyst load is 0.4-0.6 moles of n-butane per dm of catalyst, and the flow is equal to the 1.5-2 hours of substitute contact time, and after dosing the material mixture, the catalyst is rinsed with the distillate from the concentration process of trimethylolpropane that contains 0.5-1.5% per weight of formaldehyde, whereas during the synthesis and the rinsing of the catalyst bed, reflux is received all the time and the first part thereof that does not contain reagents is directed as the finished product, and the other part being received before the rinsing finish, is split in two streams, whereas one stream of 60-61% is returned for preparing the synthesis mixture, and the other stream is directed to the trimethylolpropane separation station.

3. 发明专利

PL286564A1 METHOD OF TREATMENT OF EXTRAGRADE PANTAERYTHRITE 未知
公开(公告)号：PL286564A1
公开(公告)日：1992-02-24
申请号：PL28656490
申请日：1990-08-16
申请人： INST CIEZKIEJ SYNTEZY ORGA
发明人： TRYBULA STANISLAW , TERELAK KAZIMIERZ , WANTUCH WIESLAW , BORON KAZIMIERZ , BALCEROWIAK WOJCIECH , CYPCAR WIKTOR , PLOSZAJ ANTONI , PERS MICHAL , KROSZKE JANINA
IPC分类号： C07C31/24

4. 发明专利

PL284570A1 MET5HOD OF OBTEINING TETRANITRATE 未知
公开(公告)号：PL284570A1
公开(公告)日：1991-10-07
申请号：PL28457090
申请日：1990-03-30
申请人： INST CIEZKIEJ SYNTEZY ORGA
发明人： TERELAK KAZIMIERZ , TRYBULA STANISLAW , WANTUCH WIESLAW , PERS MICHAL , BORON KAZIMIERZ , GAJOS WLADYSLAW , PLOSZAJ ANTONI , CYPCAR WIKTOR , WOJCICKI HENRYK
IPC分类号： C07C31/24

6. 发明专利

PL273240A1 METHOD OF OBTAINING PENTAERITHRITE 未知
公开(公告)号：PL273240A1
公开(公告)日：1989-12-27
申请号：PL27324088
申请日：1988-06-20
申请人： INST CIEZKIEJ SYNTEZY ORGA
发明人： TERELAK KAZIMIERZ , TRYBULA STANISLAW , WANTUCH WIESLAW , CYPCAR WIKTOR , BORON KAZIMIERZ , PERS MICHAL , BALCEROWIAK WOJCIECH , WOJCICKI HENRYK
IPC分类号： C07C20060101 , C07C31/24 , C07C

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