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1. 发明公开

EP1581589A2 PHENOLIC MODIFIED RESORCINOLIC RESINS FOR RUBBER COMPOUNDING 有权转让
标题翻译：酚化合物改性的间苯二酚的橡胶配合
公开(公告)号：EP1581589A2
公开(公告)日：2005-10-05
申请号：EP03813452.4
申请日：2003-12-12
申请人： INDSPEC CHEMICAL CORPORATION , Durairaj, Raj B. , Walkup, C. Michael , Lawrence, Mark A.
发明人： DURAIRAJ, Raj, B. , WALKUP, C., Michael , LAWRENCE, Mark, A.
IPC分类号： C08L21/00
CPC分类号： C08L61/06 , C08L7/00 , C08L21/00 , C08L61/12 , C08L2666/16 , C08L2666/04
摘要： A vulcanizable rubber composition comprises (a) a rubber component; (b) a methylene donor compound; and (c) a methylene acceptor comprising a blend of a high ortho-ortho bonded phenolic novolak resin and a resorcinolic resin. The resin blend can be made by a number of methods. For example, it can be prepared by first reacting one or more phenolic compounds represented by the following formula: where R is selected from the group consisting of H, an alkyl group of 1-16 carbon atoms and an aralkyl group of 8-12 carbon atoms with an aldehyde in the presence of an ortho directing catalyst and then combining a resorcinol-formaldehyde novolak resin to obtain a phenolic and resorcinolic novolak resin blend.

2. 发明授权

EP1581589B1 PHENOLIC MODIFIED RESORCINOLIC RESINS FOR RUBBER COMPOUNDING 有权转让
标题翻译：酚化合物改性的间苯二酚的橡胶配合
公开(公告)号：EP1581589B1
公开(公告)日：2011-01-26
申请号：EP03813452.4
申请日：2003-12-12
申请人： INDSPEC CHEMICAL CORPORATION , Durairaj, Raj B. , Walkup, C. Michael , Lawrence, Mark A.
发明人： DURAIRAJ, Raj, B. , WALKUP, C., Michael , LAWRENCE, Mark, A.
IPC分类号： C08L21/00
CPC分类号： C08L61/06 , C08L7/00 , C08L21/00 , C08L61/12 , C08L2666/16 , C08L2666/04
摘要： A vulcanizable rubber composition comprises (a) a rubber component; (b) a methylene donor compound; and (c) a methylene acceptor comprising a blend of a high ortho-ortho bonded phenolic novolak resin and a resorcinolic resin. The resin blend can be made by a number of methods. For example, it can be prepared by first reacting one or more phenolic compounds represented by the following formula: where R is selected from the group consisting of H, an alkyl group of 1-16 carbon atoms and an aralkyl group of 8-12 carbon atoms with an aldehyde in the presence of an ortho directing catalyst and then combining a resorcinol-formaldehyde novolak resin to obtain a phenolic and resorcinolic novolak resin blend.

3. 发明申请

WO2004055106A2 PHENOLIC MODIFIED RESORCINOLIC RESINS FOR RUBBER COMPOUNDING 审中-公开
标题翻译：酚醛树脂改性酚醛树脂
公开(公告)号：WO2004055106A2
公开(公告)日：2004-07-01
申请号：PCT/US2003/039823
申请日：2003-12-12
申请人： INDSPEC CHEMICAL CORPORATION , DURAIRAJ, Raj, B. , WALKUP, C., Michael , LAWRENCE, Mark, A.
发明人： DURAIRAJ, Raj, B. , WALKUP, C., Michael , LAWRENCE, Mark, A.
IPC分类号： C08L21/00
CPC分类号： C08L61/06 , C08L7/00 , C08L21/00 , C08L61/12 , C08L2666/16 , C08L2666/04
摘要： A vulcanizable rubber composition comprises (a) a rubber component; (b) a methylene donor compound; and (c) a methylene acceptor comprising a blend of a high ortho-ortho bonded phenolic novolak resin and a resorcinolic resin. The resin blend can be made by a number of methods. For example, it can be prepared by first reacting one or more phenolic compounds represented by the following formula: where R is selected from the group consisting of H, an alkyl group of 1-16 carbon atoms and an aralkyl group of 8-12 carbon atoms with an aldehyde in the presence of an ortho directing catalyst and then combining a resorcinol-formaldehyde novolak resin to obtain a phenolic and resorcinolic novolak resin blend.
摘要翻译：可硫化橡胶组合物包含（a）橡胶组分; （b）亚甲基给体化合物; 和（c）亚甲基受体，其包含高邻位键合酚醛清漆树脂和间苯二酚树脂的共混物。树脂混合物可以通过多种方法制备。例如，可以通过首先使一种或多种由下式表示的酚类化合物反应来制备：其中R选自H，1-16个碳原子的烷基和8-12个碳原子的芳烷基原子与邻位导向催化剂存在下的醛，然后混合间苯二酚 - 甲醛酚醛清漆树脂，得到酚醛和酚醛树脂的酚醛清漆树脂混合物。

4. 发明申请

WO2006036760A3 MODIFIED PHENOLIC NOVOLAK RESINS AND APPLICATIONS THEREOF 审中-公开
公开(公告)号：WO2006036760A3
公开(公告)日：2006-04-06
申请号：PCT/US2005/034059
申请日：2005-09-23
申请人： INDSPEC CHEMICAL CORPORATION , DURAIRAJ, Raj, B. , WALKUP, Michael, C. , LAWRENCE, Mark, A.
发明人： DURAIRAJ, Raj, B. , WALKUP, Michael, C. , LAWRENCE, Mark, A.
IPC分类号： C08G8/04
摘要： A modified phenolic novolak resin is prepared by reacting a phenolic compound (e.g., resorcinol) with an aliphatic polyol. The reaction mixture further reacts with a formaldehyde to produce a modified phenolic novolak resin. The reaction is typically carried out in the presence of an acid or a base catalyst. The resulting resin is characterized by a relatively low level of free resorcinol; and rubber compounds containing the resin exhibit low fuming, lower Mooney viscosity (which means better processing), better dynamic stiffness properties (G'), and/or good tear properties. Therefore, the resulting resin can be used as a methylene acceptor compound in a vulcanizable rubber composition.

5. 发明申请

WO2007106186A3 RESORCINOL RESIN-BLOCKED ISOCYANATES AND THEIR APPLICATIONS 审中-公开
公开(公告)号：WO2007106186A3
公开(公告)日：2007-09-20
申请号：PCT/US2006/061353
申请日：2006-11-29
申请人： INDSPEC CHEMICAL CORPORATION , DURAIRAJ, Raj, B. , JESIONOWSKI, Gary, A. , LAWRENCE, Mark, A.
发明人： DURAIRAJ, Raj, B. , JESIONOWSKI, Gary, A. , LAWRENCE, Mark, A.
IPC分类号： C08G18/54 , C08G8/28 , C09D161/12 , C09D175/16
摘要： Resorcinol resin-blocked isocyanate compositions are derived from the reaction between a resorcinol resin and at least two different isocyanate compounds. The resorcinol resin-blocked isocyanate compositions may have two or more unblocking temperatures and/or melting characteristics that may provide some unique properties, such as improved adhesion of reinforcing materials to rubber compounds. The resorcinol resin-blocked isocyanate compositions can be used in fabric dipping formulations and/or rubber compositions with improved properties.

6. 发明申请

WO2004055085A1 FLEXIBILIZED RESORCINOLIC NOVOLAK RESINS AND METHOD OF MAKING SAME 审中-公开
标题翻译：柔性酚醛清漆树脂及其制备方法
公开(公告)号：WO2004055085A1
公开(公告)日：2004-07-01
申请号：PCT/US2003/039839
申请日：2003-12-12
申请人： INDSPEC CHEMICAL CORPORATION , DURAIRAJ, Raj, B. , LAWRENCE, Mark, A.
发明人： DURAIRAJ, Raj, B. , LAWRENCE, Mark, A.
IPC分类号： C08G8/04
CPC分类号： C08G8/08 , C08G8/04 , C08G8/10 , C08G8/22 , C09J161/06 , C09J161/12
摘要： A flexibilized resorcinolic novolak resin is prepared by reacting a phenolic compound, such as resorcinol, with an unsaturated dihydroxy, an unsaturated aldehyde, an aliphatic dialdehyde, or a mixture thereof. An aldehyde (different from the unsaturated aldehyde and the aliphatic dialdehyde) is either simultaneously or subsequently added to the reaction mixture. The flexibilized resorcinolic novolak resin can be used in an adhesive composition for enhancing the adhesion between tire cords and rubber for tire applications.
摘要翻译：通过使酚类化合物（例如间苯二酚）与不饱和二羟基，不饱和醛，脂族二醛或其混合物反应来制备增韧的间苯二酚酚醛清漆树脂。醛（不同于不饱和醛和脂族二醛）同时或随后加入到反应混合物中。可挠曲的间苯二酚酚醛清漆树脂可用于增强轮胎帘线和用于轮胎应用的橡胶之间的粘合性的粘合剂组合物中。

7. 发明申请

WO2007100399A1 RESORCINOL-BLOCKED ISOCYANATE COMPOSITIONS AND THEIR APPLICATIONS 审中-公开
标题翻译： RESORCINOL封闭的异氰酸酯组合物及其应用
公开(公告)号：WO2007100399A1
公开(公告)日：2007-09-07
申请号：PCT/US2006/061348
申请日：2006-11-29
申请人： INDSPEC CHEMICAL CORPORATION , DURAIRAJ, Raj, B. , JESIONOWSKI, Gary, A. , LAWRENCE, Mark, A.
发明人： DURAIRAJ, Raj, B. , JESIONOWSKI, Gary, A. , LAWRENCE, Mark, A.
IPC分类号： C08G18/80
CPC分类号： C08G18/8019 , C07C271/58 , C08G18/7671 , C08G18/8067 , C08G18/8074 , C08G2170/80 , C08G2190/00 , C08G2380/00 , C08L21/00 , C08L61/04 , C08L2666/16
摘要： Resorcinol-blocked isocyanate compositions are derived from the reaction between a resorcinol compound and at least two different isocyanate compounds. The resorcinol-blocked isocyanate compositions may have two or more unblocking temperatures and/or melting characteristics that may provide some unique properties, such as improved adhesion of rubber reinforcing materials to rubber materials or compounds. The resorcinol-blocked isocyanate compositions can be used in fabric dipping formulations and/or rubber compositions with improved properties.
摘要翻译：间苯二酚封闭的异氰酸酯组合物衍生自间苯二酚化合物和至少两种不同的异氰酸酯化合物之间的反应。间苯二酚封闭的异氰酸酯组合物可以具有两个或多个未阻断的温度和/或熔融特性，其可以提供一些独特的性质，例如改善橡胶增强材料对橡胶材料或化合物的粘合性。间苯二酚封闭的异氰酸酯组合物可用于具有改进性能的织物浸渍制剂和/或橡胶组合物中。

8. 发明申请

WO2006036880A2 PHOSPHATE ESTER FLAME RETRADANTS FROM RESORCINOL-KETONE REACTION PRODUCTS 审中-公开
标题翻译：来自间苯二酚酮酮反应产物的磷酸酯火焰回收剂
公开(公告)号：WO2006036880A2
公开(公告)日：2006-04-06
申请号：PCT/US2005/034391
申请日：2005-09-21
申请人： INDSPEC CHEMICAL CORPORATION , DURAIRAJ, Raj, B. , JESIONOWSKI, Gary, A.
发明人： DURAIRAJ, Raj, B. , JESIONOWSKI, Gary, A.
IPC分类号： C08K5/49
CPC分类号： C07F9/65522 , C08K5/529
摘要： Flavan-based and spirodichroman compound-based phosphate esters prepared by reacting flavans and spirodichroman compounds with phosphorus oxychloride, monophenyl dichlorophosphate, or diphenyl chlorophosphate compounds are described. The flavans and spirodichroman compounds can be synthesized by the reaction of resorcinol with aliphatic acetone. Such phosphate esters can be used as flame retardants.
摘要翻译：描述了通过使黄烷和螺二氢二苯并吡喃化合物与三氯氧化磷，单苯基二氯磷酸酯或二苯基氯磷酸酯化合物反应制备的基于黄烷和螺二氢噻吩类化合物的磷酸酯。黄烷和spirodichroman化合物可以通过间苯二酚与脂族丙酮的反应合成。这种磷酸酯可以用作阻燃剂。

9. 发明申请

WO2004074340A1 MODIFIED RESORCINOL RESINS AND APPLICATIONS THEREOF 审中-公开
标题翻译：改性聚烯烃树脂及其应用
公开(公告)号：WO2004074340A1
公开(公告)日：2004-09-02
申请号：PCT/US2004/004428
申请日：2004-02-13
申请人： INDSPEC CHEMICAL CORPORATION , DURAIRAJ, Raj, B. , LAWRENCE, Mark
发明人： DURAIRAJ, Raj, B. , LAWRENCE, Mark
IPC分类号： C08G8/30
CPC分类号： C08G8/22 , C08G8/30
摘要： A modified resorcinol resin is prepared by reacting a phenolic compound (e.g., resorcinol) with an olefinically unsaturated compound (e.g., styrene) and two types of aldehyde: a formaldehyde and an alkyl aldehyde (e.g., butyraldehyde). The reaction is typically carried out in the presence of an acid catalyst. The resulting resin has a lower softening point and can be used as a methylene acceptor compound in a vulcanizable rubber composition.
摘要翻译：通过使酚类化合物（例如间苯二酚）与烯属不饱和化合物（例如苯乙烯）和两种醛：甲醛和烷基醛（例如丁醛）反应来制备改性间苯二酚树脂。反应通常在酸催化剂的存在下进行。所得树脂具有较低的软化点，可用作可硫化橡胶组合物中的亚甲基受体化合物。

10. 发明申请

WO2007005086A1 PROCESS FOR MAKING PHENYLENE DIOXYDIACETIC ACID AND USE THEREOF 审中-公开
标题翻译：制备苯乙烯二酸的方法及其用途
公开(公告)号：WO2007005086A1
公开(公告)日：2007-01-11
申请号：PCT/US2006/013768
申请日：2006-04-13
申请人： INDSPEC CHEMICAL CORPORATION , DURAIRAJ, Raj, B. , TACKIE, Michael, N.
发明人： DURAIRAJ, Raj, B. , TACKIE, Michael, N.
IPC分类号： C08G63/78 , C08G63/672 , C07C51/367 , C07C59/70
CPC分类号： C08G63/672 , C07C51/367 , C07C59/70
摘要： A process for making phenylene dioxydiacetic acid comprises (a) contacting a dihydroxybenzene under reaction conditions with a salt of haloacetic acid in a solution without adding a haloacetic acid to produce a salt of phenylene dioxydiacetic acid; and (b) optionally converting the salt of phenylene dioxydiacetic acid to free phenylene dioxydiacetic acid. In some embodiments, 1,3-phenylene dioxydiacetic acid (RDOA) is made by reacting resorcinol with sodium chloroacetic acid in a reaction mixture with a pH in the range of about 7 to about 11 and at a temperature from about 70 °C to 105 °C. By adjusting the reactions conditions, a relatively high yield of 1,3-phenylene dioxydiacetic acid (i.e., greater than 80%) is obtained. The purified acid can be used in the synthesis of polyester, such as polyethylene terephthalate.
摘要翻译：制备亚苯基二氧基二乙酸的方法包括（a）在反应条件下使二羟基苯与卤代乙酸盐在溶液中接触而不添加卤代乙酸以产生亚苯基二氧二肟酸的盐; 和（b）任选将亚苯基二氧代二乙酸的盐转化为游离的亚苯基二氧基二乙酸。在一些实施方案中，1,3-亚苯基二氧二氢乙酸（RDOA）是通过使间苯二酚与氯乙酸钠在反应混合物中反应制备的，反应混合物的pH为约7至约11，温度为约70℃至105℃ C。通过调整反应条件，可以获得相当高的1,3-亚苯基二氧二氢乙酸的收率（即大于80％）。纯化的酸可用于合成聚酯，如聚对苯二甲酸乙二醇酯。

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